scholarly journals Preparation and characterizations of activated carbon monolith from rubber wood and its effect on supercapacitor performances

Author(s):  
E. Taer ◽  
R. Taslim ◽  
M. Deraman
2016 ◽  
Vol 1 (1) ◽  
Author(s):  
Erman Taer

<p>Preparation of hierarchical macropore activated carbon monolith (HMACM) from rubber wood was investigated. The samples were prepared with small cutting of rubber wood in cross sectional method. The electrode preparation was started by pre-carbonization process followed by carbonization at 600 <sup>o</sup>C and physical activation process at 900<sup> o</sup>C in N<sub>2</sub> and CO<sub>2</sub> gas atmosphere, respectively. The samples then were followed by chemical activation process with combination of chemical activation agent of KOH and HNO3 solutions. The HMACMs were neutralized by immersing the samples in copious amount of water and dried the samples for 24 hours. Porosity properties were performed by N<sub>2</sub> adsorption-desorption data and morphology characterization was analyzed by scanning electron microscope (SEM) instrument. The electrochemical properties was studied by electrochemical impedance spectroscopy, cyclic voltammetry and charge-discharge at constan current methode.  The SEM micrograph and adsorption-desorption data were also proved that the HMACM sample have a hierarchical macropore at the surface and crossectional section. The porosity data shown the HMACM sample have BET surface area of 331 m<sup>2</sup>/g with average pore diameter of 1.7 nm. Equivalent series resistance and optimum capacitance specific of the HMACM electrode of 0.77 Ohm and 154 F/g, respectively. In conclusion, this study showed that the preparation method would propose as a simple method of HMACM electrode preparation technique for supercapacitor applications.</p>


2016 ◽  
Vol 1 ◽  
Author(s):  
Erman Taer

<p>Preparation of hierarchical macropore activated carbon monolith (HMACM) from rubber wood was investigated. The samples were prepared with small cutting of rubber wood in cross sectional method. The electrode preparation was started by pre-carbonization process followed by carbonization at 600 <sup>o</sup>C and physical activation process at 900<sup> o</sup>C in N<sub>2</sub> and CO<sub>2</sub> gas atmosphere, respectively. The samples then were followed by chemical activation process with combination of chemical activation agent of KOH and HNO3 solutions. The HMACMs were neutralized by immersing the samples in copious amount of water and dried the samples for 24 hours. Porosity properties were performed by N<sub>2</sub> adsorption-desorption data and morphology characterization was analyzed by scanning electron microscope (SEM) instrument. The electrochemical properties was studied by electrochemical impedance spectroscopy, cyclic voltammetry and charge-discharge at constan current methode.  The SEM micrograph and adsorption-desorption data were also proved that the HMACM sample have a hierarchical macropore at the surface and crossectional section. The porosity data shown the HMACM sample have BET surface area of 331 m<sup>2</sup>/g with average pore diameter of 1.7 nm. Equivalent series resistance and optimum capacitance specific of the HMACM electrode of 0.77 Ohm and 154 F/g, respectively. In conclusion, this study showed that the preparation method would propose as a simple method of HMACM electrode preparation technique for supercapacitor applications.</p>


2020 ◽  
Vol 44 (13) ◽  
pp. 10192-10205
Author(s):  
Erman Taer ◽  
Novi Yanti ◽  
Widya Sinta Mustika ◽  
Apriwandi Apriwandi ◽  
Rika Taslim ◽  
...  

2018 ◽  
Vol 180 ◽  
pp. 155-165 ◽  
Author(s):  
Kiman Silas ◽  
Wan Azlina Wan Ab Karim Ghani ◽  
Thomas Shean Yaw Choong ◽  
Umer Rashid

2015 ◽  
Vol 1112 ◽  
pp. 299-302
Author(s):  
Sepideh Soltaninejad ◽  
Mohamad Deraman ◽  
Rusli Daik ◽  
N.S.M. Nor ◽  
B.N.M. Dolah ◽  
...  

Fibers of oil palm empty fruit bunches were carbonized at low temperature, milled and sieved to produce self-adhesive carbon grain (SACG). Grain monolith (GMs) of SACG added with 0 %, 20 % and 40 % cellulose powder were carbonized and activated to produce porous activated carbon monolith (ACMs) supercapacitor electrodes. ACMs were investigated by nitrogen adsorption–desorption isotherm and cyclic voltammetry methods to determine the effect of cellulose on the porosity and specific capacitance of the electrodes, respectively. The results showed that the addition of cellulose in GMs reduced the specific surface area of the ACMs by a factor of 94 % to 97 %, coresponding to a decrease of 31 % to 54 % in the values of specific capacitor of the ACMs supercapacitor cells.


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