Comparison of solvent extraction and thermal desorption methods for determination of volatile polyfluorinated alkyl substances in the urban atmosphere

2013 ◽  
Vol 5 (13) ◽  
pp. 3410 ◽  
Author(s):  
Yaoxing Wu ◽  
Victor W.-C. Chang
1986 ◽  
Vol 58 (1) ◽  
pp. 258-261 ◽  
Author(s):  
Phillip T. Crisp ◽  
John. Ellis ◽  
Jan W. De Leeuw ◽  
Pieter A. Schenck

1992 ◽  
Vol 57 (8) ◽  
pp. 1632-1638 ◽  
Author(s):  
Věra Tatarkovičová ◽  
Zdeněk Stránský

The procedure for the determination of carbamate pesticides in soil was optimized. The following factors affecting the final results were investigated: extracting solvent, extraction procedure, extract purification procedure, and soil type. Triple extraction with acetone and purification of the extract on a two-stage purification column containing an activated carbon-silica gel 1+1 mixture were found optimal. The extracts after treatment were analyzed by RP-HPLC with UV detection. The method developed allows carbamate pesticides in soil to be determined at concentrations in excess of 30 μg kg-1.


Sign in / Sign up

Export Citation Format

Share Document