Characterization of photo-intermediates in the photo-reaction pathways of a bacteriorhodopsin Y185F mutant using in situ photo-irradiation solid-state NMR spectroscopy

Photo-reaction pathways of a Y185F-bR mutant and, CS*- and O-intermediates were examined using in situ photo-irradiation solid-state 13C NMR spectroscopy.

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Molecular-level characterization of probucol nanocrystal in water by in situ solid-state NMR spectroscopy

International Journal of Pharmaceutics ◽

10.1016/j.ijpharm.2011.11.028 ◽

2012 ◽

Vol 423 (2) ◽

pp. 571-576 ◽

Cited By ~ 23

Author(s):

Junying Zhang ◽

Kenjirou Higashi ◽

Waree Limwikrant ◽

Kunikazu Moribe ◽

Keiji Yamamoto

Keyword(s):

Solid State ◽

Nmr Spectroscopy ◽

Solid State Nmr ◽

Molecular Level ◽

Solid State Nmr Spectroscopy

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Use of Solid-State NMR Spectroscopy for the Characterization of Molecular Structure and Dynamics in Solid Polymer and Hybrid Electrolytes

Polymers ◽

10.3390/polym13081207 ◽

2021 ◽

Vol 13 (8) ◽

pp. 1207

Author(s):

Gabrielle Foran ◽

Nina Verdier ◽

David Lepage ◽

Cédric Malveau ◽

Nicolas Dupré ◽

...

Keyword(s):

Solid State ◽

Nmr Spectroscopy ◽

Solid State Nmr ◽

Pulse Sequence ◽

Dynamic Properties ◽

Double Resonance ◽

Solid Polymer ◽

Pulse Field ◽

Solid State Nmr Spectroscopy

Solid-state NMR spectroscopy is an established experimental technique which is used for the characterization of structural and dynamic properties of materials in their native state. Many types of solid-state NMR experiments have been used to characterize both lithium-based and sodium-based solid polymer and polymer–ceramic hybrid electrolyte materials. This review describes several solid-state NMR experiments that are commonly employed in the analysis of these systems: pulse field gradient NMR, electrophoretic NMR, variable temperature T1 relaxation, T2 relaxation and linewidth analysis, exchange spectroscopy, cross polarization, Rotational Echo Double Resonance, and isotope enrichment. In this review, each technique is introduced with a short description of the pulse sequence, and examples of experiments that have been performed in real solid-state polymer and/or hybrid electrolyte systems are provided. The results and conclusions of these experiments are discussed to inform readers of the strengths and weaknesses of each technique when applied to polymer and hybrid electrolyte systems. It is anticipated that this review may be used to aid in the selection of solid-state NMR experiments for the analysis of these systems.

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Characterization of humic acids derived from Leonardite using a solid-state NMR spectroscopy and effects of humic acids on growth and nutrient uptake of snap bean

Chemical Speciation and Bioavailability ◽

10.1080/09542299.2015.1118361 ◽

2015 ◽

Vol 27 (4) ◽

pp. 156-161 ◽

Cited By ~ 9

Author(s):

Sun Qian ◽

Weimin Ding ◽

Yuncong Li ◽

Guodong Liu ◽

Jiuai Sun ◽

...

Keyword(s):

Solid State ◽

Nmr Spectroscopy ◽

Nutrient Uptake ◽

Humic Acids ◽

Solid State Nmr ◽

Snap Bean ◽

Solid State Nmr Spectroscopy

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A kinetic study of mechanochemical halogen bond formation by in situ31P solid-state NMR spectroscopy

Chemical Communications ◽

10.1039/c7cc05051h ◽

2017 ◽

Vol 53 (71) ◽

pp. 9930-9933 ◽

Cited By ~ 9

Author(s):

Yijue Xu ◽

Lysiane Champion ◽

Bulat Gabidullin ◽

David L. Bryce

Keyword(s):

Activation Energy ◽

Solid State ◽

Nmr Spectroscopy ◽

Kinetic Study ◽

Solid State Nmr ◽

Halogen Bond ◽

Bond Formation ◽

Nmr Studies ◽

Solid State Nmr Spectroscopy

In situ 31P solid-state NMR studies of mechanochemical halogen bond formation provide insights into the cocrystallisation process and an estimate of the activation energy.

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