ON THE CAPILLARY GAS CHROMATOGRAPHIC DETERMINATION OF PETROLEUM HYDROCARBONS IN ENVIRONMENTAL SAMPLES

1999 ◽  
Vol 29 (3) ◽  
pp. 281-282
Author(s):  
Jáb Krupčik ◽  
Peter Oswald ◽  
Ivan Špánik ◽  
Eva Benická ◽  
Pavol Daučik
2019 ◽  
Vol 16 (31) ◽  
pp. 431-439
Author(s):  
Helilma de Andréa PINHEIRO ◽  
Ana Paula Mota FERREIRA ◽  
Ismael Carlos Braga ALVES ◽  
Antônio Fernandes SANTOS JÚNIOR ◽  
Raquel Bezerra dos Santos SAWCZUK ◽  
...  

The contamination of water and soil by petroleum hydrocarbons is reported quite frequently, mainly due to accidents involving transport and storage of fuels. Among the most toxic compounds the most volatile benzene, toluene, ethylbenzene and xylene (BTEX). Residues of these compounds can cause serious environmental and public health troubles. Thus, more sensitive, selective and low-cost techniques, focused on the analysis and monitoring of these contaminants are being developed in order to establish operational control and to comply with local laws, but the intellectual property of such technologies is still unknown. The present study shows the panorama about patents, thesis and dissertations which have been already published on this theme. Together, the United States and China hold the largest number of patents, and most of thesis/dissertations describe methodologies for BTEX detection in water, although numerous environmental problems caused by oils in the soil had been reported. Also, the methods based on chromatographic techniques stand out in relation to the other techniques. It was possible to verify important advances in the field of sensors, especially the electrochemical ones, in order to solve the analytical gaps.


1977 ◽  
Vol 6 (1) ◽  
pp. 221-231 ◽  
Author(s):  
Robert F. Moseman ◽  
Howard L. Crist ◽  
Thomas R. Edgerton ◽  
M. Keith Ward

1974 ◽  
Vol 57 (5) ◽  
pp. 1046-1049
Author(s):  
Richard H Larose

Abstract A method is described which permits the removal of interfering co-extractives from lindane, using high-speed liquid chromatography. Fractions are collected from the liquid chromatograph for further analysis by gas-liquid chromatography. The cleanup procedure takes less than 5 min and recoveries of more than 90% are obtained. The detection limit for water samples is 5 ng/L.


2002 ◽  
Vol 18 (3) ◽  
pp. 343-346 ◽  
Author(s):  
Hyun-Mee PARK ◽  
Young-Man KIM ◽  
Dai Woon LEE ◽  
Su-won LEE ◽  
Kang-Bong LEE

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