One-pot synthesis and characterization of chalcopyrite CuInS2 nanoparticles

2014 ◽  
Vol 2 (27) ◽  
pp. 10629-10633 ◽  
Author(s):  
Chivin Sun ◽  
Zehra Cevher ◽  
Jin Zhang ◽  
Bo Gao ◽  
Kai Shum ◽  
...  
Keyword(s):  
Reaction Times ◽  
Synthesis And Characterization ◽  
Single Source ◽  
One Pot ◽  
Single Source Precursors ◽  
Mercaptopropionic Acid ◽  
One Pot Synthesis ◽  
High Yields

We synthesized tetragonal chalcopyrite CuInS2 (CIS) nanoparticles from molecular single source precursors, (Ph3P)2Cu-(μ-SEt)2In(SEt)2, by a one-pot reaction in the presence of 3-mercaptopropionic acid at reaction times of 3 hours or less with high yields.

scholarly journals A Rapid, Convient and Diversified-Multicomponent Synthesis and Characterization of Pyrano[2,3-b]Indoles

2014 ◽  
Vol 26 ◽  
pp. 69-76
Author(s):  
H.B. Ghodasara ◽  
P.M. Singala ◽  
Viresh H. Shah
Keyword(s):  
Chromatographic Method ◽  
Reaction Times ◽  
Aromatic Aldehydes ◽  
Synthesis And Characterization ◽  
Basic Catalyst ◽  
Multicomponent Synthesis ◽  
One Pot ◽  
High Yields ◽  
Work Up

A series of pyrano[2,3-b]indoles, was efficiently synthesized via one-pot, multi component reaction (MCRs) of 1,3-bifunctional synthon(malononitrile/ethylcyano acetate), aromatic aldehydes and oxiindole in the presence of various basic catalyst. The key advantages of this process are high yields, shorter reaction times, easy work-up, and purification of products by non-chromatographic method.

scholarly journals An Efficient One-Pot Multicomponent Synthesis and Characterization of 5-Cyano-1,2,3,4-Tetrahydropyrimidine Derivatives

2014 ◽  
Vol 40 ◽  
pp. 51-60
Author(s):  
R.G. Vaghasiya ◽  
V.H. Shah
Keyword(s):  
Chromatographic Method ◽  
Reaction Times ◽  
Synthesis And Characterization ◽  
Basic Catalyst ◽  
Multicomponent Synthesis ◽  
One Pot ◽  
High Yields ◽  
Work Up

A series of pyrimidine-5-carbonitrile derivatives was efficiently synthesized via one-pot, multi component reaction (MCRs) of 1,3-bifunctional synthon (ethylcyano acetate), substituted pyrazole-4-carbaldehyde, and thiourea/urea in the presence of basic catalyst. The key advantages of this process are high yields, shorter reaction times, easy work-up, and purification of products by non-chromatographic method.

Synthesis and Characterization of Potential Single-Source Precursors to Group 13−Antimonides

1996 ◽  
Vol 15 (23) ◽  
pp. 5035-5038 ◽  
Author(s):  
Ryan A. Baldwin ◽  
Edward E. Foos ◽  
Richard L. Wells ◽  
Peter S. White ◽  
Arnold L. Rheingold ◽  
...  
Keyword(s):  
Synthesis And Characterization ◽  
Single Source ◽  
Group 13 ◽  
Single Source Precursors

One Pot Synthesis and Characterization of Ultra Fine CeO2 and Cu/CeO2 Nanoparticles. Application for Low Temperature CO Oxidation

2011 ◽  
Vol 11 (10) ◽  
pp. 8593-8598 ◽  
Author(s):  
Apostolos Fotopoulos ◽  
Jiannis Arvanitidis ◽  
Dimitris Christofilos ◽  
Konstantinos Papaggelis ◽  
M. Kalyva ◽  
...  
Keyword(s):  
Low Temperature ◽  
Co Oxidation ◽  
Synthesis And Characterization ◽  
One Pot ◽  
One Pot Synthesis ◽  
Low Temperature Co Oxidation

scholarly journals Multicomponent One Pot Synthesis and Characterization of Novel 4-Furyl-1,4-dihydropyridines

2017 ◽  
Vol 29 (4) ◽  
pp. 735-741
Author(s):  
Ansa Madeeha Zafar ◽  
Samina Aslam ◽  
Samia Khakwani ◽  
Muhammad Naeem Khan ◽  
Munawar Ali Munawar ◽  
...  
Keyword(s):  
Synthesis And Characterization ◽  
One Pot ◽  
One Pot Synthesis
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