Continuous flow synthesis of the iodination agent 1,3-diiodo-5,5-dimethyl-imidazolidine-2,4-dione telescoped with semi-continuous product isolation

2016 ◽  
Vol 1 (4) ◽  
pp. 379-386 ◽  
Author(s):  
Marta Ferreri ◽  
Audun Drageset ◽  
Cristian Gambarotti ◽  
Hans-René Bjørsvik
Keyword(s):  
Continuous Flow ◽  
Flow Mode ◽  
Target Product ◽  
Vacuum Filtration ◽  
Flow Synthesis ◽  
Work Up ◽  
Continuous Product ◽  
Mode A

A synthesis for the iodination agent DIH was devised, developed, and optimized for both batch and flow mode. A concatenated semi-continuous product work-up by means of vacuum filtration was used for the isolation of a target product that precipitated during the course of the reaction.

Reaction Calorimetry in Continuous Flow Mode: A New Approach for the Thermal Characterization of High Energetic and Fast Reactions

2020 ◽  
Vol 24 (10) ◽  
pp. 2004-2016
Author(s):  
Frederik Mortzfeld ◽  
Jutta Polenk ◽  
Bertrand Guelat ◽  
Francesco Venturoni ◽  
Berthold Schenkel ◽  
...  
Keyword(s):  
Continuous Flow ◽  
Thermal Characterization ◽  
Reaction Calorimetry ◽  
Flow Mode ◽  
New Approach ◽  
Fast Reactions ◽  
Mode A

Continuous flow synthesis concatenated with continuous flow liquid–liquid extraction for work-up and purification: selective mono- and di-iodination of the imidazole backbone

2016 ◽  
Vol 1 (4) ◽  
pp. 436-444 ◽  
Author(s):  
Audun Drageset ◽  
Hans-René Bjørsvik
Keyword(s):  
Continuous Flow ◽  
Flow Reactor ◽  
Liquid Extraction ◽  
Flow Synthesis ◽  
Liquid Liquid Extraction ◽  
Flow Processes ◽  
Work Up

Flow processes for mono- and di-iodination of the imidazole backbone were devised, developed, and implemented on the multi-jet oscillating disk (MJOD) flow reactor platform.

Continuous flow synthesis of the lamivudine precursor L-Menthyl Glyoxylate

2021 ◽  
Author(s):  
Lais S. D. Azevedo ◽  
Anderson R. Aguillon ◽  
Marcelo T. Lima ◽  
Raquel A. C. Leão ◽  
Rodrigo O. M. A. de Souza
Keyword(s):  
Continuous Flow ◽  
Flow Synthesis

Continuous Flow Synthesis of Persistent Luminescent Chromium-Doped Zinc Gallate Nanoparticles

2021 ◽  
pp. 7067-7075
Author(s):  
Xiaojun Wei ◽  
Stephen V. Kershaw ◽  
Xiaodan Huang ◽  
Mingxia Jiao ◽  
Chau Chun Beh ◽  
...  
Keyword(s):  
Continuous Flow ◽  
Flow Synthesis ◽  
Zinc Gallate

scholarly journals Continuous flow synthesis of azoxybenzenes by reductive dimerization of nitrosobenzenes with gel‐bound catalysts

2021 ◽  
Author(s):  
Carsten J. Schmiegel ◽  
Patrik Berg ◽  
Franziska Obst ◽  
Roland Schoch ◽  
Dietmar Appelhans ◽  
...  
Keyword(s):  
Continuous Flow ◽  
Flow Synthesis ◽  
Reductive Dimerization

scholarly journals Continuous Flow Synthesis of Metal–NHC Complexes**

2021 ◽  
Vol 27 (18) ◽  
pp. 5653-5657 ◽  
Author(s):  
Andreas Simoens ◽  
Thomas Scattolin ◽  
Thibault Cauwenbergh ◽  
Gianmarco Pisanò ◽  
Catherine S. J. Cazin ◽  
...  
Keyword(s):  
Continuous Flow ◽  
Flow Synthesis

scholarly journals Continuous‐Flow Synthesis of High‐Quality Few‐Layer Antimonene Hexagons

2021 ◽  
pp. 2101616
Author(s):  
Iñigo Torres ◽  
Marta Alcaraz ◽  
Roger Sanchis‐Gual ◽  
Jose A. Carrasco ◽  
Michael Fickert ◽  
...  
Keyword(s):  
Continuous Flow ◽  
High Quality ◽  
Flow Synthesis

scholarly journals Continuous-Flow Synthesis of Thioureas, Enabled by Aqueous Polysulfide Solution

Molecules ◽  
2021 ◽  
Vol 26 (2) ◽  
pp. 303
Author(s):  
András Gy. Németh ◽  
Renáta Szabó ◽  
György Orsy ◽  
István M. Mándity ◽  
György M. Keserű ◽  
...  
Keyword(s):  
Multicomponent Reaction ◽  
Continuous Flow ◽  
Flow Synthesis ◽  
Mild Conditions ◽  
Wide Range ◽  
Simple Filtration

We have developed the continuous-flow synthesis of thioureas in a multicomponent reaction starting from isocyanides, amidines, or amines and sulfur. The aqueous polysulfide solution enabled the application of sulfur under homogeneous and mild conditions. The crystallized products were isolated by simple filtration after the removal of the co-solvent, and the sulfur retained in the mother liquid. Presenting a wide range of thioureas synthesized by this procedure confirms the utility of the convenient continuous-flow application of sulfur.

scholarly journals Continuous‐Flow Synthesis of ZIF‐8 Biocomposites with Tunable Particle Size

2020 ◽  
Vol 59 (21) ◽  
pp. 8123-8127 ◽  
Author(s):  
Francesco Carraro ◽  
Jason D. Williams ◽  
Mercedes Linares‐Moreau ◽  
Chiara Parise ◽  
Weibin Liang ◽  
...  
Keyword(s):  
Particle Size ◽  
Continuous Flow ◽  
Flow Synthesis
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