Stress Induced Martensitic Transformation in Shape Memory Alloys Studied by In-Situ Neutron Diffraction Techniques

2000 ◽  
Author(s):  
P. Šittner ◽  
V. Novák ◽  
P. Lukáš ◽  
D. Neov

Abstract Shape memory alloy (SMA) elements are being embedded in smart materials and hybrid composites as actuating and/or sensing elements responding to the stress and temperature stimuli. In order to design smart composites, in-situ experimental information about evolution of internal stresses and phase fractions in the embedded SMA elements and internal stresses in neighboring matrix during actuation cycles would be of interest. Such experimental data have to be obtained nondestructively from the microscopic particles or fibres deep in the bulk specimens exposed to stress and/or thermal variations. In-situ neutron diffraction experimental techniques fulfill in principle these requirements. However, reliable evaluation of internal stresses from neutron diffraction experiments in the smart SMA composites can be made only after the lattice plane responses of monolithic SMAs in thermomechanical cyclic loads are fully understood. In this paper, the results of the in-situ investigations of stress induced martensitic transformation (SIMT) in tensile tests carried out on monolithic CuAlZnMn SMA polycrystal are reported, and the observed lattice plane responses are interpreted using a selfconsistent model of SMA polycrystal.

2005 ◽  
Vol 502 ◽  
pp. 339-344 ◽  
Author(s):  
Jozef Zrník ◽  
O. Muránsky ◽  
Petr Lukáš ◽  
Petr Šittner ◽  
Z. Nový

The precise characterization of the multiphase microstructure of low alloyed TRIP steels is of great importance for the interpretation and optimisation of their mechanical properties. In-situ neutron diffraction experiment was employed for monitoring of conditioned austenite transformation to ferrite, and also for retained austenite stability evaluation during subsequent mechanical loading. The progress in austenite decomposition to ferrite is monitored at different transformation temperatures. The relevant information on the course of transformation is extracted from neutron diffraction spectra. The integrated intensities of austenite and ferrite neutron diffraction profiles over the time of transformation are then assumed as a measure of the volume fractions of both phases in dependence on transformation temperature. Useful information was also obtained on retained austenite stability in TRIP steel during mechanical testing. The in-situ neutron diffraction experiments were conducted at two different diffractometers to assess the reliability of neutron diffraction technique in monitoring the transformation of retained austenite during room temperature tensile test. In both experiments the neutron investigation was focused on the volume fraction quantification of retained austenite as well as on internal stresses rising in structure phases due to retained austenite transformation.


2011 ◽  
Vol 681 ◽  
pp. 31-36
Author(s):  
Marc Seefeldt ◽  
Steven Dillien ◽  
Uwe Stuhr

The load transfer among ferrite orientations and between ferrite and martensite was analysed in DP 600 steel by means of neutron diffraction duringin situtensile tests on the multiple pulse overlap time-of-flight strain scanner POLDI. The material had 0.07 wt% C and a martensite volume fraction of 15%.In situtests were done in “Young” as well as in “Poisson setup”. The martensite phase could not be probed due to its low tetragonality. The curves of the lattice plane strains as a function of the externally applied macroscopic stress reveal (1) plastic relaxations of transformation and intergranular stresses in the compliant <100> oriented grains, and (2) a second inflection point in the fully plastic part indicating the onset of plastic deformation of the hard phase.


2002 ◽  
Vol 74 (0) ◽  
pp. s1121-s1123 ◽  
Author(s):  
P. Luk�? ◽  
P. ?ittner ◽  
D. Lugovoy ◽  
D. Neov ◽  
M. Ceretti

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