Effect of pressure on the phase transformations and mechanical properties of 10 mol% Mg-PSZ sintered by HPHT

MgO (10 mol%)-stabilized zirconia ceramics were obtained using high-pressure high-temperature (HPHT) sintering. The effects of the sintering pressure (2.5, 3.7, and 5.0 GPa) on the phase transformations and hardness were...

Effects of Different Air Particle Abrasion Protocols on the Biaxial Flexural Strength and Fractography of High/Ultra-Translucent Zirconia

In this study, the biaxial flexural strength (BFS) and fractography of high/ultra-translucent monolithic zirconia ceramics subjected to different mechanical surface pretreatments were evaluated. A total of 108 disc-shaped samples (12 mm diameter, 1.2 mm thickness) of three zirconia materials (5Y-ZP KATANA Zirconia UTML (ML), 3Y-TZP DD Bio ZX2 (DB), and 5Y-ZP DD cube X2 (DC)) were used. The BFS was investigated after subjecting the samples to surface treatment using air abrasion particles of two types (aluminum oxide or glass microbeads). The data were analyzed using two-way analysis of variance, followed by Scheffe’s post hoc test for multiple comparisons. The mean ± standard deviation BFS for DB was highest after treatment with 50 µm Al2O3 (1626.05 ± 31.9 MPa), with lower values being observed following treatment with 50 µm glass microbeads (1399.53 ± 24.2 MPa) and in the control sample (1198.51 ± 21.1 MPa). The mean ± standard deviation (SD) BFSs for DC and ML were the highest in the control groups. Surface air abrasion with 50 µm Al2O3 particles and 2 bar pressure is recommended for 3Y-TZP translucent zirconia, while no abrasion of 5Y-ZP translucent zirconia ceramic.

Analytical and Experimental Investigation on Cutting Force in Longitudinal-Torsional Coupled Rotary Ultrasonic Machining Zirconia Ceramics

Ceramics and other hard-and-brittle materials are very effectively processed by longitudinal-torsional coupled rotary ultrasonic machining (LTC-RUM). However, the cutting force evolution and the effects of processing parameters on the material removal mechanism in LTC-RUM need to be clarified for machining optimization. This paper proposes a cutting force model of the LTC-RUM of zirconia ceramics via the brittle material removal mechanism. Firstly, the kinematic analysis of a single abrasive grain was performed, with further consideration of the material removal volume, the effective contact time, and the impact force per one ultrasonic vibration cycle. Then, the longitudinal-torsional coupled vibration of the core tool was analyzed from the standpoint of wave energy conversion. The analytical model was finalized and experimentally verified by LTC-RUM tests. The cutting force curves predicted via the proposed model were in good agreement with the experimental results. The results obtained are considered instrumental in predicting the effects of processing parameters on cutting force during LTC-RUM of ceramics and their further optimization.

Optimization of Machining Parameters for Milling Zirconia Ceramics by Polycrystalline Diamond Tool

Zirconia ceramics are widely used in many fields because of their excellent physical and mechanical properties. However, there are some challenges to machine zirconia ceramics with high processing efficiency. In order to optimize parameters for milling zirconia ceramics by polycrystalline diamond tool, finite element method was used to simulate machining process based on Johnson-Cook constitutive model. The effects of spindle speed, feed rate, radial and axial cutting depth on cutting force, tool flank wear and material removal rate were investigated. The results of the simulation experiment were analyzed and optimized by the response surface method. The optimal parameter combination was obtained when the spindle speed, feed rate, radial and axial cutting depth were 8000 r/min, 90.65 mm/min, 0.10 mm and 1.37 mm, respectively. Under these conditions, the cutting force was 234.81 N, the tool flank wear was 33.40 μm when the milling length was 60 mm and the material removal rate was 44.65 mm3/min.

Investigation on the Effect of Dynamic Fracture Toughness to Zirconia Ceramic Grinding Performance with Different Grain Sizes

To reveal the material removal mechanism of zirconia ceramics, an improved prediction models of the critical grinding force and maximum subsurface damage depth models are developed based on the dynamic fracture toughness. The effects of three different grain sizes on the material removal mechanism during brittle- ductile transition process of zirconia ceramics is analyzed through grinding experiments. And the influence of grain size on grinding force, workpiece surface roughness, surface fragmentation rate and subsurface damage depth in grinding are discussed. The results of the experiment results indicated that the value of dynamic fracture toughness tends to decrease with an increase in equivalent grinding thickness, and the ductile removal range of zirconia ceramics expands for the reason that the critical grinding force considering dynamic fracture toughness is higher than the static grinding force considering static fracture toughness, and the maximum subsurface damage depth is closer to actual maximum subsurface damage depth. Besides the smaller the grain size of zirconia ceramics, the higher the surface quality of grinding.

The Influence of Specimen Geometry and Loading Conditions on the Mechanical Properties of Porous Brittle Media

Dynamic tests of fine-grained fired dioxide-zirconia ceramics under compression under uniaxial stress conditions were carried out. The influence of the specimen length on the obtained strength and deformation properties of ceramics is investigated. The thickness of the specimen has a significant impact on the course of the obtained dynamic stress–strain diagrams: short specimens have a much more sloping area of active loading branch. The main contribution to the modulus of the load branch resulting from tests of brittle porous media is made by the geometry of the specimens and the porosity of the material. When choosing the length of specimens for dynamic tests, the optimal geometry of the tested specimens is preferable in accordance with the Davies–Hunter criterion, when the contributions of axial and radial inertia are mutually compensated, and the contribution of the effects of friction in the resulting diagram is minimal. When choosing the geometry of specimens of brittle porous media, the structure of the material should be taken into account so that the size of the specimen (both length and diameter) exceeds the size of the internal fractions of the material by at least five times.