Thin film adhesion measurement by nanoindentation: Review of methodologies and validation by means of finite element simulations

Author(s):  
Jan Albrecht ◽  
Marie Weissbach ◽  
Juergen Auersperg ◽  
Rainer Dudek ◽  
Eberhard Kaulfersch ◽  
...  
Author(s):  
David A. Dillard ◽  
Caleb Scott ◽  
Kris Mount ◽  
Dingying Xu ◽  
Kai-Tak Wan ◽  
...  

A probe test is proposed to quantify the adhesion of thin films and coatings. Using a micromanipulator, a tungsten probe is advanced into the edge of a polymeric coating. Debonds initiate at the loading point and propagate into semicircular cracks at the interface as the probe slides under the coating. The size of the debond is related to the interfacial fracture energy; poorer adhesion results in larger debonds for a given probe displacement. Approximate closed-form and finite element analyses of the geometry have been conducted, along with a significant number of experiments on as-produced and environmentally-conditioned specimens. The technique is showing considerable promise for characterizing coating adhesion, and has certain advantages over existing techniques for certain application.


2006 ◽  
Vol 88 (19) ◽  
pp. 191911 ◽  
Author(s):  
V. Kireev ◽  
Y. Liu ◽  
Y. Braiman ◽  
B. Radhakrishnan ◽  
C. H. Hsueh ◽  
...  

2004 ◽  
Vol 4 (2) ◽  
pp. 163-168 ◽  
Author(s):  
M.J. Cordill ◽  
D.F. Bahr ◽  
N.R. Moody ◽  
W.W. Gerberich

1997 ◽  
Vol 12 (10) ◽  
pp. 2673-2685 ◽  
Author(s):  
Maarten P. de Boer ◽  
Michael Kriese ◽  
William W. Gerberich

We have investigated mechanical probing of a precracked fine line structure as a new type of thin film fracture mechanics specimen. An idealized mechanics analysis is first presented. Experimentally, two types of precracks are formed. A thin carbon layer to which other layers weakly adhere creates a “processed precrack” by integrated circuit processing techniques. An “indented processed precrack” is formed by precision alignment of a sharp microwedge. The processed precrack is found to reduce the critical tangential load by 50% from a non-precracked line, while the indented processed precrack lowers the load by 200%. From this, a reasonable value of adhesion may be directly calculated. Crack path behavior is observed to depend on strength of the interface. In the case of a weak interface, the crack remains in the interface as it extends. For a strong interface, it kinks into the substrate if the crack is initially short, but remains in the interface if it is initially long. Given the experimental evidence, the mechanics are slightly modified to quantitatively model the experimental data.


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