In-situ SEM study of crack initiation, propagation and interfacial debonding of Ni-P coating during tensile tests: Heat treatment effect

2017 ◽  
Vol 123 ◽  
pp. 106-114 ◽  
Author(s):  
H. Bouaziz ◽  
O. Brinza ◽  
N. Haddar ◽  
M. Gasperini ◽  
M. Feki
Keyword(s):  
Heat Treatment ◽  
Crack Initiation ◽  
Treatment Effect ◽  
Tensile Tests ◽  
Interfacial Debonding ◽  
Sem Study

scholarly journals Study of the Microstructure and Crack Evolution Behavior of Al-5Fe-1.5Er Alloy

Materials ◽  
2019 ◽  
Vol 12 (1) ◽  
pp. 172 ◽  
Author(s):  
Ming Li ◽  
Zhiming Shi ◽  
Xiufeng Wu ◽  
Huhe Wang ◽  
Yubao Liu
Keyword(s):  
Electron Microscopy ◽  
Crack Initiation ◽  
Tensile Tests ◽  
Eutectic Structure ◽  
Interface Structure ◽  
X Ray ◽  
Transmission Electron ◽  
The Matrix ◽  
Evolution Behavior

In this work, the microstructure of Al-5Fe-1.5Er alloy was characterized and analyzed using X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM) and energy-dispersive X-ray spectroscopy (EDS) techniques. The effect of microstructure on the behavior of crack initiation and propagation was investigated using in situ tensile testing. The results showed that when 1.5 wt.% Er was added in the Al-5Fe alloy, the microstructure consisted of α-Al matrix, Al3Fe, Al4Er, and Al3Fe + Al4Er eutectic phases. The twin structure of Al3Fe phase was observed, and the twin plane was {001}. Moreover, a continuous concave and convex interface structure of Al4Er was observed. Furthermore, Al3Fe was in the form of a sheet with a clear gap inside. In situ tensile tests of the alloy at room temperature showed that the crack initiation mainly occurred in the Al3Fe phase, and that the crack propagation modes included intergranular and trans-granular expansions. The crack trans-granular expansion was due to the strong binding between Al4Er phases and surrounding organization, whereas the continuous concave and convex interface structure of Al4Er provided a significant meshing effect on the matrix and the eutectic structure.

scholarly journals Study of the Microstructure and Crack Evolution Behavior of Al-5Fe-1.5Er Alloy

2018 ◽  
Author(s):  
Ming Li ◽  
Zhiming Shi ◽  
Xiufeng Wu ◽  
Huhe Wang ◽  
Yubao Liu
Keyword(s):  
Crack Initiation ◽  
Tensile Tests ◽  
Eutectic Structure ◽  
Interface Structure ◽  
Crack Evolution ◽  
Binding Ability ◽  
Initiation And Propagation ◽  
The Matrix ◽  
Evolution Behavior

The microstructure of Al-5Fe-1.5Er alloy was characterized and analyzed by using XRD, SEM, TEM and EDS. The effect of microstructure on the behavior of crack initiation and propagation was investigated by in situ tensile testing. Results show that the microstructure consists of α-Al matrix, Al3Fe, Al4Er, eutectic phase Al3Fe + Al4Er, while the 1.5 wt.% Er was added in Al-5Fe alloy. The twin structure of the Al3Fe phase was observed, and the twin plane is {001}. Moreover, a continuous concave and convex interface structure of the Al4Er has been found. Al3Fe is in the form of a sheet with a clear gap inside.In situ tensile tests of the alloy at room temperature show that the crack initiation occured mainly in the Al3Fe phase, and that the crack propagation modes include intergranular and transgranular expansion. Crack transgranular expansion is due to the strong binding ability between Al4Er phases and surrounding organization, and the continuous concave and convex interface structure of the Al4Er provides a significant meshing effect on the matrix and eutectic structure.

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