Fluorescence polarization method for studying molecular orientation of mono- and multilayered polyimide films prepared by the Langmuir-Blodgett technique

1991 ◽  
Vol 24 (3) ◽  
pp. 659-665 ◽  
Author(s):  
Shinzaburo Ito ◽  
Koichi Kanno ◽  
Satoru Ohmori ◽  
Yoshihiko Onogi ◽  
Masahide Yamamoto
ChemInform ◽  
2010 ◽  
Vol 22 (7) ◽  
pp. no-no
Author(s):  
T. KAMATA ◽  
J. UMEMURA ◽  
T. TAKENAKA ◽  
K. TAKEHARA ◽  
K. ISOMURA ◽  
...  

1989 ◽  
Vol 28 (Part 1, No. 12) ◽  
pp. 2552-2555 ◽  
Author(s):  
Kazuo Iida ◽  
Tsukasa Nohara ◽  
Kazuyuki Totani ◽  
Shuhei Nakamura ◽  
Goro Sawa

2006 ◽  
Vol 69 (11) ◽  
pp. 2712-2719 ◽  
Author(s):  
VINCENZO LIPPOLIS ◽  
MICHELANGELO PASCALE ◽  
ANGELO VISCONTI

A fluorescence polarization immunoassay previously described for deoxynivalenol (DON) screening in wheat was optimized for the rapid quantification of DON in durum wheat kernels, semolina, and pasta. A background signal was observed in both spiked and naturally contaminated samples, strictly depending on the testing matrix. After subtracting the background DON level for durum wheat (0.27 μg of DON per g), semolina (0.08 μg of DON per g), and pasta (0.04 μg of DON per g), an accurate quantification of DON was possible at levels greater than 0.10 μg/g for all matrices. Average recoveries from spiked samples (0.25 to 1.75 μg/g) were 98, 102, and 101% for wheat, semolina, and pasta, respectively. Comparative analyses of 35 naturally contaminated durum wheat samples, 22 semolina samples, and 26 pasta samples performed by both the fluorescence polarization method and high-pressure liquid chromatography/immunoaffinity cleanup showed a good correlation (r > 0.995). The fluorescence polarization method showed better accuracy and precision with respect to the high-pressure liquid chromatography method and is suitable for the rapid and quantitative determination of DON in durum wheat–based products at levels foreseen by existing or coming international regulations.


1998 ◽  
Vol 102 (33) ◽  
pp. 6425-6432 ◽  
Author(s):  
Xiaoxi Chen ◽  
Christopher C. Moser ◽  
Denis L. Pilloud ◽  
P. Leslie Dutton

1995 ◽  
Vol 413 ◽  
Author(s):  
D. W. Cheong ◽  
J. -I Chen ◽  
J. Kumar ◽  
S. K. Tripathy

ABSTRACTNonlinear optical (NLO) LB films of polyamic acid containing a stable NLO dye were prepared and imidized either chemically or thermally. The optical properties and molecular orientation of these LB films were studied. From the absorption spectra, we infer that the derivative of the pnitroazobenzene chromophore covalently attatched to polyamic acid did not show significant aggregation. Quadratic dependence of SHG on the number of layers in polyamic acid films indicated the noncentrosymmetric organization of polar NLO chromophores. A second-order nonlinear coefficient (d33) of 23.4 pm/V was observed at 1064 nm after absorption correction. In polyimide films, SH intensity was dramatically reduced due to the collapse of the layered structure upon imidization process. In-plane isotropy of the LB films of polyamic acid and polyimide were lost upon irradiation of polarized light.


1978 ◽  
Vol 10 (5) ◽  
pp. 485-494 ◽  
Author(s):  
Akira Hayashi ◽  
Kyosuke Kinoshita ◽  
Masaru Kuwano ◽  
Atsumi Nose

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