Direct determination of polycyclic aromatic hydrocarbons in extracts of particulate matter

1987 ◽  
Vol 59 (7) ◽  
pp. 970-973 ◽  
Author(s):  
A. E. Elsaid ◽  
A. P. D'Silva ◽  
V. A. Fassel ◽  
R. L. M. Dobson
Keyword(s):  
Polycyclic Aromatic Hydrocarbons ◽  
Particulate Matter ◽  
Aromatic Hydrocarbons ◽  
Direct Determination ◽  
Polycyclic Aromatic

scholarly journals Development of Automated Column Chromatography System and Its Application to the Determination of Polycyclic Aromatic Hydrocarbons in Suspended Particulate Matter

2009 ◽  
Vol 58 (4) ◽  
pp. 287-292 ◽  
Author(s):  
Tomoaki Okuda ◽  
Toshiharu Kuroda ◽  
Tomio Nara ◽  
Kazuki Okamoto ◽  
Yumi Okabayashi ◽  
...  
Keyword(s):  
Polycyclic Aromatic Hydrocarbons ◽  
Particulate Matter ◽  
Suspended Particulate Matter ◽  
Column Chromatography ◽  
Aromatic Hydrocarbons ◽  
Suspended Particulate ◽  
Polycyclic Aromatic

scholarly journals Determination of Polycyclic Aromatic Hydrocarbons in Airborne Particulate Matter by Gas ChromatographyTriple Quadrupole Tandem Mass Spectrometry

2010 ◽  
Vol 93 (1) ◽  
pp. 284-294 ◽  
Author(s):  
Antonia Garrido Frenich ◽  
Rosa Martínez Ocaña ◽  
José L Martínez Vidal
Keyword(s):  
Polycyclic Aromatic Hydrocarbons ◽  
Particulate Matter ◽  
Aromatic Hydrocarbons ◽  
Treatment Time ◽  
Airborne Particulate Matter ◽  
Airborne Particulate ◽  
Srm 1649A ◽  
Polycyclic Aromatic ◽  
The City

Abstract An accurate and sensitive method for the identification and the quantification of 24 polycyclic aromatic hydrocarbons (PAHs) in airborne particulate matter has been developed and validated using GC/MS/MS with a triple quadrupole analyzer. Ultrasonic extraction (USE) and pressurized liquid extraction (PLE) were evaluated. PLE was selected because it provided better recoveries and reduced treatment time and use of solvents compared to USE. Cleanup of PLE extracts was not necessary. The accuracy of the optimized method was tested using a standard reference material of urban dust (SRM 1649a). PAH recoveries were between 70 and 99 (except for naphthalene, which was lower than 20) with RSDs ranging from 2.6 to 15.3. Linearity in the range 5500 ng/mL provided R2 values higher than 0.99 for all compounds. LODs for PAHs ranged from 0.001 to 0.435 ng/mL and LOQs ranged from 0.003 to 0.757 ng/mL. The proposed method was applied to the analysis of real samples collected in the city of Almera, Spain, where some PAHs were found at levels lower than the legislated limit.

Determination of polycyclic aromatic hydrocarbons (PAHs) in particulate matter collected with low volume samplers

Talanta ◽  
2007 ◽  
Vol 72 (4) ◽  
pp. 1357-1361 ◽  
Author(s):  
P BRUNO ◽  
M CASELLI ◽  
G DEGENNARO ◽  
M TUTINO
Keyword(s):  
Polycyclic Aromatic Hydrocarbons ◽  
Particulate Matter ◽  
Aromatic Hydrocarbons ◽  
Polycyclic Aromatic ◽  
Low Volume

Pre-concentration of water samples with BEA zeolite for the direct determination of polycyclic aromatic hydrocarbons with laser-excited time-resolved Shpol'skii spectroscopy

2013 ◽  
Vol 110 ◽  
pp. 246-255 ◽  
Author(s):  
Walter B. Wilson ◽  
Andréia A. Costa ◽  
Huiyong Wang ◽  
Andres D. Campiglia ◽  
José A. Dias ◽  
...  
Keyword(s):  
Polycyclic Aromatic Hydrocarbons ◽  
Aromatic Hydrocarbons ◽  
Water Samples ◽  
Direct Determination ◽  
Time Resolved ◽  
Bea Zeolite ◽  
Polycyclic Aromatic ◽  
Shpol'skii Spectroscopy

Direct Determination of Soil Surface-Bound Polycyclic Aromatic Hydrocarbons in Petroleum-Contaminated Soils by Real-Time Aerosol Mass Spectrometry

2000 ◽  
Vol 72 (20) ◽  
pp. 5040-5046 ◽  
Author(s):  
Ryan P. Rodgers ◽  
Alexandru C. Lazar ◽  
Peter T. A. Reilly ◽  
William B. Whitten ◽  
J. Michael Ramsey
Keyword(s):  
Mass Spectrometry ◽  
Polycyclic Aromatic Hydrocarbons ◽  
Aromatic Hydrocarbons ◽  
Contaminated Soils ◽  
Direct Determination ◽  
Soil Surface ◽  
Aerosol Mass ◽  
Aerosol Mass Spectrometry ◽  
Polycyclic Aromatic
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