Direct Observation of PFPE Lubricants on Magnetic Disks

2009 ◽  
Vol 45 (2) ◽  
pp. 862-866 ◽  
Author(s):  
H. Tani ◽  
N. Tagawa
2003 ◽  
Vol 39 (5) ◽  
pp. 2744-2746 ◽  
Author(s):  
Xiaobin Zhu ◽  
V. Metlushko ◽  
B. Ilic ◽  
P. Grutter

Author(s):  
Yinbo He ◽  
Yasunaga Mitsuya ◽  
Hedong Zhang ◽  
Kenji Fukuzawa

This paper deals with the measurement of friction force exerted on molecularly thin lubricant film surfaces using a specially arranged pin-on-disk type friction tester. The measurements were carried out by sliding a 1.5-mm-diameter glass ball slider on a rotating disk surface with small loading force. Polar and non-polar PFPE lubricants were dip-coated on magnetic disks covered with diamond-like-carbon (DLC) film. Lubricant film thickness was varied to constitute multiple layered film structures on the DLC surface. To clarify the stratified effect of thin lubricant film on friction, a lightly loading force and a slow rotational speed were selected. The tested results showed that the friction force on non-polar lubricant surfaces increase slightly for mono-layer and multi-layer cases, while the friction force on polar lubricants show steady and gradual increase with increasing loading force. We conclude that friction force at small loading force is dependent intimately on the thickness, molecular weight and end-group functionality.


2020 ◽  
Vol 2020 (0) ◽  
pp. S16101
Author(s):  
Hiroshi TANI ◽  
Tsuyoshi SHIMIZU ◽  
Ryosuke SAGATA ◽  
Renguo LU ◽  
Shinji KOGANEZAWA ◽  
...  

2007 ◽  
Vol 27 (1) ◽  
pp. 1-11 ◽  
Author(s):  
Y. He ◽  
Y. Fujikawa ◽  
H. Zhang ◽  
K. Fukuzawa ◽  
Y. Mitsuya

Author(s):  
R. W. Anderson ◽  
D. L. Senecal

A problem was presented to observe the packing densities of deposits of sub-micron corrosion product particles. The deposits were 5-100 mils thick and had formed on the inside surfaces of 3/8 inch diameter Zircaloy-2 heat exchanger tubes. The particles were iron oxides deposited from flowing water and consequently were only weakly bonded. Particular care was required during handling to preserve the original formations of the deposits. The specimen preparation method described below allowed direct observation of cross sections of the deposit layers by transmission electron microscopy.The specimens were short sections of the tubes (about 3 inches long) that were carefully cut from the systems. The insides of the tube sections were first coated with a thin layer of a fluid epoxy resin by dipping. This coating served to impregnate the deposit layer as well as to protect the layer if subsequent handling were required.


Author(s):  
John M. Wehrung ◽  
Richard J. Harniman

Water tables in aquifer regions of the southwest United States are dropping off at a rate which is greater than can be replaced by natural means. It is estimated that by 1985 wells will run dry in this region unless adequate artificial recharging can be accomplished. Recharging with surface water is limited by the plugging of permeable rock formations underground by clay particles and organic debris.A controlled study was initiated in which sand grains were used as the rock formation and water with known clay concentrations as the recharge media. The plugging mechanism was investigated by direct observation in the SEM of frozen hydrated sand samples from selected depths.


Author(s):  
N. E. Paton ◽  
D. de Fontaine ◽  
J. C. Williams

The electron microscope has been used to study the diffusionless β → β + ω transformation occurring in certain titanium alloys at low temperatures. Evidence for such a transformation was obtained by Cometto et al by means of x-ray diffraction and resistivity measurements on a Ti-Nb alloy. The present work shows that this type of transformation can occur in several Ti alloys of suitable composition, and some of the details of the transformation are elucidated by means of direct observation in the electron microscope.Thin foils were examined in a Philips EM-300 electron microscope equipped with a uniaxial tilt, liquid nitrogen cooled, cold stage and a high resolution dark field device. Selected area electron diffraction was used to identify the phases present and the ω-phase was imaged in dark field by using a (101)ω reflection. Alloys were water quenched from 950°C, thinned, and mounted between copper grids to minimize temperature gradients in the foil.


Author(s):  
J.L. Williams ◽  
K. Heathcote ◽  
E.J. Greer

High Voltage Electron Microscope already offers exciting experimental possibilities to Biologists and Materials Scientists because the increased specimen thickness allows direct observation of three dimensional structure and dynamic experiments on effectively bulk specimens. This microscope is designed to give maximum accessibility and space in the specimen region for the special stages which are required. At the same time it provides an ease of operation similar to a conventional instrument.


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