An Efficient synthesis of Weinreb amides and ketones via palladium nanoparticles on ZIF-8 catalysed carbonylative coupling

RSC Advances ◽  
2014 ◽  
Vol 4 (57) ◽  
pp. 30019-30027 ◽  
Author(s):  
Tuan Thanh Dang ◽  
Anqi Chen ◽  
Abdul Majeed Seayad

Palladium nanoparticles on ZIF-8 as a robust and recyclable catalyst for Weinreb amide and ketone synthesis through carbonylative coupling.

Author(s):  
Nurcahyo I. Prakoso ◽  
Fuyuhiko Matsuda ◽  
Taiki Umezawa

An efficient synthesis of α,β-dichlorinated ketones from α,β-dichlorinated Weinreb amides is described. Quenching with nonaqueous HCl avoided side reactions associated with the typical a work-up procedure. The amide accepted various...


2021 ◽  
pp. 106328
Author(s):  
Tiefeng Xu ◽  
Panting Lu ◽  
Sebastian Wohlrab ◽  
Wenxing Chen ◽  
Armin Springer ◽  
...  

2011 ◽  
Vol 7 ◽  
pp. 1334-1341 ◽  
Author(s):  
Sanny Verma ◽  
Suman L Jain ◽  
Bir Sain

PEG-embedded potassium tribromide ([K+PEG]Br3 −) was found to be an efficient and recyclable catalyst for the synthesis of functionalized piperidines in high yields in a one step, three component coupling between aldehyde, amine and β-keto ester. At the end of the reaction the [K+PEG]Br3 − was readily regenerated from the reaction mixture by treating the residue containing [K+PEG]Br− with molecular bromine.


2013 ◽  
Vol 54 (6) ◽  
pp. 478-482 ◽  
Author(s):  
K.M. Sharnabai ◽  
G. Nagendra ◽  
T.M. Vishwanatha ◽  
Vommina V. Sureshbabu

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