Cancelled article – The hydrothermal temperature dependence of ZnO nanostructure morphologies grown on GaN/Al2O3

In this paper, we demonstrated the acicular-like ZnO nanostructure powder were prepared by hydrothermal method. We used the industrial aerosol elemental zinc powders through high energy ball mill, and then took ball mill zinc powder into autoclave reactor direct synthesis high length to diameter ratio of acicular-like ZnO nanostructure powder. The samples phase were studied by XRD, the morphology of the sample were observed by SEM, the samples of luminous performance were studied by Fluorescence spectrophotometer. When the hydrothermal temperature is 200°C, hydrothermal time is 24 h, mineralizer of NaOH concentration is 1 mol/L, the samples were washed by alcohol and then dried at 80°C for 3 hours. We had synthesized the high dispersion, high length to diameter ratio up to 50 acicular-like ZnO nanostructure powder.

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Effect of Hydrothermal Reaction Conditions on the Sizes and Morphologies of ZnO Nanorods

Advanced Materials Research ◽

10.4028/www.scientific.net/amr.765-767.3170 ◽

2013 ◽

Vol 765-767 ◽

pp. 3170-3175 ◽

Cited By ~ 1

Author(s):

Jian Jiao Zhang ◽

Hong Yan Yue ◽

Er Jun Guo ◽

Li Ping Wang ◽

Chun Yu Zhang ◽

...

Keyword(s):

Hydrothermal Reaction ◽

Zno Nanorods ◽

Influence Factors ◽

Particle Morphology ◽

Precursor Concentration ◽

X Ray Diffraction ◽

Reaction Conditions ◽

Hydrothermal Temperature ◽

Zno Nanostructure ◽

Temperature Time

The influence factors of hydrothermal treatment on the formation process of ZnO nanorods are investigated involving with hydrothermal temperature, time and precursor concentration. The as-obtained products were characterized by Scanning Electron microscope (SEM) and X-ray diffraction (XRD), respectively. XRD result indicates that the obtained ZnO nanorods are high-quality single crystals. SEM results indicate that both the diameter and the length of ZnO nanorods increase with increasing the hydrothermal time and temperature. The precursor concentration prominently determines the morphologies of ZnO nanostructure from initial particle morphology to rod-like, and to final slice-like morphology.

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Correction to: Hydrothermal temperature dependence of CaWO4 nanoparticles: structural, optical, morphology and photocatalytic activity

Journal of Materials Science Materials in Electronics ◽

10.1007/s10854-021-07490-1 ◽

2021 ◽

Author(s):

F. X. Nobre ◽

R. Muniz ◽

E. R. do Nascimento ◽

R. S. Amorim ◽

R. S. Silva ◽

...

Keyword(s):

Photocatalytic Activity ◽

Temperature Dependence ◽

Hydrothermal Temperature

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Temperature Dependence of the Critical Electron Dose for Fatty Acid Monolayers

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100053188 ◽

1982 ◽

Vol 40 ◽

pp. 78-79

Author(s):

Kenneth H. Downing ◽

Robert M. Glaeser

Keyword(s):

Electron Beam ◽

Fatty Acid ◽

Inelastic Scattering ◽

Temperature Dependence ◽

Structural Damage ◽

Direct Result ◽

Second Step ◽

Strong Temperature Dependence ◽

Electron Dose ◽

Covalent Bonds

The structural damage of molecules irradiated by electrons is generally considered to occur in two steps. The direct result of inelastic scattering events is the disruption of covalent bonds. Following changes in bond structure, movement of the constituent atoms produces permanent distortions of the molecules. Since at least the second step should show a strong temperature dependence, it was to be expected that cooling a specimen should extend its lifetime in the electron beam. This result has been found in a large number of experiments, but the degree to which cooling the specimen enhances its resistance to radiation damage has been found to vary widely with specimen types.

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Temperature Dependence of Magnetic Domains and Wall Structures

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s042482010009573x ◽

1972 ◽

Vol 30 ◽

pp. 496-497

Author(s):

Sonoko Tsukahara ◽

Tadami Taoka ◽

Hisao Nishizawa

Keyword(s):

Temperature Dependence ◽

Domain Walls ◽

Magnetic Domain ◽

Iron Film ◽

Objective Lens ◽

Lorentz Microscopy ◽

Domain Structures ◽

Wall Structures ◽

Crystal Films ◽

Metallurgical Structure

The high voltage Lorentz microscopy was successfully used to observe changes with temperature; of domain structures and metallurgical structures in an iron film set on the hot stage combined with a goniometer. The microscope used was the JEM-1000 EM which was operated with the objective lens current cut off to eliminate the magnetic field in the specimen position. Single crystal films with an (001) plane were prepared by the epitaxial growth of evaporated iron on a cleaved (001) plane of a rocksalt substrate. They had a uniform thickness from 1000 to 7000 Å.The figure shows the temperature dependence of magnetic domain structure with its corresponding deflection pattern and metallurgical structure observed in a 4500 Å iron film. In general, with increase of temperature, the straight domain walls decrease in their width (at 400°C), curve in an iregular shape (600°C) and then vanish (790°C). The ripple structures with cross-tie walls are observed below the Curie temperature.

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