Effect of annealing temperature on structural, morphological and optical properties of nanocrystalline TiO2 thin films synthesized by sol–gel dip coating method

2020 ◽  
Vol 23 ◽  
pp. 68-72
Author(s):  
Kutraleeswaran Manickam ◽  
Venkatachalam Muthusamy ◽  
Saroja Manickam ◽  
T.S. Senthil ◽  
Gowthaman Periyasamy ◽  
...  
Keyword(s):  
Thin Films ◽  
Optical Properties ◽  
Annealing Temperature ◽  
Sol Gel ◽  
Dip Coating ◽  
Tio2 Thin Films ◽  
Nanocrystalline Tio2 ◽  
Coating Method ◽  
Dip Coating Method

Effect of annealing temperature on nanocrystalline TiO2 thin films prepared by sol–gel dip coating method

Optik ◽  
2013 ◽  
Vol 124 (23) ◽  
pp. 6201-6204 ◽  
Author(s):  
A. Ranjitha ◽  
N. Muthukumarasamy ◽  
M. Thambidurai ◽  
R. Balasundaraprabhu ◽  
S. Agilan
Keyword(s):  
Thin Films ◽  
Annealing Temperature ◽  
Sol Gel ◽  
Dip Coating ◽  
Tio2 Thin Films ◽  
Nanocrystalline Tio2 ◽  
Coating Method ◽  
Dip Coating Method

scholarly journals Characteristics and optical properties of Fe3+ doped SiO2/TiO2 thin films prepared by the sol-gel dip-coating method

2013 ◽  
Vol 16 (1) ◽  
pp. 92-100
Author(s):  
Chien Mau Dang ◽  
Dam Duy Le ◽  
Tam Thi Thanh Nguyen ◽  
Dung Thi My Dang
Keyword(s):  
Thin Films ◽  
Optical Properties ◽  
Sol Gel ◽  
Dip Coating ◽  
X Ray Diffraction ◽  
Tio2 Thin Films ◽  
Water Contact ◽  
Glass Substrates ◽  
Coating Method ◽  
Dip Coating Method

In this study, we have successfully synthesized Fe3+ doped SiO2/TiO2 thin films on glass substrates using the sol-gel dip-coating method. After synthesizing, the samples were annealed at 5000C in the air for 1 hour. The characteristics and optical properties of Fe3+ doped SiO2/TiO2 films were then investigated by X-ray diffraction (XRD), ultraviolet-visible spectroscopy (UV-vis) and Fourier transform infrared spectroscopy (FT-IR). An antifogging ability of the glass substrates coated with the fabricated film is investigated and explained by a water contact angle under visible-light. The analyzed results also show that the crystalline phase of TiO2 thin films comprised only the anatase TiO2, but the crystalline size decreased from 8.8 to 5.9 nm. We also observed that the absorption edge of Fe3+- doped SiO2/TiO2 thin films shifted towards longer wavelengths (i.e. red shifted) from 371.7nm to 409.2 nm when the Fe3+-doped concentration increased from 0 to 1 % mol.

Investigation on the Structural and Optical Properties of Nanocrystalline TiO2 Thin Films

2013 ◽  
Vol 678 ◽  
pp. 103-107 ◽  
Author(s):  
Arumugam Ranjitha ◽  
Natarajan Muthukumarasamy ◽  
Santhanam Agilan ◽  
Mariyappan Thambidurai ◽  
Rangasamy Balasundraprabhu ◽  
...  
Keyword(s):  
Thin Films ◽  
Sol Gel ◽  
Dip Coating ◽  
Band Gap Energy ◽  
Tio2 Thin Films ◽  
Nanocrystalline Tio2 ◽  
Structural Investigations ◽  
Force Microscopy ◽  
Coating Method ◽  
Dip Coating Method

Nanocrystalline TiO2 thin films were prepared by sol-gel dip coating method. The structural investigations were carried out using x-ray diffraction technique. Anatase TiO2 thin films with tetragonal phase were obtained and the grain size was observed to lie in the range of 21-25 nm. Analysis on the surface topography of prepared films have been carried out using atomic force microscopy (AFM). The band gap energy is calculated from the absorption spectra of TiO2 films and is found to lie in the range 3.3 to 3.7 eV.

Comparative study of multilayered ZnO/TiO2/ZnO and TiO2/ZnO/TiO2 thin films prepared by sol–gel dip coating method

2017 ◽  
Vol 28 (23) ◽  
pp. 17499-17504 ◽  
Author(s):  
M. I. Khan ◽  
Muhammad Saleem ◽  
K. A. Bhatti ◽  
Rabia Qindeel ◽  
Hayat Saeed Althobaiti ◽  
...  
Keyword(s):  
Thin Films ◽  
Comparative Study ◽  
Sol Gel ◽  
Dip Coating ◽  
Tio2 Thin Films ◽  
Coating Method ◽  
Dip Coating Method

Synthesis and Characterization of Nanocrystalline TiO2 Thin Films by Sol-Gel Dip Coating Method

2013 ◽  
Vol 678 ◽  
pp. 108-112 ◽  
Author(s):  
Narayanaswamy Gokilamani ◽  
N. Muthukumarasamy ◽  
Mariyappan Thambidurai
Keyword(s):  
Thin Films ◽  
Sol Gel ◽  
Dip Coating ◽  
X Ray Diffraction ◽  
Tio2 Thin Films ◽  
Atomic Force ◽  
Coating Method ◽  
Nanocrystalline Titanium ◽  
Dip Coating Method

Nanocrystalline titanium dioxide (TiO2) thin films have been prepared by dip coating method. The TiO2 thin films have been coated on glass substrate and annealed at 400, 450 and 500° C respectively. The X- ray diffraction pattern shows that TiO2 nanocrystalline thin films are of anatase structure and the grain size is found to be in the range of 20-35 nm. The annealed films have been observed to be nanocrystalline in nature and the crystallinity has been observed to improve on annealing. The surface topography of the films has been studied using atomic force microscope. The optical properties have been studied using transmittance spectra. The band gap has been found to lie in the range of 3.70 to 3.83 eV depending on the annealing temperature.

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