Iron Oxide Nanoparticles Prepared by Modified Co-Precipitation Method

2014 ◽  
Vol 50 (1) ◽  
pp. 1-4 ◽  
Author(s):  
Saira Riaz ◽  
Mahwish Bashir ◽  
Shahzad Naseem
2013 ◽  
Vol 756 ◽  
pp. 74-79 ◽  
Author(s):  
Bashiru Kayode Sodipo ◽  
Azlan Abdul Aziz

Superparamagnetic iron oxide nanoparticles (SPION) of sizes 5 to10 nm were synthesized by the co-precipitation method. They are coated with silica nanoparticles using sonication method. The SPION was produced under the optimum pH of 10, peptized in acidic medium and redispersed in water. The silica nanoparticles were produced through the Stöbermethod. Sonochemical coating of silica nanoparticle on the SPION was successfulat a pH value lower than 5. Otherwise, at higher pH value (but lower than point zero charge (PZC)), the SPION were found to be unstable. Fast hydrolysis of triethoxyvinylsilane(TEVS) shows that silica forms its own particles without coating onto the surfaces of the SPION. Under optimized experimental condition, sonochemical method of coating silica nanoparticles onto the SPION can be considered as an alternative for effective and prompt method that rely mainly on pH of the suspension.


2017 ◽  
Vol 41 (5) ◽  
pp. 2055-2061 ◽  
Author(s):  
Tokeer Ahmad ◽  
Ruby Phul ◽  
Nafeesa Khatoon ◽  
Meryam Sardar

Iron oxide nanoparticles (IONPs) were preparedviaa co-precipitation method and were then characterized and evaluated for their antibacterial activity after modification withOcimum sanctumleaf extract.


2015 ◽  
Vol 15 (5) ◽  
pp. 3870-3878 ◽  
Author(s):  
S. Vikram ◽  
M. Dhakshnamoorthy ◽  
R. Vasanthakumari ◽  
A. R. Rajamani ◽  
Murali Rangarajan ◽  
...  

2017 ◽  
Vol 105 (2) ◽  
Author(s):  
Gehan E. Sharaf El-Deen ◽  
Neama G. Imam ◽  
Refaat R. Ayoub

AbstractSuperparamagnetic iron oxide nanoparticles (IO-MNPs) coated with natural polymers, starch (IO-S MNPs) and dextrin (IO-D MNPs), were synthesized by modified co-precipitation method. IO and hybrid-IO-MNPs were characterized by XRD, SEM, HRTEM, FT-IR spectroscopy, vibrating sample magnetometer (VSM) and zeta potential (ZP). IO-S MNPs and IO-D MNPs have IO core-shell structure with core of 10.8 nm and 13.8 nm and shell of 7.5 nm and 5.9 nm, respectively. The efficiency of the hybrid IO-MNPs for sorption of


RSC Advances ◽  
2015 ◽  
Vol 5 (24) ◽  
pp. 18420-18428 ◽  
Author(s):  
A. B. Salunkhe ◽  
V. M. Khot ◽  
J. M. Ruso ◽  
S. I. Patil

Superparamagnetic iron oxide nanoparticles are synthesized through the co precipitation method by using the new generation base diisopropylamine (DIPA) which electrostatically complexes with the iron ions, reduces them and subsequently caps the nanoparticles.


Author(s):  
Sema Salgın ◽  
Uğur Salgın ◽  
Nagihan Soyer

: In this study, magnetic iron oxide nanoparticles were synthesized by cost effective and an easy co-precipitation method. The effects of reaction parameters such as the mole ratio of Fe2+/Fe3+ (1/1, 1/2 and 1/3) and the base type (NaOH and NH4OH) on the average hydrodynamic diameter, zeta potential, chemical and morphological structure and saturation magnetization values of magnetic iron oxide nanoparticles were systematically investigated. Magnetic iron oxide nanoparticles synthesized at the mole ratio of 1/2 using NH4OH base gave better results in terms of particle size and particle shape, magnetization value. In order to prevent the formation of different phases in the co-precipitation method, an alternative approach was developed and the reaction was performed using inert supercritical CO2 atmosphere.


2008 ◽  
Vol 47-50 ◽  
pp. 1076-1079
Author(s):  
M.A. Do ◽  
H.J. Lee ◽  
J.H. Yeum ◽  
Y.M. Chang ◽  
H.D. Ghim ◽  
...  

Ultrasmall superparamagnetic iron oxide nanoparticles (USPION) as magnetic resonance imaging were synthesized through a sonochemical co-precipitation method with poly (ethyleneimine) (PEI). The size of the USPION was controlled by poly (ethyleneimine) (PEI) contents, ultrasonic exposure time, and Na4OH concentration. The characteristics of PEI-USPION were studied by X-ray diffractometry, magnetic property measurement system, scanning electron microscopy, transmission electron microscopy, and particle size analysis. The PEI-USPION had an average size of 5~10nm with a narrow size distribution, a perfect magnetite crystal structure, and high saturation magnetization.


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