In Situ EBSD Study on the Microstructural Transformation of the Ni5W Substrate for Coated Conductors

2021 ◽  
Vol 27 (1) ◽  
pp. 36-43
Author(s):  
Xinyu Wu ◽  
Hongli Suo ◽  
Jiazhi Li ◽  
Yaotang Ji ◽  
Lin Ma ◽  
...  

Abstract

2020 ◽  
Vol 26 (3) ◽  
pp. 365-372
Author(s):  
Yaotang Ji ◽  
Hongli Suo ◽  
ZiLi Zhang ◽  
Lin Ma ◽  
Jiazhi Li ◽  
...  

AbstractAdvanced Ni8W/Ni12W/Ni8W alloy composite substrates used in YBCO-coated conductors with a strong cube texture and high yield strength have been fabricated, and a CeO2 buffer layer film was successfully deposited on the composite substrates. Through in situ tensile testing coupled with electron backscattered diffraction (EBSD) analysis, the stability of the cube texture of Ni8W/Ni12W/Ni8W alloy composite substrates has been investigated. The stress–strain curve shows that the yield strength (at 0.2% strain) of the composite substrates exceeds 250 Mpa. The orientation of grains and boundaries on the surface of the substrates was almost unchanged, while the strain exceeds 0.2%, which indicated that the composite substrates are adequate for depositing buffer layers and YBCO layers by the reel-to-reel process.


2008 ◽  
Vol 468 (24) ◽  
pp. 2351-2355 ◽  
Author(s):  
Ľ. Kopera ◽  
V. Šmatko ◽  
W. Prusseit ◽  
M. Polák ◽  
R. Semerad ◽  
...  

2003 ◽  
Vol 17 (04n06) ◽  
pp. 468-476 ◽  
Author(s):  
M. BINDI ◽  
L. GIANNI ◽  
S. ZANNELLA ◽  
A. BOTARELLI ◽  
A. BALDINI ◽  
...  

We report on the in-situ preparation and characterization of coated conductors consisting of a ≈ 400 nm thick YBCO superconducting film grown by thermal co-evaporation on a ≈ 200 nm thick CeO2 buffer layer grown by e-beam evaporation on biaxially textured Ni-Cr and Ni-V substrates. We studied the degree of texture of both YBCO and CeO2 layers as a function of substrate temperature during deposition and of oxygen partial pressure. X-ray diffraction patterns reveal that the highest degree of (100) texture of the buffer layer, necessary for the subsequent growth of the YBCO film with the desired c-axis orientation, is achieved at substrate temperatures of the order of 670-730°C. The backfilling of the chamber with oxygen during the cooling-down of the substrates after deposition of the CeO2 layer greatly improves the degree of crystallization of the buffer layer. YBCO films show good superconducting properties with critical temperatures Tc of the order of 87 K. Work is in progress to scale up the process for long tapes.


2000 ◽  
Vol 659 ◽  
Author(s):  
Teresa Puig ◽  
Anna Puig-Molina ◽  
Narcís Mestres ◽  
Harm Van Seijen ◽  
Francesc Alsina ◽  
...  

ABSTRACTTwo novel complementary and non-destructive techniques for texture analysis of YBCO coated conductors are presented. Micro-Raman (μ-Raman) spectroscopy enables an easy analysis of the film homogeneity by determining the distribution of a- and c-oriented grains within the tape with a 1 μm spatial resolution and acquisition times of 5 min/spot. In addition, synchrotron x-ray diffraction analysis in transmission geometry and 2D detectors enables, with acquisition times of 100 ms, simultaneous observation of a- and c- crystallites and in-plane textures of substrates, buffers and superconducting layer. Thus, opening the field of this technique to in-situ analysis of epitaxial growth of coated conductors prepared by ex-situ processes. Results from these two techniques for stainless steel tapes buffered with IBAD-YSZ and coated with PLD-YBCO are analyzed.


2021 ◽  
Vol 538 ◽  
pp. 148028
Author(s):  
Z.F. Wu ◽  
Y.X. Liang ◽  
J.L. Du ◽  
Y. Yan ◽  
X.F. Zhang ◽  
...  

2006 ◽  
Vol 47 ◽  
pp. 17-24 ◽  
Author(s):  
E. Gilioli ◽  
Andrea Gauzzi ◽  
Massimiliano Bindi ◽  
S. Rampino ◽  
F. Pattini ◽  
...  

We report on recent progress towards the continuous deposition of YBCO Coated Conductors (CC) by thermal co-evaporation. This is an attractive vacuum technique thanks to the simplicity, low cost and intrinsic uniformity over large areas. Recently, we published the in situ preparation route of 1 μm thick superconducting YBCO films deposited onto CeO2 buffered Ni biaxially textured tapes using a reel-to-reel system; end-to-end critical current densities Jc's at 77 K and self-field, measured by transport measurements are in the 1-2 MA/cm2 range for 1 m. long samples, with zero-resistance Tc= 87 K and transition widths DTc<3 K. In spite of the very good CC’s performances reported by a number of laboratories all over the world, several steps must be optimized in order to limit the CC production costs, in particular concerning the complexity of the CC architecture and the choice and optimization of the YBCO deposition technique. We specifically address the following critical points regarding: 1) the in situ oxidation of the YBCO layer using a novel supersonic nozzle, 2) the deposition by thermal or e-beam evaporation of thick crack-free CeO2 buffer layers and 3) the scaling-up of the deposition process using a new multichamber system.


Author(s):  
William Richard Iliffe ◽  
Nianhua Peng ◽  
Greg D Brittles ◽  
Rod Bateman ◽  
Roger P Webb ◽  
...  

1984 ◽  
Vol 75 ◽  
pp. 743-759 ◽  
Author(s):  
Kerry T. Nock

ABSTRACTA mission to rendezvous with the rings of Saturn is studied with regard to science rationale and instrumentation and engineering feasibility and design. Future detailedin situexploration of the rings of Saturn will require spacecraft systems with enormous propulsive capability. NASA is currently studying the critical technologies for just such a system, called Nuclear Electric Propulsion (NEP). Electric propulsion is the only technology which can effectively provide the required total impulse for this demanding mission. Furthermore, the power source must be nuclear because the solar energy reaching Saturn is only 1% of that at the Earth. An important aspect of this mission is the ability of the low thrust propulsion system to continuously boost the spacecraft above the ring plane as it spirals in toward Saturn, thus enabling scientific measurements of ring particles from only a few kilometers.


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