Single step solution combustion synthesis of hexagonal WO3 powders as visible light photocatalysts

2020 ◽  
Vol 240 ◽  
pp. 122152 ◽  
Author(s):  
S. Samet Kaplan ◽  
M. Seref Sonmez
2009 ◽  
Vol 24 (1) ◽  
pp. 245-252 ◽  
Author(s):  
Robert Ianoş

Single-phase nanocrystalline 4CaO·Al2O3·Fe2O3 powders were prepared directly from the combustion reaction using a new cost-effective, time-saving, and environmentally friendly version of solution combustion synthesis. Instead of a single fuel, a fuel mixture of urea and β-alanine was used. It was shown by x-ray diffraction, energy-dispersive x-ray analysis, thermogravimetric analysis, and optical microscopy that this new version of the solution combustion synthesis allows the maximization of the exothermic effect associated with the combustion reaction. On the other hand, it was shown that the traditional version of combustion synthesis involving the use of a single fuel, such as urea or β-alanine, does not ensure the formation of Ca4Al2Fe2O10 unless subsequent thermal treatments are applied. It was suggested that the occurrence of combustion reactions cannot be regarded only in terms of adiabatic temperature, as the kinetic aspects overrule the thermodynamic ones.


RSC Advances ◽  
2014 ◽  
Vol 4 (100) ◽  
pp. 56784-56790 ◽  
Author(s):  
G. P. Nagabhushana ◽  
D. Samrat ◽  
G. T. Chandrappa

Nanoparticles of ultra-porous MoO3 were synthesized in a single step by a solution combustion reaction using molybdenum metal powder for the first time as a precursor.


CrystEngComm ◽  
2015 ◽  
Vol 17 (31) ◽  
pp. 5889-5894 ◽  
Author(s):  
Pengqi Chen ◽  
Mingli Qin ◽  
Dezhi Zhang ◽  
Zheng Chen ◽  
Baorui Jia ◽  
...  

One-dimensional W18O49 nanoneedles were fabricated by solution combustion synthesis and exhibited an excellent visible light-driven photocatalytic performance.


2008 ◽  
Author(s):  
Emilio Moran ◽  
Miguel ïngel. Alario-Franco ◽  
Marco L. Garcia-Guaderrama ◽  
Oscar Blanco

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