Shipboard flow injection method for the determination of manganese in sea-water using in-valve preconcentration and catalytic spectrophotometric detection

The Analyst ◽  
1991 ◽  
Vol 116 (7) ◽  
pp. 707 ◽  
Author(s):  
I. Ya. Kolotyrkina ◽  
L. K. Shpigun ◽  
Yury A. Zolotov ◽  
G. I. Tsysin
2011 ◽  
Vol 289 (1) ◽  
pp. 67-73 ◽  
Author(s):  
Jorge L. Guzmán-Mar ◽  
Aracely Hernández-Ramírez ◽  
Ulrico J. López-Chuken ◽  
Pedro L. López-de-Alba ◽  
Víctor Cerdà

1995 ◽  
Vol 309 (1-3) ◽  
pp. 259-270 ◽  
Author(s):  
Richard G.J. Bellerby ◽  
David R. Turner ◽  
Geoffrey E. Millward ◽  
Paul J. Worsfold

The Analyst ◽  
1996 ◽  
Vol 121 (8) ◽  
pp. 1037 ◽  
Author(s):  
Alexander Malahoff ◽  
Irina Ya. Kolotyrkina ◽  
Lilly K. Shpigun

1992 ◽  
Vol 266 (2) ◽  
pp. 345-351 ◽  
Author(s):  
Kenneth H. Coale ◽  
Kenneth S. Johnson ◽  
Paul M. Stout ◽  
Carole M. Sakamoto

2000 ◽  
Vol 49 (1) ◽  
pp. 59-64 ◽  
Author(s):  
Hiroki OHURA ◽  
Toshihiko IMATO ◽  
Ikuo MATSUO ◽  
Sumio YAMASAKI

2018 ◽  
Vol 33 (2) ◽  
pp. 47
Author(s):  
Orlando Fatibello-Filho ◽  
Heberth Juliano Vieira

A spectrophotometric flow injection method for the determination of paracetamol in pharmaceutical formulations is proposed. The procedure was based on the oxidation of paracetamol by sodium hypochloride and the determination of the excess of this oxidant using o-tolidine dichloride as chromogenic reagent at 430 nm. The analytical curve was linear in the paracetamol concentration range from 8.50 x 10-6 to 2.51 x 10-4 mol L-1 with a detection limit of 5.0 x 10-6 mol L-1. The relative standard deviation was smaller than 1.2% for 1.20 x 10-4 mol L-1 paracetamol solution (n = 10). The results obtained for paracetamol in pharmaceutical formulations using the proposed flow injection method and those obtained using a USP Pharmacopoeia method are in agreement at the 95% confidence level.


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