Acetone detection properties of single crystalline tungsten oxide plates synthesized by hydrothermal method using cetyltrimethyl ammonium bromide supermolecular template

2012 ◽  
Vol 162 (1) ◽  
pp. 259-268 ◽  
Author(s):  
Shuyang Liu ◽  
Fei Zhang ◽  
He Li ◽  
Ting Chen ◽  
Yude Wang
2014 ◽  
Vol 722 ◽  
pp. 42-45
Author(s):  
Yun Fei Zhuang ◽  
Ya Lan Bian

Using titanium trichloride (TiCl3) as the precursor, sodium chloride (NaCl) as the mineralizer, cetyltrimethyl ammonium bromide (CTAB) as surfactant, titanium oxides (TiO2) nanomicrospheres were synthesized by hydrothermal method. X-ray diffraction (XRD) and scanning electron microscopy (SEM) were employed to characterize the crystal structure and morphology of the microspheres. The results indicate that the spheres were rutile with diameters of about 1μm ~5μm. The spheres were composed of radially aligned nanorods with diameters of about 40nm and lengths of 500nm. The influences of the concentration of surfactant and the concentration of mineralizer were also researched. The microsphere diameter and grain size both reduce with the increase of the concentration of CTAB. The microspheres get larger and more complete with the higher mineralizer concentration.


2016 ◽  
Vol 30 (32n33) ◽  
pp. 1650400 ◽  
Author(s):  
Yuanyuan Han ◽  
Dan Wang ◽  
Danyang Liang ◽  
Shiqi Wang ◽  
Guoxin Lu ◽  
...  

Scheelite (CaWO4)-type microphosphors were synthesized by the precipitation method assisted with cetyltrimethyl ammonium bromide (CTAB). All compounds crystallized in the tetragonal structure with space group [Formula: see text] (No. 88). FE-SEM micrographs illustrate the spherical-like morphologies and rough surface. PL spectra indicate the broad emission peak maximum at 613 nm under UV excitation. Luminescence decay curves monitored by [Formula: see text] transition ([Formula: see text] nm) of Eu[Formula: see text] in doped CaWO4 are presented, the curves exhibit a single-exponential feature and the lifetime for doped CaWO4 is 0.61 ms.


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