Improved route to a diphenoxide-based precursor for chemical vapour deposition of parylene AF-4
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In this work, we present the synthesis of an alternative precursor for chemical vapour deposition of parylene AF-4 to the widely used standard, octafluoro[2.2]paracyclophane. The standard precursor suffers from uncertainties in its supply chain and its synthesis is of low yield. A comparison between different reaction parameters and solvents is drawn by means of thermal, laboratory-scale and microwave-assisted reactions and quantitative nuclear magnetic resonance (qNMR) studies.
2011 ◽
Vol 258
(3)
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pp. 1045-1051
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2002 ◽
Vol 82
(1)
◽
pp. 137-165
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1999 ◽
Vol 09
(PR8)
◽
pp. Pr8-395-Pr8-402
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1999 ◽
Vol 09
(PR8)
◽
pp. Pr8-373-Pr8-380
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2001 ◽
Vol 11
(PR3)
◽
pp. Pr3-189-Pr3-196
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