Ionic liquids-based microwave-assisted extraction of active components from pigeon pea leaves for quantitative analysis

2013 ◽  
Vol 102 ◽  
pp. 75-81 ◽  
Author(s):  
Zuofu Wei ◽  
Yuangang Zu ◽  
Yujie Fu ◽  
Wei Wang ◽  
Meng Luo ◽  
...  
Molecules ◽  
2019 ◽  
Vol 24 (15) ◽  
pp. 2770 ◽  
Author(s):  
Yunchang Fan ◽  
Zeyu Niu ◽  
Chen Xu ◽  
Lei Yang ◽  
Tuojie Yang

Rheum palmatum L. (R. palmatum L.) is a traditional Chinese herb and food, in which rhein and emodin are the main bioactive components. The extraction of the two compounds from R. palmatum L. is, thus, of great importance. In this work, protic ionic liquids (PILs) were applied in the microwave-assisted extraction (MAE) of rhein and emodin from R. palmatum L., which avoids the toxicity of organic solvents. The results of the present study indicate that PILs possessing higher polarity exhibit higher extraction ability due to their stronger absorption ability for microwave irradiation. Compared with conventional solvents, such as methanol, trichloromethane, and deep eutectic solvents (DESs), the PIL, 1-butyl-3-himidazolium methanesulfonate ([BHim]MeSO3) reported herein is more efficient. The selected extraction conditions of liquid–solid ratio, microwave irradiation time, microwave irradiation power, and PIL concentration were 40 g·g−1, 50 s, 280 W, and 80%, respectively. Under the selected conditions, the extraction yields of rhein and emodin were 7.8 and 4.0 mg·g−1, respectively. These results suggest that PILs are efficient extraction solvents for the separation of active components from natural products.


2020 ◽  
Vol 252 ◽  
pp. 117448 ◽  
Author(s):  
Renata Débora Pinto Rodrigues ◽  
Amanda Sousa e Silva ◽  
Thalita Adrielly Viana Carlos ◽  
Ana Karine Pessoa Bastos ◽  
Rílvia Saraiva de Santiago-Aguiar ◽  
...  

Talanta ◽  
2010 ◽  
Vol 80 (3) ◽  
pp. 1292-1297 ◽  
Author(s):  
Wenyan Ma ◽  
Yanbin Lu ◽  
Ruilin Hu ◽  
Jihang Chen ◽  
Zizhang Zhang ◽  
...  

2012 ◽  
Vol 716 ◽  
pp. 28-33 ◽  
Author(s):  
Zaixiang Lou ◽  
Hongxin Wang ◽  
Song Zhu ◽  
Shangwei Chen ◽  
Ming Zhang ◽  
...  

2007 ◽  
Vol 18 (4) ◽  
pp. 333-340 ◽  
Author(s):  
Fatemeh Nazari ◽  
Samad Nejad Ebrahimi ◽  
Mohammad Talebi ◽  
Ali Rassouli ◽  
Hamid Reza Bijanzadeh

2012 ◽  
Vol 13 (4) ◽  
pp. 5163-5178 ◽  
Author(s):  
Lei Yang ◽  
Xiaowei Sun ◽  
Fengjian Yang ◽  
Chunjian Zhao ◽  
Lin Zhang ◽  
...  

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