Preparation of nanocomposite thin films by sol-gel and photochemical metal–organic deposition of Ba0.5Sr0.5TiO3 and PbZr0.48Ti0.52O3

1999 ◽  
Vol 2 (4) ◽  
pp. 297-301 ◽  
Author(s):  
Youmao Shi ◽  
Guizhi Li ◽  
Ross H Hill
2006 ◽  
Vol 928 ◽  
Author(s):  
Christoph Peters ◽  
Matthias Bockmeyer ◽  
Reinhard Krüger ◽  
André Weber ◽  
Ellen Ivers-Tiffée

ABSTRACTVia metal organic deposition (MOD) sapphire substrates were multiple dip-coated with a molecular dispersive 8 mol% Y2O3 doped ZrO2 (8YSZ) sol to prepare dense, crack-free thin films. The thin films were consecutively exposed to a tempering program with several rapid thermal annealing (RTA) steps and a final dwell temperature between 500 °C and 1400 °C for 24 h. Grain growth, phase, stoichiometry and macroscopic density of the thin films were analyzed by XRD and SEM. Grain sizes ranged between a few nanometers in diameter at 500 °C and several hundreds of nanometers at 1400 °C.


2015 ◽  
Vol 04 (01) ◽  
pp. 1-8
Author(s):  
Kais Daoudi ◽  
Zied Othmen ◽  
Saoussen El Helali ◽  
Meherzi Oueslati ◽  
Tetsuo Tsuchiya

2017 ◽  
Vol 9 (11) ◽  
pp. e447-e447 ◽  
Author(s):  
Masashi Miura ◽  
Boris Maiorov ◽  
Michio Sato ◽  
Motoki Kanai ◽  
Takeharu Kato ◽  
...  

2008 ◽  
Vol 516 (7) ◽  
pp. 1499-1502 ◽  
Author(s):  
V. Musat ◽  
E. Fortunato ◽  
A.M. Botelho do Rego ◽  
R. Monteiro

2014 ◽  
Vol 564 ◽  
pp. 170-178 ◽  
Author(s):  
S. Kermadi ◽  
N. Agoudjil ◽  
S. Sali ◽  
M. Boumaour ◽  
S. Bourgeois ◽  
...  

1990 ◽  
Vol 200 ◽  
Author(s):  
Cheng-Chen Hsueh ◽  
Martha L. MeCartney

ABSTRACTFerroelectric PZT thin films were prepared by sol-gel methods and RF magnetron sputtering. Sputtered PZT fast fired at 650° for 30 minutes showed microporosity. For the sol-gel route, solution precursors had a significant effect on the microstructure of the crystalline PZT films. PZT thin films derived from metal-organic precursors dissolved in n-propanol were observed to have large and microporous spherulitic grains on the order of 2 μm and phase separation in acetic acid-catalyzed films. In contrast, PZT precursors originated from alcohol exchanges with 2-methoxyethanols resulted in dense films with fine grains of ∼0.2 μm and clear evidence of ferroelectric domains. The dense sol-gel films possessed superior dielectric and ferroelectric properties.


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