A sequential injection method for the determination of piroxicam in pharmaceutical formulations using europium sensitized fluorescence

Talanta ◽  
2004 ◽  
Vol 64 (5) ◽  
pp. 1343-1350 ◽  
Author(s):  
S ALKINDY
2018 ◽  
Vol 33 (2) ◽  
pp. 47
Author(s):  
Orlando Fatibello-Filho ◽  
Heberth Juliano Vieira

A spectrophotometric flow injection method for the determination of paracetamol in pharmaceutical formulations is proposed. The procedure was based on the oxidation of paracetamol by sodium hypochloride and the determination of the excess of this oxidant using o-tolidine dichloride as chromogenic reagent at 430 nm. The analytical curve was linear in the paracetamol concentration range from 8.50 x 10-6 to 2.51 x 10-4 mol L-1 with a detection limit of 5.0 x 10-6 mol L-1. The relative standard deviation was smaller than 1.2% for 1.20 x 10-4 mol L-1 paracetamol solution (n = 10). The results obtained for paracetamol in pharmaceutical formulations using the proposed flow injection method and those obtained using a USP Pharmacopoeia method are in agreement at the 95% confidence level.


2008 ◽  
Vol 29 (4) ◽  
pp. 348-355 ◽  
Author(s):  
Raluca-Ioana Stefan-van Staden ◽  
Jacobus Frederick van Staden ◽  
Hassan Y. Aboul-Enein ◽  
Marius Constantin Mirica ◽  
Ionel Balcu ◽  
...  

2008 ◽  
Vol 24 (12) ◽  
pp. 1599-1603 ◽  
Author(s):  
Sarawut SOMNAM ◽  
Jaroon JAKMUNEE ◽  
Kate GRUDPAN ◽  
Narong LENGHOR ◽  
Shoji MOTOMIZU

2013 ◽  
Vol 85 (22) ◽  
pp. 11026-11033 ◽  
Author(s):  
Jixin Qiao ◽  
Xiaolin Hou ◽  
Peter Steier ◽  
Robin Golser

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