Multinuclear NMR screening of pharmaceuticals using standardization by 2H integral of a deuterated solvent

2021 ◽  
pp. 114530
Author(s):  
Yulia B. Monakhova ◽  
Bernd W.K. Diehl
Keyword(s):  
Nmr Screening ◽  
Multinuclear Nmr

Arylation of enelactams using TIPSOTf: reaction scope and mechanistic insight

2021 ◽  
Author(s):  
Tomasz J. Idzik ◽  
Zofia M. Myk ◽  
Łukasz Struk ◽  
Magdalena Perużyńska ◽  
Gabriela Maciejewska ◽  
...  
Keyword(s):  
Reaction Mechanism ◽  
Multinuclear Nmr ◽  
Mechanistic Insight ◽  
Nmr Study ◽  
Wide Range

Triisopropylsilyltrifluoromethanesulfonate can be effectively used for the arylation of a wide range of enelactams. The multinuclear NMR study provided deep insights into the reaction mechanism.

NMR screening of Greek olive oils

Planta Medica ◽  
2014 ◽  
Vol 80 (16) ◽  
Author(s):  
A Argyropoulou ◽  
D Benaki ◽  
M Spraul ◽  
H Schaefer ◽  
AL Skaltsounis ◽  
...  
Keyword(s):  
Nmr Screening ◽  
Olive Oils

scholarly journals Dichloro(η6-p-cymene)(P,P-diphenyl-N-propyl-phosphinous amide-κP)ruthenium(II)

Molbank ◽  
10.3390/m1217 ◽  
2021 ◽  
Vol 2021 (2) ◽  
pp. M1217
Author(s):  
Rebeca González-Fernández ◽  
Pascale Crochet ◽  
Victorio Cadierno
Keyword(s):  
Ir Spectroscopy ◽  
Elemental Analysis ◽  
Title Compound ◽  
Room Temperature ◽  
Toluene Solution ◽  
Catalytic Behavior ◽  
Multinuclear Nmr

The title compound, i.e., [RuCl2(η6-p-cymene)(PPh2NHnPr)] (2), was obtained in a 71% yield by reacting a toluene solution of the chlorophosphine complex [RuCl2(η6-p-cymene)(PPh2Cl)] (1) with two equivalents of n-propylamine at room temperature. The aminophosphine complex 2 was characterized by elemental analysis, multinuclear NMR (31P{1H}, 1H and 13C{1H}) and IR spectroscopy. In addition, its catalytic behavior in the hydration of benzonitrile was briefly explored.

Automation of Biomolecular NMR Screening

2003 ◽  
Vol 3 (1) ◽  
pp. 55-67 ◽  
Author(s):  
Alfred Ross ◽  
Hans Senn
Keyword(s):  
Nmr Screening ◽  
Biomolecular Nmr
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