CO2 electrolysis – Complementary operando XRD, XAS and Raman spectroscopy study on the stability of CuxO foam catalysts

2020 ◽  
Vol 389 ◽  
pp. 592-603 ◽  
Author(s):  
Abhijit Dutta ◽  
Motiar Rahaman ◽  
Burkhard Hecker ◽  
Jakub Drnec ◽  
Kiran Kiran ◽  
...  
1997 ◽  
Vol 51 (1) ◽  
pp. 101-107 ◽  
Author(s):  
H. G. M. Edwards ◽  
D. W. Farwell ◽  
J. M. C. Turner ◽  
A. C. Williams

The adaptation and construction of an environmental chamber suitable for FT-Raman spectroscopy is described for the recording of Raman spectra of specimens at temperatures from 25 to 125 °C while exposed to different controlled synthetic atmospheric conditions. Test spectra were obtained from sulfur to illustrate the stability and applications of the system. The α rhombic/β monoclinic phase change in sulfur was monitored as a function of time, and bands sensitive to this phase change have been identified.


2013 ◽  
Vol 57 (1) ◽  
pp. 3111-3117 ◽  
Author(s):  
V. Duboviks ◽  
R. C. Maher ◽  
G. Offer ◽  
L. F. Cohen ◽  
N. P. Brandon

2018 ◽  
Vol 2018 ◽  
pp. 1-13 ◽  
Author(s):  
Kodanda Rama Rao Chebattina ◽  
V. Srinivas ◽  
N. Mohan Rao

The aim of the paper is to investigate the effect of size of multiwalled carbon nanotubes (MWCNTs) as additives for dispersion in gear oil to improve the tribological properties. Since long pristine MWCNTs tend to form clusters compromising dispersion stability, they are mildly processed in a ball mill to shorten the length and stabilized with a surfactant before dispersing in lubricant. Investigations are made to assess the effect of ball milling on the size and structure of MWCNTs using electron microscopy and Raman spectroscopy. The long and shortened MWCNTs are dispersed in EP 140 gear oil in 0.5% weight. The stability of the dispersed multiwalled carbon nanotubes is evaluated using light scattering techniques. The antiwear, antifriction, and extreme pressure properties of test oils are evaluated on a four-ball wear tester. It is found that ball milling of MWCNTs has a strong effect on the stability and tribological properties of the lubricant. From Raman spectroscopy, it is found that ball milling time of up to 10 hours did not produce any defects on the surface of MWCNTs. The stability of the lubricant and the antiwear, antifriction, and extreme pressure properties have improved significantly with dispersion shortened MWCNTs. Ball milling for longer periods produces defects on the surface of MWCNTs reducing their advantage as oil additives.


2015 ◽  
Vol 57 (11) ◽  
pp. 2286-2289 ◽  
Author(s):  
A. S. Oreshonkov ◽  
A. K. Khodzhibaev ◽  
A. S. Krylov ◽  
M. F. Umarov ◽  
A. N. Vtyurin

Author(s):  
Nicolas Bisbrouck ◽  
Marco Bertani ◽  
Frédéric Angeli ◽  
Thibault Charpentier ◽  
Dominique de Ligny ◽  
...  

Author(s):  
Shuo Zhang ◽  
Hongsheng Jia ◽  
Mingxing Song ◽  
He Shen ◽  
Li Dongfei ◽  
...  

2021 ◽  
Vol 606 ◽  
pp. 412726
Author(s):  
Gabriela Gomes Miranda ◽  
Raphael Lucas de Sousa e Silva ◽  
Hermínia Veridiana dos Santos Pessoni ◽  
A. Franco

2016 ◽  
Vol 61 (3) ◽  
pp. 428-431
Author(s):  
A. A. Yugov ◽  
A. A. Donskov ◽  
T. G. Yugova ◽  
I. A. Belogorohov ◽  
Yu. N. Parhomenko

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