An Experimental Study on the Uptake Factor of Tungsten Oxide Particles Resulting from an Accidentally Dropped Storage Container

2013 ◽  
Vol 10 (7) ◽  
pp. 357-367
Author(s):  
Zhi Gao ◽  
J. S. Zhang ◽  
Jerry G.A. Byington
2021 ◽  
Vol 40 (1) ◽  
pp. 171-177
Author(s):  
Yue Wang ◽  
Ben Fu Long ◽  
Chun Yu Liu ◽  
Gao An Lin

Abstract Herein, the evolution of reduction process of ultrafine tungsten powder in industrial conditions was investigated. The transition process of morphology and composition was examined via SEM, XRD, and calcination experiments. The results show that the reduction sequence of WO2.9 was WO2.9 → WO2.72 → WO2 → W on the surface, but WO2.9 → WO2 → W inside the oxide particles. With the aid of chemical vapor transport of WO x (OH) y , surface morphology transformed into rod-like, star-shaped cracking, floret, irregularly fibrous structure, and finally, spherical tungsten particles.


2011 ◽  
Vol 11 (6) ◽  
pp. 4659-4666 ◽  
Author(s):  
Vijay Bhooshan Kumar ◽  
Clara Ermine Sawian ◽  
Dambarudhar Mohanta ◽  
Shashi Baruah ◽  
NashreenS. Islam

ACS Omega ◽  
2017 ◽  
Vol 2 (8) ◽  
pp. 5104-5110 ◽  
Author(s):  
Yohei Ishida ◽  
Shingo Motono ◽  
Wataru Doshin ◽  
Tomoharu Tokunaga ◽  
Hiroki Tsukamoto ◽  
...  

2015 ◽  
Vol 2015 (0) ◽  
pp. _OS1406-34-_OS1406-34
Author(s):  
Tomoki MIFUNE ◽  
Hiroyuki MIYAMOTO ◽  
Hiroshi FUJIWARA ◽  
Takuya GOTO

2011 ◽  
Vol 62 (2) ◽  
pp. 248-255 ◽  
Author(s):  
S. Aravinth ◽  
Binu Sankar ◽  
S.R. Chakravarthi ◽  
R. Sarathi

2019 ◽  
Vol 61 (1) ◽  
pp. 163
Author(s):  
Х.А. Абдуллин ◽  
А.А. Азаткалиев ◽  
М.Т. Габдуллин ◽  
Ж.К. Калкозова ◽  
Б.Н. Мукашев ◽  
...  

AbstractNanopowder tungsten oxide and metallic tungsten are obtained via pyrolysis of ammonium metatungstate. Two methods are used for the synthesis of tungsten oxide: the use of a fibrous matrix and pyrolysis of aerosol particles. Tungsten oxide particles are formed during the pyrolysis in air. Metallic tungsten nanoparticles are obtained via subsequent thermal reduction of tungsten oxide in hydrogen. The structure and morphology of the samples are studied with X-ray diffraction and scanning electron microscopy. Tungsten nanopowders with average sizes from 7 to 30 nm are obtained depending on synthesis temperature. The electrochemical characteristics of electrodes coated with tungsten nanoparticles are studied with cyclic voltammetry, impedance spectroscopy, and galvanostatic charge–discharge methods. An electrode with W nanoparticles exhibited a specific low-frequency capacitance of about 90 F/g due to thin tungsten oxide film on the surface of tungsten nanoparticles.


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