Effect of Slab Reheating Temperature on Cold Rolling Texture Evolution of Nb-Containing Grain-Oriented Silicon Steel

Texture control of grain-oriented silicon steel is the key factor to ensure the magnetic properties of the finished product. Nb-containing grain-oriented silicon steel with different slab reheating temperatures was hot rolled followed by single-stage or two-stage cold rolling, and the textures were also analyzed. In the single-stage cold rolling process, as the slab reheating temperature is reduced, the intensity of the rotating cube texture {100}<011> and Goss texture {011}<100> drops, and that of the {111}<112> texture increases. In the two-stage cold rolling process, with the decrease in the slab reheating temperature, the intensity of the {111}<112> texture increases from 4.958 to 6.809. At the same slab reheating temperature, the intensity of the rotating cube texture declines more significantly in the two-stage cold rolling process. Finally, two-stage cold rolling with the slab reheating temperature of 1220 °C is found to be more beneficial for the formation of a sharp Goss texture during the second recrystallization. The magnetic induction intensity B800 of the final product is 1.87T, and the iron loss P1.7/50 is 1.36 W/kg.

Study on the anodic oxidation performance of a rolled AA5252 aluminum alloy sheet with different thicknesses

Microstructures of AA5252 aluminum alloy sheets from surface to the center were observed by use of scanning electron microscope with electron backscatter detector assembly, and treated by anodic oxidation. Results showed that changes of the grain structures and textures of the AA5252 alloy sheets occur from the surface to the center layers. The anodic oxidation surface quality of the AA5252 aluminum alloy is closely related to the area ratio and distribution uniformity of Cube texture.

Study on the Formability and Texture evolution of AA6061 Alloy Processed by Repetitive Corrugation and Straightening.

The enhanced mechanical properties obtained by refining the grain size down to the ultrafine-grained (UFG) regime have attracted considerable attention in recent years. The severe plastic deformation (SPD) techniques allow obtaining ultrafine-grained materials. Different SPD techniques permit processing sheet shape materials such as repetitive corrugation and straightening (RCS) and accumulative roll bonding (ARB). In this study, the formability of an AA 6061-T6 processed by RCS was evaluated. The forming limit diagrams (FLD) were obtained by Nakazima tests of samples in initial condition (T6 state) and after one and two RCS cycles. The FLD curves showed that the forming capacity decreased from the first RCS cycle. Likewise, uniaxial tensile tests at different temperatures and strain rates were conducted to analyze the effect of the RCS process on the strain rate sensitivity. They showed a relatively high strain rate sensitivity coefficient in the samples after one and two RCS cycles, which indicates an improvement of i) the capacity of the material to delay the onset of the necking and ii) the formability at increasing temperatures. Finally, texture analysis was carried out employing X-ray diffraction, calculating the orientation distribution functions (ODFs). The initial texture showed a predominant cube texture component, whereas, for further RCS cycles, a weakening of the cube texture and an increment of the S texture component were observed.

Microstructural Evolutions of 2N Grade Pure Al and 4N Grade High-Purity Al during Friction Stir Welding

The grain refinement mechanisms along the material flow path in pure and high-purity Al were examined, using the marker insert and tool stop action methods, during the rapid cooling friction stir welding using liquid CO2. In pure Al subjected to a low welding temperature of 0.56Tm (Tm: melting point), the resultant microstructure consisted of a mixture of equiaxed and elongated grains, including the subgrains. Discontinuous dynamic recrystallization (DDRX), continuous dynamic recrystallization (CDRX), and geometric dynamic recrystallization are the potential mechanisms of grain refinement. Increasing the welding temperature and Al purity encouraged dynamic recovery, including dislocation annihilation and rearrangement into subgrains, leading to the acceleration of CDRX and inhibition of DDRX. Both C- and B/-type shear textures were developed in microstructures consisting of equiaxed and elongated grains. In addition, DDRX via high-angle boundary bulging resulted in the development of the 45° rotated cube texture. The B/ shear texture was strengthened for the fine microstructure, where equiaxed recrystallized grains were fully developed through CDRX. In these cases, the texture is closely related to grain structure development.

Effects of Oxide Inclusions on Texture of 1235 Al-Alloy after Deformation

Texture characteristics of compressed 1235 Al-alloy treated by different purification methods are studied by electron backscattered diffraction. The effects of oxide inclusions on texture components of material are studied as well. The main textures in hot-compressed 1235 Al-alloy are Cube texture, R texture, Gross texture, Brass texture, and Rotated cube texture. The lower the content of oxide inclusions in the material, the smaller the total relative ratio of textures. The total relative ratio of textures goes to the smallest by 1.8 % in high-efficient purified 1235 Al-alloy by oxide inclusion content of 0.051 %. The purification results have obvious effects on types and percentage of texture in the deformed alloy. With the decreasing content of oxide inclusion, the ratio of deformation texture decreases and recrystallization texture increases. Brass texture is gradually replaced by Goss texture in the deformation textures. R texture is the main texture in recrystallization textures. Therefore, reducing the content of oxide inclusions is effective for improving the hot deformation properties of 1235 Al-alloy.

Evolution of the Shear Band in Cold-Rolling of Strip-Cast Fe-1.3% Si Non-Oriented Silicon Steel

Cube texture and microstructural evolution of as-cast non-oriented silicon steel (1.3% Si) during cold rolling and annealing were studied. The results showed that the as-cast microstructure with grain size in the range of 100–500 μm had a weak texture. The strong orientation was mainly located at {100} and {110} planes. A significant content of shear-deformed grains oriented with {110}<110> were obtained by cold-rolling, and many regions oriented with Cube texture were distributed in the shear bands. During cold-rolling, the orientation of the shear-deformed microstructure tilted towards the {111}<112> orientation, while the matrix orientation retained {110}<110>. On further cold-rolling, the residual part of {110}<110> experienced shear deformation, forming more shear bands, strengthening the Cube orientation. During annealing, Cube orientation grains nucleated in the shear bands leading to strong Cube texture, and corresponding B50 was 1.83T/1.79T.

Shear Banding in Rotated Goss Grains and its Effect on the Formation of Cube Texture in Non-Oriented Electrical Steel

Cube texture ({001}<100>) is a desired final texture in non-oriented electrical steel sheets used as magnetic cores because it contains two easy <100> axes in the sheet plane, which is beneficial to the magnetic properties. However, the cube texture is very difficult to form in non-oriented electrical steels through conventional rolling and annealing. It has been shown that after conventional rolling, the deformed <111>//ND (normal direction) grains provided nucleation sites for the unfavourable <111>//ND texture during recrystallization, leading to a final <111>//ND texture. To eliminate the <111>//ND texture and promote the {001}<100> texture, an uncommon rolling process, i.e. inclined rolling, was adopted in this study. By rotating the hot rolling direction by 60° around the ND, an uncommon initial texture, the rotated Goss ({110}<110>), was intentionally generated. This was intended to change the orientation flow during plastic deformation, and suppress the formation of the conventional <111>//ND texture in the deformed microstructure. Plane-strain compression (rolling) of the rotated Goss grains produced shear bands within these grains due to their large Taylor factor. Electron backscatter diffraction (EBSD) characterization of the shear bands illustrated that, crystallites with the cube orientation were formed within these shear bands. During recrystallization, the shear bands provided preferential nucleation sites, and the cube crystallites preferentially nucleate within the shear bands. These cube crystals can then grow into the deformed matrix, and lead to the formation of a strong cube texture in the final annealed steel sheets.