Moist vs over‐dried etched dentin: FE‐SEM/TEM and bond strength evaluation of resin‐dentin interfaces produced by universal adhesives

To evaluate the bond strength of different universal adhesives on deciduous tooth dentineand their relationship with the composition and potential of hydrogen (pH). Methods: An in vitromicro push-out test on 150 samples (n = 50) per group per adhesive, namely, Adhese Universal(ADH; Ivoclar Vivadent), Futurabond U (FUT; Voco GmbH) (Test), and Scotchbond Universal withpre-conditioning (SCO; 3M) (Control), to record bond strength (BS) and type of adhesive failure.Results: The results of the different adhesives (megapascals (MPa)) varied, showing no statisticalsignificance. The corresponding averages are in MPa: ADH, 13.66 2.81; FUT, 14.48 2.88; SCO,14.98 3.96. Additionally, the frequency of type of failure was as follows: mixed (60.7%), adhesive(27.3%), and cohesive (12%). Conclusions: SCO, with a pH of 2.7, showed greater resistance tofracture, while FUT, with a pH of 2.3 and no pre-conditioning, approached the same values, being aone-step adhesive. No relationship was found between failure and type of adhesive.

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Effects of adhesive application time and air blowing pressure on dentin bond strength of self-etch mode universal adhesives

Journal of Adhesion Science and Technology ◽

10.1080/01694243.2021.1917905 ◽

2021 ◽

pp. 1-15

Author(s):

Buket Karalar ◽

Yusuf Ziya Bayındır

Keyword(s):

Bond Strength ◽

Application Time ◽

Air Blowing ◽

Universal Adhesives ◽

Adhesive Application ◽

Self Etch

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Effect of air-blowing time and long-term storage on bond strength of universal adhesives to dentin

Clinical Oral Investigations ◽

10.1007/s00784-018-2656-y ◽

2018 ◽

Vol 23 (6) ◽

pp. 2629-2635 ◽

Cited By ~ 1

Author(s):

Pipop Saikaew ◽

Jiale Fu ◽

A. F. M. Almas Chowdhury ◽

Ricardo M. Carvalho ◽

Hidehiko Sano

Keyword(s):

Bond Strength ◽

Long Term Storage ◽

Air Blowing ◽

Universal Adhesives ◽

Term Storage

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Microshear bond strength of universal adhesives for use with artificially demineralized enamel, with and without pre-etching

Journal of Adhesion Science and Technology ◽

10.1080/01694243.2018.1482812 ◽

2018 ◽

Vol 33 (4) ◽

pp. 346-354

Author(s):

Sezer Demirbuğa ◽

Nazire Nurdan Çakır ◽

Aysun Tuğçe Akay

Keyword(s):

Bond Strength ◽

Demineralized Enamel ◽

Universal Adhesives ◽

Microshear Bond Strength

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Bond strength of three different universal adhesives after different thermal cycling protocols

Journal of Adhesion Science and Technology ◽

10.1080/01694243.2018.1514962 ◽

2018 ◽

Vol 32 (24) ◽

pp. 2741-2752

Author(s):

Fatma Dilsad Oz ◽

Zeynep Bilge Kutuk ◽

Ece Balkan ◽

Canan Ozturk ◽

Sevil Gurgan

Keyword(s):

Bond Strength ◽

Thermal Cycling ◽

Universal Adhesives

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Effect of Different Protocols in Preconditioning With EDTA in Sclerotic Dentin and Enamel Before Universal Adhesives Applied in Self-etch Mode

Operative Dentistry ◽

10.2341/16-014-l ◽

2017 ◽

Vol 42 (3) ◽

pp. 284-296 ◽

Cited By ~ 3

Author(s):

EC Martini ◽

SO Parreiras ◽

MF Gutierrez ◽

AD Loguercio ◽

A Reis

Keyword(s):

Bond Strength ◽

Adhesive Systems ◽

Microtensile Bond Strength ◽

Universal Adhesive ◽

Etching Pattern ◽

Bonding Performance ◽

Universal Adhesives ◽

Microshear Bond Strength ◽

Self Etch ◽

Main Factor

SUMMARY Objectives: The aim of this study was to investigate the effect of different protocols of 17% ethylene diamine tetra-acetic acid (EDTA) conditioning on the etching pattern and immediate bond strength of universal adhesives to enamel and sclerotic dentin. Methods and Materials: Forty bovine teeth with sclerotic dentin and 20 human third molars were randomly divided into eight groups resulting from the combination of the main factors surface treatment (none, two-minute EDTA conditioning manual application, 30-second EDTA manual application, 30-second EDTA sonic application) and adhesives systems (Scotchbond Universal Adhesive [SBU] and Prime & Bond Elect [PBE]). Resin-dentin and enamel-dentin bond specimens were prepared and tested under the microtensile bond strength (μTBS) and microshear bond strength (μSBS) tests, respectively. The etching pattern produced on the unground enamel and the sclerotic dentin surfaces under the different protocols and adhesive systems was evaluated under scanning electron microscopy. Results: For enamel, only the main factor adhesive was significant (p<0.0001), with SBU showing the highest μSBS. In sclerotic dentin, the lowest mean was observed for the group without EDTA application and the highest mean in the group with EDTA application with the sonic device for 30 seconds. Regardless of the EDTA protocol, the highest means of μTBS were observed for SBU (p<0.05). Conclusions: EDTA conditioning improves the bonding performance of universal adhesives in the self-etch mode on sclerotic dentin, mainly when applied for 30 seconds with the aid of a sonic device. EDTA pretreatment also improves the retentive etching pattern of enamel, but it does not result in higher enamel bond strength.

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MICRO SHEAR BOND STRENGTH EVALUATION FOR IMMEDIATELY SEALED DENTINE WITH HYBRID CERAMICS AFTER DIFFERENT PROVISIONALIZATION PERIODS: IN VITRO STUDY

Egyptian Dental Journal ◽

10.21608/edj.2017.76223 ◽

2017 ◽

Vol 63 (4) ◽

pp. 2651-2659

Author(s):

Maha Taymour ◽

Reham Elbasty

Keyword(s):

Bond Strength ◽

Shear Bond Strength ◽

In Vitro Study ◽

Vitro Study ◽

Strength Evaluation

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Effects of Multipurpose, Universal Adhesives on Resin Bonding to Zirconia Ceramic

Operative Dentistry ◽

10.2341/13-303-l ◽

2015 ◽

Vol 40 (1) ◽

pp. 55-62 ◽

Cited By ~ 37

Author(s):

J-H Kim ◽

S-Y Chae ◽

Y Lee ◽

G-J Han ◽

B-H Cho

Keyword(s):

Bond Strength ◽

Artificial Aging ◽

Resin Cement ◽

Zirconia Ceramic ◽

Single Bond ◽

Surface Conditioning ◽

Universal Adhesives ◽

Bond Strengths ◽

Microshear Bond Strength ◽

Composite Cylinders

SUMMARY This study evaluated the effects of single-bottle, multipurpose, universal adhesives on the bond strength of resin cement to zirconia ceramic. Polished zirconia ceramic (Cercon base) discs were randomly divided into four groups (n=40) according to the applied surface-conditioning agent: Single Bond 2, Single Bond Universal, All-Bond Universal, and Alloy Primer. Cured composite cylinders (Ø 0.8 mm × 1 mm) were cemented to the conditioned zirconia specimens with resin cement (RelyX ARC). The bonded specimens were subjected to a microshear bond-strength test after 24 hours of water storage and after 10,000 cycles of thermocycling. The surface-conditioning agent significantly influenced the bond strength (p<0.05). Single Bond Universal showed the highest initial bond strength (37.7 ± 5.1 MPa), followed by All-Bond Universal (31.3 ± 5.6 MPa), Alloy Primer (26.9 ± 5.1 MPa), and Single Bond 2 (8.5 ± 4.6 MPa). Artificial aging significantly reduced the bond strengths of all the test groups (p<0.05). After 10,000 cycles of thermocycling, All-Bond Universal showed the highest bond-strength value (26.9 ± 6.4 MPa). Regardless of artificial aging, Single Bond Universal and All-Bond Universal showed significantly higher bond strengths than Alloy Primer, a conventional metal primer.

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