Simultaneous determination of eight vitamin E isomers and α-tocopherol acetate in functional foods and nutritional supplements by gas chromatography – mass spectrometry

2015 ◽  
Vol 7 (8) ◽  
pp. 3353-3362 ◽  
Author(s):  
Dan Lu ◽  
Yi Yang ◽  
Xin Wu ◽  
Li Zeng ◽  
Yongxin Li ◽  
...  

A gas chromatography-mass spectrometry (GC-MS) has been developed for the simultaneous determination of eight VE isomers and α-tocopherol acetate in functional foods.

1989 ◽  
Vol 72 (2) ◽  
pp. 349-354 ◽  
Author(s):  
Lee Q Huang

Abstract A multiresidue method was developed for the simultaneous determination of low parts per billion (ppb) concentrations of the herbicides alachlor, metolachlor, atrazine, and simazine in water and soil using isotope dilution gas chromatography/mass spectrometry (GC/MS). Known amounts of 15N,13C-alachlor and 2H5-atrazine were added to each sample as internal standards. The samples were then prepared by a solid phase extraction with no further cleanup. A high resolution GC/low resolution MS system with data acquisition in selected ion monitoring mode was used to quantitate herbicides in the extract. The limit of detection was 0.05 ppb for water and 0.5 ppb for soil. Accuracy greater than 80% and precision better than 4% was demonstrated with spiked samples.


2020 ◽  
Vol 75 (10) ◽  
pp. 1330-1334
Author(s):  
Dotse Selali Chormey ◽  
Buse Tuğba Zaman ◽  
Esra Maltepe ◽  
Çağdaş Büyükpınar ◽  
Ayşe Evrim Bulgurcuoğlu ◽  
...  

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