scholarly journals Room-temperature deformation of single crystals of ZrB2 and TiB2 with the hexagonal AlB2 structure investigated by micropillar compression

2021 ◽  
Vol 11 (1) ◽  
Author(s):  
Zhenghao Chen ◽  
Bhaskar Paul ◽  
Sanjib Majumdar ◽  
Norihiko L. Okamoto ◽  
Kyosuke Kishida ◽  
...  
Keyword(s):  
Single Crystals ◽  
Plastic Flow ◽  
Room Temperature ◽  
Resolve Shear Stress ◽  
Temperature Deformation ◽  
Slip Systems ◽  
Compression Tests ◽  
Plastic Deformation Behavior ◽  
Bulk Single Crystals ◽  
Micropillar Compression

AbstractThe plastic deformation behavior of single crystals of two transition-metal diborides, ZrB2 and TiB2 with the AlB2 structure has been investigated at room temperature as a function of crystal orientation and specimen size by micropillar compression tests. Although plastic flow is not observed at all for their bulk single crystals at room temperature, plastic flow is successfully observed at room temperature by the operation of slip on {1$${\bar{1}}$$ 1 ¯ 00}<11$${\bar{2}}$$ 2 ¯ 3> in ZrB2 and by the operation of slip on {1$${\bar{1}}$$ 1 ¯ 00}<0001> and {1$${\bar{1}}$$ 1 ¯ 00}<11$${\bar{2}}$$ 2 ¯ 0> in TiB2. Critical resolve shear stress values at room temperature are very high, exceeding 1 GPa for all observed slip systems; 3.01 GPa for {1$${\bar{1}}$$ 1 ¯ 00}<11$${\bar{2}}$$ 2 ¯ 3> slip in ZrB2 and 1.72 GPa and 5.17 GPa, respectively for {1$${\bar{1}}$$ 1 ¯ 00}<0001> and {1$${\bar{1}}$$ 1 ¯ 00}<11$${\bar{2}}$$ 2 ¯ 0> slip in TiB2. The identified operative slip systems and their CRSS values are discussed in comparison with those identified in the corresponding bulk single crystals at high temperatures and those inferred from micro-hardness anisotropy in the early studies.

scholarly journals Room temperature deformation of single crystals of Ti5Si3 with the hexagonal D88 structure investigated by micropillar compression tests

2020 ◽  
Vol 10 (1) ◽  
Author(s):  
Kyosuke Kishida ◽  
Takayoshi Fukuyama ◽  
Takuto Maruyama ◽  
Haruyuki Inui
Keyword(s):  
Fracture Toughness ◽  
Transition Metal ◽  
Single Crystals ◽  
Room Temperature ◽  
Specimen Size ◽  
Temperature Deformation ◽  
Compression Tests ◽  
Axis Orientation ◽  
Plastic Deformation Behavior ◽  
Micropillar Compression

Abstract Micropillar compression tests of Ti5Si3 single crystals were conducted at room temperature as a function of loading axis orientation and specimen size in order to investigate their room temperature plastic deformation behavior. Plastic flow by the operation of three deformation modes, {1$${\overline{1}}$$ 1 ¯ 00}[0001], {2$${\overline{1}}$$ 1 ¯ $${\overline{1}}$$ 1 ¯ 2} < 2$${\overline{1}}$$ 1 ¯ $${\overline{1}}$$ 1 ¯ $${\overline{3}}$$ 3 ¯  > and {1$${\overline{1}}$$ 1 ¯ 01} < 2$${\overline{1}}$$ 1 ¯ $${\overline{1}}$$ 1 ¯ $${\overline{3}}$$ 3 ¯  > slip were observed in [2$${\overline{2}}$$ 2 ¯ 05]-, [0001]- and [4$${\overline{3}}$$ 3 ¯ $${\overline{1}}$$ 1 ¯ 0]-oriented micropillar specimens deformed at room temperature, respectively. The CRSS values were evaluated to be very high above 2.7 GPa and were confirmed to increase up to about 6 GPa with the decrease in the specimen size. The fracture toughness values are evaluated to be 0.45 MPa m1/2 (notch plane // (0001)) and 0.73 MPa m1/2 (notch plane //(1$${\overline{1}}$$ 1 ¯ 00)) based on the results of micro-cantilever bend tests of chevron-notched specimens. The fracture toughness values are considerably lower than those for D8l-Mo5SiB2 and D8l-Nb5Si3 evaluated by the same method, indicating the inherent brittleness of binary Ti5Si3 compared to the other transition-metal silicides of the TM5Si3 type (TM: transition-metal).

High Temperature Deformation of Single Crystalline Cr3Si (A15) Intermetallic Compound

1990 ◽  
Vol 213 ◽  
Author(s):  
C. Steve Chang ◽  
D. P. Pope
Keyword(s):  
High Temperature ◽  
Intermetallic Compound ◽  
Single Crystals ◽  
Intermetallic Compounds ◽  
High Temperature Deformation ◽  
Temperature Deformation ◽  
Slip Systems ◽  
Compression Tests ◽  
Single Crystalline ◽  
Slip Traces

AbstractHigh temperature compression tests were performed on Cr 3Si single crystalline and poly crystalline samples. Slip systems were determined to be of the {001}<010> type based on an analysis of slip traces and Laue spots. Single crystals show significant compressive ductility at temperatures above 0.7Tm. The implication of cube slip on the ductility of A15-type intermetallic compounds is discussed.

Soft and Hard Modes of Deformation in Mosi2 Single Crystals

1994 ◽  
Vol 364 ◽  
Author(s):  
K. Ito ◽  
T. Yano ◽  
H. Inui ◽  
M. Yamaguchi
Keyword(s):  
Single Crystals ◽  
Plastic Flow ◽  
Deformation Behavior ◽  
Crystal Orientation ◽  
Room Temperature ◽  
Intermediate Temperature ◽  
Slip Systems ◽  
Anomalous Increase ◽  
Temperature Range ◽  
Intermediate Temperature Range

AbstractThe deformation behavior of MoSi2 single crystals has been studied in the temperature range of -196<1500°C. While [001]-oriented crystals can be plastically deformed only above 1300°C, plastic flow is possible from temperatures as low as room temperature for single crystals with orientations other than [001]. Five slip systems, {110)<111], {011)<100], {010)<100], {023)<100] and {013)<331], are identified to be operative, depending on crystal orientation. An anomalous increase in CRSS is observed in the intermediate temperature range for the former three slip systems. Schmid’s law is generally valid for the soft modes, {110)<111], {011)<100] and {023)<100]. In contrast, the CRSS for the hard mode, {013)<331], strongly depends on crystal orientation with the higher values for orientations closer to [001].

Plastic Deformation of Mo(Si,Al)2 Single Crystals with the C40 Structure

1996 ◽  
Vol 460 ◽  
Author(s):  
M. Moriwaki ◽  
K. Ito ◽  
H. Inui ◽  
M. Yamaguchi
Keyword(s):  
Single Crystals ◽  
Deformation Behavior ◽  
Basal Slip ◽  
Room Temperature ◽  
Slip Systems ◽  
Temperature Range ◽  
Al Content ◽  
Partial Dislocations ◽  
Increasing Temperature ◽  
Critical Resolved Shear Stress

ABSTRACTThe deformation behavior of single crystals of Mo(Si,Al)2 with the C40 structure has been studied as a function of crystal orientation and Al content in the temperature range from room temperature to 1500°C in compression. Plastic flow is possible only above 1100°C for orientations where slip along <1120> on (0001) is operative and no other slip systems are observed over whole temperature range investigated. The critical resolved shear stress for basal slip decreases rapidly with increasing temperature and the Schmid law is valid. Basal slip appears to occur through a synchroshear mechanism, in which a-dislocations (b=1/3<1120>) dissociate into two synchro-partial dislocations with the identical Burgers vector(b*1/6<1120>) and each synchro-partial further dissociates into two partials on two adjacent planes.

Synthesis and Characterization of Mechanically Alloyed and HIP-Consolidated Fe-25Al-10Ti Intermetallic Alloy

2000 ◽  
Vol 646 ◽  
Author(s):  
Su-Ming Zhu ◽  
Makoto Tamura ◽  
Kazushi Sakamoto ◽  
Kunihiko Iwasaki
Keyword(s):  
Yield Strength ◽  
Tribological Properties ◽  
Room Temperature ◽  
Hot Isostatic Pressing ◽  
Microstructural Characterization ◽  
Intermetallic Alloy ◽  
High Temperature Deformation ◽  
Temperature Deformation ◽  
Positive Temperature ◽  
Compression Tests

ABSTRACTThe present study is concerned with the processing, microstructural characterization, mechanical and tribological properties of fine-grained Fe-25Al-10Ti intermetallic alloy. The alloy was synthesized from elemental powders by mechanical alloying in an attritor-type ball milling system for 100 h, followed by hot isostatic pressing (HIP). After HIP treatment at 1073 K under an ultra-high pressure of 980 MPa, fully dense compacts with a grain size of about 200 nm were produced. Mechanical properties were evaluated by compression tests from room temperature to 1073 K. At room temperature, the alloy exhibits yield strength as high as 2.4 GPa, together with considerable rupture strain of 0.16. The yield strength decreases monotonically with increasing test temperature with no positive temperature dependence observed. The grain growth after high temperature deformation is not severe, indicating that the alloy has a relatively high thermal stability. Finally, tribological properties of the alloy were evaluated by using a ball-on-disk type wear tester and compared with those for gray cast iron, a currently used material for automotive brake rotors.

Influence of Dislocation Mobility on Room and High Temperature Ductility of -Oriented Nial Single Crystals

1994 ◽  
Vol 364 ◽  
Author(s):  
M. A. Morris ◽  
J. P. Perez ◽  
R. Darolia
Keyword(s):  
High Temperature ◽  
Single Crystals ◽  
Room Temperature ◽  
Tensile Tests ◽  
Slip Systems ◽  
Dislocation Mobility ◽  
Screw Dislocations ◽  
Large Density ◽  
Thin Foils

AbstractThe dislocation configurations produced by room and high temperature compression of <100> oriented single crystals of binary NiAl and in those containing iron and hafnium additions have been analysed and compared to those obtained by hardness indentation and TEM insitu tensile tests. Kinking occurs during room temperature compression such that <100> dislocations are activated in all cases but the iron-containing alloy also exhibited a large density of <111> screw dislocations. The latter however, appear immobile when they are created by hardness indentations of thin foils, while only pile-ups of <100> segments can propagate. Similarly, although different slip systems are present after high temperature compression, only <100> dislocation segments have been confirmed to be mobile after room temperature hardness indentation of these predeformed thin foils. The improvement in ductility observed at room temperature in the predeformed specimens of the binary and the iron containing alloys has been attributed to the increased production of these mobile <100> dislocations.

Structure Characteristics of Cubic and Orthorhombic Phases of High Density Scintillator Pbf2 from 4.2–300 K

1994 ◽  
Vol 348 ◽  
Author(s):  
Ivan Shmyt'ko ◽  
I.B. Savchenko ◽  
N.V. Klassen ◽  
B.Sh. Bagautdinov ◽  
G.A. Emel'chenko ◽  
...  
Keyword(s):  
Phase Transition ◽  
Plastic Deformation ◽  
Temperature Dependence ◽  
Single Crystals ◽  
Room Temperature ◽  
Cell Parameter ◽  
Structure Characteristics ◽  
Pseudocubic Phase ◽  
Bulk Single Crystals ◽  
Structural Aspects

ABSTRACTAn anomaly of the temperature dependence of the unit cell parameter has been observed for β–PbF2 single crystals at 200 K that is interpreted as a phase transition to a pseudocubic lattice. Such a pseudocubic phase is observable at room temperature after uniaxial plastic deformation of the bulk single crystals. The structural aspects of the β→α transition have been established. The as-grown crystals of α–PbF2 phase are shown to undergo a phase transition at 100 K.

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