Evaluation of the adsorption properties of nucleobase-modified sorbents for a solid-phase extraction of water-soluble compounds

Talanta ◽  
2020 ◽  
Vol 217 ◽  
pp. 121052 ◽  
Author(s):  
Hiroya Murakami ◽  
Miho Omiya ◽  
Yuta Miki ◽  
Tomonari Umemura ◽  
Yukihiro Esaka ◽  
...  
Keyword(s):  
Solid Phase Extraction ◽  
Solid Phase ◽  
Adsorption Properties ◽  
Water Soluble ◽  
Phase Extraction ◽  
Modified Sorbents

Commercially available color-catching sheets for magnetic textile solid phase extraction of water-soluble dyes

Measurement ◽  
2021 ◽  
Vol 172 ◽  
pp. 108877
Author(s):  
Ivo Safarik ◽  
Jitka Prochazkova ◽  
Eva Baldikova ◽  
Kristyna Pospiskova
Keyword(s):  
Solid Phase Extraction ◽  
Solid Phase ◽  
Water Soluble ◽  
Phase Extraction

A Simple and Sensitive Dispersive Micro-Solid-Phase Extraction Coupled with High-Performance Liquid Chromatography for Quantification of Honokiol and Magnolol in Complex Matrices

2020 ◽  
Vol 103 (5) ◽  
pp. 1406-1411
Author(s):  
Chu Chu ◽  
Jing Li ◽  
Shan Wang ◽  
Lvnan Weng ◽  
Luyi Jiang ◽  
...  
Keyword(s):  
High Performance Liquid Chromatography ◽  
Liquid Chromatography ◽  
Solid Phase Extraction ◽  
High Performance ◽  
Solid Phase ◽  
Water Soluble ◽  
Phase Extraction ◽  
Patent Medicines ◽  
Chinese Patent

Abstract Background Honokiol and magnolol were considered as markers for the analysis of Cortex Magnoliae Officinalis, its related Chinese Patent Medicines and their metabolites. However, the determination of these two analytes in a water-soluble sample is difficult and therefore requires a more efficient method. Objective To develop a sensitive method for the determination of honokiol and magnolol in a water-soluble sample for better quality control of Cortex Magnoliae Officinalis and its related Chinese Patent Medicines. Method In this work, a combination of dispersive micro-solid-phase extraction (DMSPE) and high-performance liquid chromatography (HPLC) has been developed for simultaneous preconcentration and determination of honokiol and magnolol in complex bio-samples. Several experimental factors affecting the extraction efficiency were optimized by single factor test. Results Under the optimized extraction conditions, the proposed method exhibited good linearity of not less than 0.9998, satisfactory precision with relative standard deviation of less than 1.3%, and acceptable mean recoveries of 97.3% and 101.5% for honokiol and magnolol, respectively. Furthermore, the method exhibits extremely high sensitivity with detection limits of 0.0097 and 0.0231 ng/mL, which is even more sensitive than those methods developed by MS. Conclusions The method established in this study is fast, economic, accurate, easy to operate, and importantly well suited to the extraction and analysis of honokiol and magnolol in a real complex sample matrix.

scholarly journals Effectiveness of Liquid-Liquid Extraction, Solid Phase Extraction, and Headspace Technique for Determination of Some Volatile Water-Soluble Compounds of Rose Aromatic Water

2017 ◽  
Vol 2017 ◽  
pp. 1-7 ◽  
Author(s):  
Hale Seçilmiş Canbay
Keyword(s):  
Solid Phase Extraction ◽  
Solid Phase ◽  
Extraction Methods ◽  
Liquid Extraction ◽  
Water Soluble ◽  
Gas Chromatography Mass Spectrometry ◽  
Phase Extraction ◽  
Liquid Liquid Extraction ◽  
Cosmetic Industry

Steam distillation is used to isolate scent of rose flowers. Rose aromatic water is commonly used in European cuisine and aromatherapy besides its use in cosmetic industry for its lovely scent. In this study, three different sampling techniques, liquid-liquid extraction (LLE), headspace technique (HS), and solid phase extraction (SPE), were compared for the analysis of volatile water-soluble compounds in commercial rose aromatic water. Some volatile water-soluble compounds of rose aromatic water were also analyzed by gas chromatography mass spectrometry (GCMS). In any case, it was concluded that one of the solid phase extraction methods led to higher recoveries for 2-phenylethyl alcohol (PEA) in the rose aromatic water than the liquid-liquid extraction and headspace technique. Liquid-liquid extraction method provided higher recovery ratios for citronellol, nerol, and geraniol than others. Ideal linear correlation coefficient values were observed by GCMS for quantitative analysis of volatile compounds (r2≥0.999). Optimized methods showed acceptable repeatability (RSDs < 5%) and excellent recovery (>95%). For compounds such as α-pinene, linalool, β-caryophyllene, α-humulene, methyl eugenol, and eugenol, the best recovery values were obtained with LLE and SPE.

Simultaneous Preconcentration and Determination of Brilliant Blue and Sunset Yellow in Foodstuffs by Solid-Phase Extraction Combined UV-Vis Spectrophotometry

2018 ◽  
Vol 101 (6) ◽  
pp. 1850-1856 ◽  
Author(s):  
Abdullah Taner Bişgin
Keyword(s):  
Solid Phase Extraction ◽  
Flow Rate ◽  
Solid Phase ◽  
Ethanol Solution ◽  
Water Soluble ◽  
Brilliant Blue ◽  
Phase Extraction ◽  
Sunset Yellow ◽  
Food Dyes

Abstract Background: Brilliant Blue and Sunset Yellow, two highly water-soluble synthetic food dyes, are the most popular food dyes used and consumed. Although they are not highly toxic, some health problems can be observed when excessive amounts of food products containing these dyes are consumed. Objectives: The aim of the study was to develop a simultaneous UV-Vis combined solid-phase extraction method, based on the adsorption onto Amberlite XAD-8 resin, for determination of Brilliant Blue and Sunset Yellow dyes. Methods: Sample solution was poured into the reservoir of the column and permitted to gravitationally pass through the column at 2 mL/min flow rate. Adsorbed dyes were eluted to 5 mL of final volume with 1 mol/L HNO3 in ethanol solution by applying a 2 mL/min flow rate. Dye concentrations of the solution were determined at 483 and 630 nm for Sunset Yellow and Brilliant Blue, respectively. Results: The detection limits of the method for Brilliant Blue and Sunset Yellow were determined as 0.13 and 0.66 ng/mL, respectively. Preconcentration factor was 80. Brilliant Blue contents of real food samples were found to be between 11 and 240 μg/g. Sunset Yellow concentrations of foodstuffs were determined to be between 19 and 331 μg/g. Conclusions: Economical, effective, and simple simultaneous determination of Brilliant Blue and Sunset Yellow was achieved by using a solid-phase extraction combined UV-Vis spectrometry method. Highlights: The method is applicable and suitable for routine analysis in quality control laboratories without the need for expert personnel and high operational costs because the instrumentation is simple and inexpensive.

Effects of pendant-like hydrophilic monomers on the adsorption properties of reversed-phase-type sorbents for solid-phase extraction

2019 ◽  
Vol 1075 ◽  
pp. 106-111 ◽  
Author(s):  
Hiroya Murakami ◽  
Hiroki Tomita ◽  
Takuya Aoyanagi ◽  
Takashi Sugita ◽  
Yuta Miki ◽  
...  
Keyword(s):  
Solid Phase Extraction ◽  
Solid Phase ◽  
Reversed Phase ◽  
Adsorption Properties ◽  
Phase Extraction ◽  
Phase Type ◽  
Hydrophilic Monomers

Dispersion solid-phase extraction of flavonoid with amphiphilic monomersN-vinyl pyrrolidone and 1H,1H,7H-dodecafluoroheptyl methacrylate based poly(styrene-divinylbenzene) and silica

2018 ◽  
Vol 10 (38) ◽  
pp. 4680-4688 ◽  
Author(s):  
Yuxin Ma ◽  
Dandan Han ◽  
Yingjie Lei ◽  
Tao Zhu
Keyword(s):  
Solid Phase Extraction ◽  
Solid Phase ◽  
Silica Matrix ◽  
Adsorption Properties ◽  
Vinyl Pyrrolidone ◽  
Phase Extraction ◽  
Novel Materials ◽  
Styrene Divinylbenzene

Novel materials have been synthesized based on a S-DVB or silica matrix functionalized with NVP or NVP–DMFA and their adsorption properties were studied.

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