Preparation and characterization of Ni/mZSM-5 zeolite with a hierarchical pore structure by using KIT-6 as silica template: an efficient bi-functional catalyst for the reduction of nitro aromatic compounds

RSC Advances ◽  
2015 ◽  
Vol 5 (43) ◽  
pp. 34398-34414 ◽  
Author(s):  
Omid Mazaheri ◽  
Roozbeh Javad Kalbasi

Ni/mZSM-5 hierarchical zeolite and the acidic form of it were prepared as novel bi-functional catalysts which showed excellent activity for reduction of nitro aromatic compounds in aqueous medium at room temperature.

2009 ◽  
Vol 20 (11) ◽  
pp. 1371-1375 ◽  
Author(s):  
Dong Liang ◽  
Yan Wang ◽  
Jing Hong Ma ◽  
Jian Hong Liu ◽  
Shu Wei Chen ◽  
...  

2011 ◽  
Author(s):  
Danling Wang ◽  
Antao Chen ◽  
Qifeng Zhang ◽  
Guozhong Cao

2017 ◽  
Vol 52 (20) ◽  
pp. 12445-12454 ◽  
Author(s):  
Qingquan Kong ◽  
Wei Feng ◽  
Xiaodong Zhu ◽  
Chenghua Sun ◽  
Juan Ma ◽  
...  

Author(s):  
Bradley L. Thiel ◽  
Chan Han R. P. ◽  
Kurosky L. C. Hutter ◽  
I. A. Aksay ◽  
Mehmet Sarikaya

The identification of extraneous phases is important in understanding of high Tc superconducting oxides. The spectroscopic techniques commonly used in determining the origin of superconductivity (such as RAMAN, XPS, AES, and EXAFS) are surface-sensitive. Hence a grain boundary phase several nanometers thick could produce irrelevant spectroscopic results and cause erroneous conclusions. The intergranular phases present a major technological consideration for practical applications. In this communication we report the identification of a Cu2O grain boundary phase which forms during the sintering of YBa2Cu3O7-x (1:2:3 compound).Samples are prepared using a mixture of Y2O3. CuO, and BaO2 powders dispersed in ethanol for complete mixing. The pellets pressed at 20,000 psi are heated to 950°C at a rate of 5°C per min, held for 1 hr, and cooled at 1°C per min to room temperature. The samples show a Tc of 91K with a transition width of 2K. In order to prevent damage, a low temperature stage is used in milling to prepare thin foils which are then observed, using a liquid nitrogen holder, in a Philips 430T at 300 kV.


RSC Advances ◽  
2021 ◽  
Vol 11 (22) ◽  
pp. 13245-13255
Author(s):  
Mehdi Davoodi ◽  
Fatemeh Davar ◽  
Mohammad R. Rezayat ◽  
Mohammad T. Jafari ◽  
Mehdi Bazarganipour ◽  
...  

New nanocomposite of zeolitic imidazolate framework-67@magnesium aluminate spinel (ZIF-67@MgAl2O4) has been fabricated by a simple method at room temperature with different weight ratios.


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