Continuous-flow synthesis of fluorine-containing fine chemicals with integrated benchtop NMR analysis

2017 ◽  
Vol 2 (3) ◽  
pp. 315-323 ◽  
Author(s):  
Thomas H. Rehm ◽  
Christian Hofmann ◽  
Dorothee Reinhard ◽  
Hans-Joachim Kost ◽  
Patrick Löb ◽  
...  
Keyword(s):  
Chemical Synthesis ◽  
Continuous Flow ◽  
Fine Chemicals ◽  
Nmr Analysis ◽  
Online Analysis ◽  
Flow Synthesis ◽  
Fine Chemical

Fluorine fine chemical synthesis takes a step ahead using integrated NMR online-analysis with a benchtop NMR spectrometer.

scholarly journals Integrating continuous flow synthesis with in-line analysis and data generation

2018 ◽  
Vol 16 (33) ◽  
pp. 5946-5954 ◽  
Author(s):  
Marcus Baumann
Keyword(s):  
Continuous Flow ◽  
Fine Chemicals ◽  
Data Generation ◽  
Flow Synthesis ◽  
Niche Area ◽  
Industrial Settings ◽  
Line Analysis

Continuous flow synthesis of fine chemicals has successfully advanced from an academic niche area to a rapidly growing field of its own that directly impacts developments and applications in industrial settings.

scholarly journals Iridium-based hydride transfer catalysts: from hydrogen storage to fine chemicals

2018 ◽  
Vol 54 (56) ◽  
pp. 7711-7724 ◽  
Author(s):  
Zhiyao Lu ◽  
Valeriy Cherepakhin ◽  
Ivan Demianets ◽  
Paul J. Lauridsen ◽  
Travis J. Williams
Keyword(s):  
Chemical Synthesis ◽  
Hydrogen Storage ◽  
Hydrogen Transfer ◽  
Hydride Transfer ◽  
Central Research ◽  
Fine Chemicals ◽  
Research Focus ◽  
Fine Chemical

Selective hydrogen transfer remains a central research focus in catalysis: hydrogenation and dehydrogenation have central roles, both historical and contemporary, in all aspects of fuel, agricultural, pharmaceutical, and fine chemical synthesis.

Pt-Catalyzed selective oxidation of alcohols to aldehydes with hydrogen peroxide using continuous flow reactors

2021 ◽  
Vol 19 (5) ◽  
pp. 1115-1121
Author(s):  
Yoshihiro Kon ◽  
Takuya Nakashima ◽  
Akira Yada ◽  
Tadahiro Fujitani ◽  
Shun-ya Onozawa ◽  
...  
Keyword(s):  
Hydrogen Peroxide ◽  
Selective Oxidation ◽  
Continuous Flow ◽  
Fine Chemicals ◽  
Flow Reactors ◽  
Flow Synthesis ◽  
Oxidation Of Alcohols ◽  
Continuous Flow Reactors ◽  
Pt Catalyzed

Pt-catalyzed continuous flow synthesis of aldehydes from alcohols has been developed, in which various aldehydes for obtaining valuable fine chemicals were given in up to 98% yields for over 5 days by using hydrogen peroxide as an oxidant.

Use of immobilized organic base catalysts for continuous-flow fine chemical synthesis

2008 ◽  
Vol 258 (2) ◽  
pp. 289-295 ◽  
Author(s):  
L SOLDI ◽  
W FERSTL ◽  
S LOEBBECKE ◽  
R MAGGI ◽  
C MALMASSARI ◽  
...  
Keyword(s):  
Chemical Synthesis ◽  
Continuous Flow ◽  
Organic Base ◽  
Fine Chemical ◽  
Base Catalysts

Continuous flow synthesis of the lamivudine precursor L-Menthyl Glyoxylate

2021 ◽  
Author(s):  
Lais S. D. Azevedo ◽  
Anderson R. Aguillon ◽  
Marcelo T. Lima ◽  
Raquel A. C. Leão ◽  
Rodrigo O. M. A. de Souza
Keyword(s):  
Continuous Flow ◽  
Flow Synthesis

Continuous Flow Synthesis of Persistent Luminescent Chromium-Doped Zinc Gallate Nanoparticles

2021 ◽  
pp. 7067-7075
Author(s):  
Xiaojun Wei ◽  
Stephen V. Kershaw ◽  
Xiaodan Huang ◽  
Mingxia Jiao ◽  
Chau Chun Beh ◽  
...  
Keyword(s):  
Continuous Flow ◽  
Flow Synthesis ◽  
Zinc Gallate

scholarly journals Continuous flow synthesis of azoxybenzenes by reductive dimerization of nitrosobenzenes with gel‐bound catalysts

2021 ◽  
Author(s):  
Carsten J. Schmiegel ◽  
Patrik Berg ◽  
Franziska Obst ◽  
Roland Schoch ◽  
Dietmar Appelhans ◽  
...  
Keyword(s):  
Continuous Flow ◽  
Flow Synthesis ◽  
Reductive Dimerization

scholarly journals Continuous Flow Synthesis of Metal–NHC Complexes**

2021 ◽  
Vol 27 (18) ◽  
pp. 5653-5657 ◽  
Author(s):  
Andreas Simoens ◽  
Thomas Scattolin ◽  
Thibault Cauwenbergh ◽  
Gianmarco Pisanò ◽  
Catherine S. J. Cazin ◽  
...  
Keyword(s):  
Continuous Flow ◽  
Flow Synthesis

scholarly journals Continuous‐Flow Synthesis of High‐Quality Few‐Layer Antimonene Hexagons

2021 ◽  
pp. 2101616
Author(s):  
Iñigo Torres ◽  
Marta Alcaraz ◽  
Roger Sanchis‐Gual ◽  
Jose A. Carrasco ◽  
Michael Fickert ◽  
...  
Keyword(s):  
Continuous Flow ◽  
High Quality ◽  
Flow Synthesis

scholarly journals Continuous-Flow Synthesis of Thioureas, Enabled by Aqueous Polysulfide Solution

Molecules ◽  
2021 ◽  
Vol 26 (2) ◽  
pp. 303
Author(s):  
András Gy. Németh ◽  
Renáta Szabó ◽  
György Orsy ◽  
István M. Mándity ◽  
György M. Keserű ◽  
...  
Keyword(s):  
Multicomponent Reaction ◽  
Continuous Flow ◽  
Flow Synthesis ◽  
Mild Conditions ◽  
Wide Range ◽  
Simple Filtration

We have developed the continuous-flow synthesis of thioureas in a multicomponent reaction starting from isocyanides, amidines, or amines and sulfur. The aqueous polysulfide solution enabled the application of sulfur under homogeneous and mild conditions. The crystallized products were isolated by simple filtration after the removal of the co-solvent, and the sulfur retained in the mother liquid. Presenting a wide range of thioureas synthesized by this procedure confirms the utility of the convenient continuous-flow application of sulfur.

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