Suzuki–Miyaura Cross-Couplings under Acidic Conditions
Keyword(s):
Suzuki–Miyaura reactions with Pd(PPh3)4 have been carried out using lithium N-phenylsydnone-4-carboxylate as additive, which gave best yields at pH 5.7 in a mixture of acetic acid, water, and sodium carbonate. Reaction parameters such as the Pd source, the solvent, reaction time and temperature, acid, base and carboxylate have been varied and some representative examples of the Suzuki–Miyaura reaction have been examined.
2011 ◽
Vol 311-313
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pp. 1514-1517
2004 ◽
Vol 94
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pp. 1965-1968
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1964 ◽
Vol 9
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pp. 215-217
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1974 ◽
Vol 52
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pp. 1013-1017
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1981 ◽
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pp. 619-620
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2007 ◽
Vol 23
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pp. 323-328
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