Comparison of fracture resistance as measured by the indentation fracture method and fracture toughness determined by the single-edge-precracked beam technique using silicon nitrides with different microstructures

2007 ◽  
Vol 27 (6) ◽  
pp. 2347-2354 ◽  
Author(s):  
Hiroyuki Miyazaki ◽  
Hideki Hyuga ◽  
Kiyoshi Hirao ◽  
Tatsuki Ohji
2009 ◽  
Vol 409 ◽  
pp. 308-312
Author(s):  
Jana Špaková ◽  
Ján Dusza

Study compare R-curve behaviour of silicon nitride obtained using Vickers indented beam specimens and single edge V-notched beam (SEVNB). R-curve measurement realized by Vickers indented beam was reported by Krause. Crack growth using single edge V-notched beam was observed in situ. The indentation experiments, in comparison with SEVNB method revealed higher R-curve values (KR=3.3 – 4.8 MPa.m1/2). The discrepancy in the R-curve results is attributed to inaccuracy related to the determination of indentation toughness. The indentation fracture toughness may include the aspects of crack opening behaviour, residual indentation stress intensity.


2008 ◽  
Vol 403 ◽  
pp. 53-56
Author(s):  
Hiroyuki Miyazaki ◽  
Hideki Hyuga ◽  
Yuichi Yoshizawa ◽  
Kiyoshi Hirao ◽  
Tatsuki Ohji

Six kinds of silicon nitrides with different microstructures were fabricated by changing the amount of sintering additives, Al2O3 and Y2O3. The hardness decreased with an increase in the amount of additives, whereas the indentation fracture resistance increased in the samples with large amount of additives due to the formation of coarse and elongated grains. The wear property of various Si3N4 ceramics was investigated in the sliding contact test without lubricant and was compared with the mechanical properties. The specific wear rate varied notably from 4x10-4 to 6x10-6 mm-3N-1m-1 depending on the compositions, which was difficult to explain directly from the hardness and fracture resistance. An indentation fracture model for material removal could correlate the wear properties with a function of hardness and fracture resistance of the materials, suggesting that the indentation model was likely to be valid for analyzing the wear behavior in this study.


2021 ◽  
Author(s):  
Abay Namen ◽  
Radu Iovita ◽  
Klaus G. Nickel ◽  
Aristeidis Varis ◽  
Zhaken Taimagambetov ◽  
...  

The study of lithic raw material quality has become one of the major interpretive tools to investigate the raw material selection behaviour and its influence to the knapping technology. In order to make objective assessments of raw material quality, their mechanical properties (e.g., fracture resistance, hardness, modulus of elasticity) should be measured. However, such comprehensive investigations are lacking for the Palaeolithic of Kazakhstan. In this work, we investigate geological and archaeological lithic raw material samples of chert, porphyry, and shale collected from the Inner Asian Mountain Corridor (henceforth IAMC). Selected samples of aforementioned rocks were tested by means of Vickers and Knoop indentation methods to determine one aspect of their mechanical properties: their indentation fracture resistance (a value closely related to fracture toughness). These tests were complemented by traditional petrographic studies to characterise the mineralogical composition and evaluate the level of impurities that could have potentially affected the mechanical properties. The results show that materials, such as porphyry, previously thought to be of lower quality due to the anisotropic composition and coarse feldspar and quartz phenocrysts embedded in a silica rich matrix, possess fracture toughness values that can be compared to those of chert. Thus, it appears that different raw materials cannot be distinguished from the point of view of indentation fracture resistance, calling for detailed supplementary analyses of different fracture properties. This work also offers first insight into the quality of archaeological porphyry that was utilised as a primary raw material at various Middle and Upper Palaeolithic sites in the IAMC.


1995 ◽  
Vol 410 ◽  
Author(s):  
Leszek Hozer ◽  
Yet-Ming Chiang ◽  
Svetlana Ivanova ◽  
Isa Bar-On

ABSTRACTIn this paper we demonstrate a liquid exchange process to introduce a ductile metal reinforcement phase in the amount of 10–30 vol. % into reaction-bonded silicon carbides (RBSCs). Immersion of RBSC in pure Al or Al-Si melts enables diffusional replacement of secondary phase silicon with metal. The Al and Al-Si exchanged composites show improvement in fracture toughness (single edge precracked beam technique) to 6–7 MPa·m1/2 as compared to 3–4 MPa·m1/2 in otherwise similar siliconized silicon carbide. Increased fracture strength (four point flexure) was also observed after the liquid exchange process.


1997 ◽  
Vol 12 (7) ◽  
pp. 1785-1789 ◽  
Author(s):  
Leszek Hozer ◽  
Yet-Ming Chiang ◽  
Svetlana Ivanova ◽  
Isa Bar-On

In this paper we demonstrate a novel liquid-exchange process to replace a secondary silicon phase in reaction-bonded siliconized silicon carbides (RBSC's) with a ductile metal reinforcement phase. When RBSC is exchanged with pure Al or Al–Si liquid, secondary phase silicon is dissolved and is substituted by Al or Al–Si alloy. The resulting composites show improvements in fracture toughness (single-edge precracked beam technique), with KIC value up to 8.6 Mpa · m1/2, compared to 3–4 MPa · m1/2 in otherwise similar siliconized silicon carbide. Increased fracture strength (four point flexure) was also observed after the liquid exchange process. The processing furthermore allows the coefficient of thermal expansion to be adjusted, and the thermal conductivity increased, for electronic packaging applications.


2007 ◽  
Vol 352 ◽  
pp. 45-48 ◽  
Author(s):  
Hiroyuki Miyazaki ◽  
Hideki Hyuga ◽  
Yuichi Yoshizawa ◽  
Kiyoshi Hirao ◽  
Tatsuki Ohji

The influence of two measuring conditions, the elapsed time after indentation and the condition of edge of an indenter, on the indentation fracture toughness of silicon nitrides was assessed. No slow crack-growth after unloading was confirmed by optical microscopic observation of a crack tip induced by the indentation, which led to the negligible difference in fracture toughness measured at 1 and 30 min after the indentation. Measurements with relatively new and used indenters gave almost the same fracture toughness data, indicating that the crack lengths were hardly affected by the slight damage of the corner of the indenter. It was suggested that the large scattering of the indentation fracture toughness reported by the round-robin tests such as VAMAS was not originated from these factors.


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