scholarly journals Hierarchical synthesis of iron oxide nanoparticles by polyol cum Calcination Method and determination of its optical and magnetic behavior

2020 ◽  
Vol 249 ◽  
pp. 122950
Author(s):  
Affia Saddique ◽  
Zahoor Ahmad ◽  
Clare Hoskins ◽  
Muhammad Aslam Mirza ◽  
Asima Naz ◽  
...  
2010 ◽  
Vol 644 ◽  
pp. 51-55 ◽  
Author(s):  
Juan Fco Luna Martínez ◽  
E. Reyes-Melo ◽  
Virgilio González-González ◽  
A. Torres-Castro ◽  
Carlos Guerrero-Salazar ◽  
...  

In this work, iron oxide nanoparticles (~5 nm) embedded in a chitosan polymer film, were synthesized. In order to obtain this nanostructured material, firstly a homogenous film of Fe(II)-chitosan was prepared. The resulting composite film has a thickness of ~140μm. Iron oxide nanoparticles were in-situ synthesized by treating the composite film with H2O2 under alkaline conditions. The morphological analysis by Transmission Electron Microscopy (TEM) shows the nanoparticles were embedded and stabilized in chitosan polymer film. The magnetic behavior was studied by magnetization measurements. The magnetization curves at room temperature showed that iron oxide nanoparticles have a superparamagnetic behavior.


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