The effect of magnetic domain structure on Bragg reflection in transmission electron microscopy

1964 ◽  
Vol 10 (104) ◽  
pp. 277-290 ◽  
Author(s):  
J. P. Jakubovics
1991 ◽  
Vol 232 ◽  
Author(s):  
A. D. Beale ◽  
M. G. Hetherington ◽  
J. P. Jakubovics ◽  
B. A. Lewis ◽  
C. B. Scruby

ABSTRACTMagnetoacoustic emission (MAE) and Barkhausen emission (BE) measurements have been carried out on steel specimens heat treated to produce various microstructures ranging from martensitic/bainitic to ferritic/pearlitic. The magnetic domain structure of the specimens has been studied using transmission electron microscopy, and micromagnetic processes have been observed using an in-situ magnetizing device. The results are used in the interpretation of the MAE and BE measurements.


Materials ◽  
2021 ◽  
Vol 14 (11) ◽  
pp. 2849
Author(s):  
Marcin Jan Dośpiał

This paper presents domain and structure studies of bonded magnets made from nanocrystalline Nd-(Fe, Co)-B powder. The structure studies were investigated using scanning electron microscopy (SEM), high-resolution transmission electron microscopy (HRTEM), Mössbauer spectroscopy and X-ray diffractometry. On the basis of performed qualitative and quantitative phase composition studies, it was found that investigated alloy was mainly composed of Nd2(Fe-Co)14B hard magnetic phase (98 vol%) and a small amount of Nd1.1Fe4B4 paramagnetic phase (2 vol%). The best fit of grain size distribution was achieved for the lognormal function. The mean grain size determined from transmission electron microscopy (TEM) images on the basis of grain size distribution and diffraction pattern using the Bragg equation was about ≈130 nm. HRTEM images showed that over-stoichiometric Nd was mainly distributed on the grain boundaries as a thin amorphous border of 2 nm in width. The domain structure was investigated using a scanning electron microscope and metallographic light microscope, respectively, by Bitter and Kerr methods, and by magnetic force microscopy. Domain structure studies revealed that the observed domain structure had a labyrinth shape, which is typically observed in magnets, where strong exchange interactions between grains are present. The analysis of the domain structure in different states of magnetization revealed the dynamics of the reversal magnetization process.


2011 ◽  
Vol 17 (S2) ◽  
pp. 1892-1893
Author(s):  
A Bencan ◽  
T Rojac ◽  
G Drazic ◽  
M Kosec ◽  
D Damjanovic

Extended abstract of a paper presented at Microscopy and Microanalysis 2011 in Nashville, Tennessee, USA, August 7–August 11, 2011.


1984 ◽  
Vol 37 ◽  
Author(s):  
A. F. Marshall ◽  
F. Hellman ◽  
B. Oh

AbstractFilms of Nb3Sn vapor deposited at low rates and high temperatures on (1102) sapphire form an epitaxial <100> single crystal matrix with a domain structure of misoriented regions bounded by low-angle dislocation boundaries. Nucleation of other orientations at the interface result in a highly oriented but polycrystalline film through approximately the first thousand Angstroms of film thickness. After this point random orientations become overgrown by epitaxial <100> regions. At slightly lower temperatures many small <100> grains with a second epitaxial relationship also nucleate at the interface. These rotated grains persist through greater thicknesses than random orientations. The misorientation defect structure of the single crystal matrix is analyzed by transmission electron microscopy.


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