Application of the Master Curve Approach for Abnormal Material Conditions

Author(s):  
Tapio Planman ◽  
William Server ◽  
Kim Wallin ◽  
Stan Rosinski

The range of applicability of Master Curve testing Standard ASTM E 1921 is limited to macroscopically homogeneous steels with “uniform tensile and toughness properties”. A majority of structural steels appear to satisfy this requirement by exhibiting fracture toughness data which comply with the assumed KJc vs. temperature dependence and scatter within the specified validity area. As indicated in ASTM E 1921 a criterion for material macroscopic inhomogeneity is often applied using the 2% lower bound (possibly also the 98% upper bound). Data falling below this 2% lower-limit curve may be an indication of material inhomogeneity or susceptibility to grain boundary fracture. When this situation occurs, it is recommended to analyze the material with the so-called SINTAP procedure, which is intended for randomly inhomogeneous materials to assure a conservative lower-bound estimate. When a data set distinctly consists of two or more different data populations instead of one (due to variation of irradiation dose or specimen extraction depth, for instance) adoption of a bimodal (or a multimodal) Master Curve model is generally appropriate. These modal models provide information if the deviation of distributions is statistically significant or if different distributions truly exist for values of reference transition temperature, T0, characteristic of separate data populations. In the case of data sets representing thick-walled structures (i.e., reactor pressure vessels), indications of abnormal fracture toughness data can be encountered such that material inhomogeneity or fracture modes other than pure cleavage should be suspected. A state-of-the-art review for extended, non-standard Master Curve data and techniques highlights limits of applicability in situations where the basic ASTM E 1921 procedure is not appropriate for material homogeneity or different fracture modes.

2019 ◽  
Vol 141 (6) ◽  
Author(s):  
Jong-Min Kim ◽  
Seok-Min Hong ◽  
Min-Chul Kim ◽  
Bong-Sang Lee

Abstract The standard master curve (MC) approach has a major limitation in that it is only applicable to homogeneous datasets. In nature, steels are macroscopically inhomogeneous. Reactor pressure vessel (RPV) steel has different fracture toughness with varying distance from the inner surface of the wall due to the higher cooling rate at the surface (deterministic material inhomogeneity). On the other hand, the T0 value itself behaves like a random parameter when the datasets have large scatter because the datasets are for several different materials (random inhomogeneity). In this paper, four regions, the surface, 1/8 T, 1/4 T, and 1/2 T, were considered for fracture toughness specimens of Korean Standard Nuclear Plant (KSNP) SA508 Gr. 3 steel to provide information on deterministic material inhomogeneity and random inhomogeneity effects. Fracture toughness tests were carried out for the four regions at three test temperatures in the transition region and the microstructure of each region was analyzed. The amount of upper bainite increased toward the center, which has a lower cooling rate; therefore, the center has lower fracture toughness than the surface so reference temperature (T0) is higher. The fracture toughness was evaluated using the bimodal master curve (BMC) approach. The results of the BMC analyses were compared with those obtained via a conventional master curve analyses. The results indicate that the bimodal master approach considering inhomogeneous materials provides a better description of scatter in the fracture toughness data than a conventional master curve analysis does.


Author(s):  
Kim Wallin

The standard Master Curve (MC) deals only with materials assumed to be homogeneous, but MC analysis methods for inhomogeneous materials have also been developed. Especially the bi-modal and multi-modal analysis methods are becoming more and more standard. Their drawback is that these methods are generally reliable only with sufficiently large data sets (number of valid tests, r ≥ 15–20). Here, the possibility of using the multi-modal analysis method with smaller data sets is assessed, and a new procedure to conservatively account for possible inhomogeneities is proposed.


Author(s):  
Volodymyr M. Revka ◽  
Liudmyla I. Chyrko

An important issue in the safety operation of WWER-1000 type reactor is a decrease in fracture toughness for reactor pressure vessel steels due to neutron irradiation. This effect for RPV metal is known as radiation embrittlement. The radiation induced temperature shift of the fracture toughness transition curve is considered as a measure of the embrittlement rate. The Charpy impact and fracture toughness specimens are included in the surveillance program for an assessment of changes in fracture toughness of RPV materials. The present analysis is based on a large data set which includes mostly experimental results for pre-cracked Charpy specimens from a WWER-1000 RPV surveillance program. A Master curve approach is applied to analyze the surveillance test data with respect to a shape of the fracture toughness transition curve and a scatter of KJC values. The RPV base and weld metal in unirradiated, thermally aged and irradiated conditions are considered in this study. The maximum shift in a reference temperature T0 due to irradiation is 107 degree Celsius. It is shown that the Master curve, 5 % and 95 % tolerance bounds describe adequately the temperature dependence and the statistical scatter of KJC values for WWER-1000 RPV steels both in unirradiated condition and after irradiation up to design as well as long term operation neutron fluence. Furthermore, a development of the Weibull plots for considered data sets is shown that the Weibull slope is close to the expected one of 4 on average. Finally, a comparison of the reference temperature T0 and a scatter of KJC values derived from the pre-cracked Charpy and 0,5T C(T) specimens of base and weld metal in unirradiated condition is done. The analysis has shown a significant discrepancy between the T0 values derived from the two different types of specimens for both RPV metals.


Author(s):  
Udo Rindelhardt ◽  
Hans-Werner Viehrig ◽  
Joerg Konheiser ◽  
Jan Schuhknecht

Between 1973 and 1990 4 units of the Russian NPP type WWER-440/230 were operated in Greifswald (former GDR). The operation was stopped after the German reunification, because the units did not completely follow western nuclear safety standards. Material probes from the pressure vessels were gained in the frame of the ongoing decommissioning procedure. The investigations of this material started with material from the circumferential core weld of unit 1. This weld was annealed after 13 cycles and operated further for 2 cycles. Additionally, starting with cycle 11, dummy assemblies were inserted to reduce the neutron fluence in the RPV wall. Firstly this paper presents results of the RPV fluence calculations depending on different loading schemes and on the axial weld position based on the Monte Carlo code TRAMO. The results show, that the use of the dummy assemblies reduces the flux by a factor of 2 – 5 depending on the azimuthal position. The fluence increase is reduced to 1/6 at the position of the maximum fluence. The neutron fluence at the different circumferential welds is closely related to their distance to the core. The circumferential core weld (SN0.1.4) received a fluence of 2.4·1019 neutrons/cm2 at the inner surface, it decreases to 0.8·1019 neutrons/cm2 at the outer surface. The neutron fluences at the both other welds are 2 resp. 4 orders of magnitude smaller according to their distances to the core. It should be mentioned that in this cases the fluence gradient can be negative through the wall. The material investigations were done using a trepan from the circumferential core weld. Master Curve and Charpy V-notch testing were applied. Specimens from 7 locations through the thickness of the welding seam were tested. The reference temperature T0 was calculated with the measured fracture toughness values, KJc, at brittle failure of the specimen. Generally the KJc values measured on pre-cracked and side-grooved Charpy size SE(B) specimens of the investigated weld metal follows the course of the Master Curve. The KJc values show a remarkable scatter. In addition the MC SINTAP procedure was applied to determine T0SINTAP of the brittle fraction of the data set. There are remarkable differences between T0 and T0SINTAP indicating macroscopic inhomogeneous weld metal. The highest T0 was about 50°C at a distance of 22 mm from the inner surface of the weld. It is 40 K higher compared with T0 at the inner surface. This is important for the assessment of ductile-to-brittle temperatures measured with sub size Charpy specimens made of weld metal from the inner RPV wall. This material does not represent the most conservative condition. Nevertheless, the Charpy transition temperature TT41J estimated with results of sub size specimens after the recovery annealing was confirmed by the testing of standard Charpy V-notch specimens. The VERLIFE procedure prepared for the integrity assessment of WWER RPV was applied on the measured results. It enables the determination of a reference temperature, RTT0 to index a lower bound fracture toughness curve. This curve agrees with the MC 5% fractile as specified in ASTM E1921-05. The measured KJc values are not enveloped by this lower bound curve. However, the VERLIFE lower bound curve indexed with the SINTAP reference temperature RTT0SINTAP envelops the KJc values. Therefore for a conservative integrity assessment the fracture toughness curve indexed with a RT representing the brittle fraction of a dataset of measured KJc values has to be applied.


2013 ◽  
Vol 135 (6) ◽  
Author(s):  
Naoki Miura ◽  
Naoki Soneda ◽  
Shu Sawai ◽  
Shinsuke Sakai

The Master Curve gives the relation between the median of fracture toughness of ferritic steels and the temperature in the ductile–brittle transition temperature region. The procedure used to determine the Master Curve is provided in the current American Society for Testing and Materials (ASTM) E1921 standard. By considering the substitution of the alternative lower-bound curves based on the Master Curve approach for the KIc curves based on reference data sets in the present codes such as ASME Code Cases N-629 and N-631, the statistical characteristic should be well incorporated in the determination of the lower-bound curves. Appendix X4 in the ASTM standard describes the procedure used to derive the lower-bound curves; however, it appears to be addressed without sufficient consideration of the statistical reliability. In this study, we propose a rational determination method of lower-bound fracture toughness curves using the Master Curve approach. The method considers the effect of sample size in the determination of the tolerance-bound curve. The adequacy of the proposed method was verified by comparing the tolerance-bound curve with the fracture toughness database for national reactor pressure vessel (RPV) steels including plate and forging obtained from 4 T to 0.4 T C(T) specimens and 0.4 T SE(B) specimens. The method allows the application of the Master Curve using fewer specimens, which can coexist with the present surveillance program.


Author(s):  
J. Brian Hall ◽  
Benjamin E. Mays ◽  
Matthew DeVan

The current approach in evaluating the Pressurized Water Reactor (PWR) inlet and outlet nozzle corner regions with respect to plant heat-up and cool-down pressure-temperature limit curves contains a number of conservatisms. These conservatisms include postulation of a large ¼ thickness flaw at the nozzle corner region and use of RTNDT (reference nil-ductility temperature) or an estimation of RTNDT. The paper herein discusses generic fracture toughness of nozzle forging material SA-508 Class 2 for use with postulated smaller surface flaws in developing pressure-temperature limit curves for nozzle corners for nuclear power plant operations. ASME Appendix G uses the lower bound KIC curve, which has inherent margin since RTNDT is a conservative method for locating the KIC curve. RTNDT is based on the drop weight test, which is a crack arrest transition temperature measurement, and the Charpy impact test, which is a blunt notch impact test. These data are conservatively bounded by the KIC curve, which is a lower bound crack initiation toughness curve. In contrast, the master curve method is based on an initiation transition temperature fracture toughness test technique per ASTM E1921. The master curve index temperature (T0) provides a more accurate measure of the material fracture toughness than KIC indexed with RTNDT. Since many of the nuclear pressure vessels were fabricated to ASME Code editions prior to 1972, RTNDT was not measured for the nozzles. In many cases, RTNDT has been estimated. Therefore, for this work, the fracture toughness was generically established based on conservative T0 measurements of 22 representative forgings with a margin of two standard deviations to ensure a conservative lower bound toughness using ASME Appendix G, G-2110. The properties of a forging are better near the surface due to the faster cooling rate during heat treatment. The difference in reactor pressure vessel fracture toughness was established for forgings near the surface at the postulated flaw location as allowed by ASME Section III, NB-2223.2 relative to the traditional ¼ thickness location. The near-surface forging toughness was conservatively determined through evaluation of 31 near-surface and approximate ¼ thickness location fracture toughness measurements.


Author(s):  
Jongmin Kim ◽  
Minchul Kim ◽  
Kwonjae Choi ◽  
Bongsang Lee

The standard master curve approach has the major limitation, which is only applicable to homogeneous datasets. In nature, steels are macroscopically inhomogeneous and thus the fracture toughness has larger scatters than expected by a conventional master curve approach. RPV steel has different fracture toughness with varying distance from the inner surface of the wall. Regarding this, a clear tendency was reported in that the toughness extracted near the surface had to be higher than in the center region due to the higher quenching rate at the surface (deterministic material inhomogeneity). On the other hand, the T0 value itself behaves like a random parameter when the datasets have a large scatter due to the datasets consisting of several different materials such as welding region (random inhomogeneity). In the present paper, four regions, the surface, 1/8T, 1/4T and 1/2T, were considered for fracture toughness specimens of KSNP (Korean Standard Nuclear Plant) SA508 Gr. 3 steel to provide deterministic material inhomogeneity and random inhomogeneity effect. Specimens were extracted from these four regions and fracture toughness tests were performed at various temperatures in the transition region. Several concepts were provided for the master curve of inhomogeneous materials such as a bimodal and random inhomogeneous master curve scheme, and among them, the bimodal master curve analyses were reviewed and compared with a conventional master curve approach to find the random inhomogeneity. The bimodal master curve considering inhomogeneous materials provides better description of scatter in fracture toughness data than conventional master curve analysis, but it is unclear to provide evidence that the bimodal analysis lines follow the data more closely than the conventional master curve analysis.


Author(s):  
Kim R. W. Wallin ◽  
Gerhard Nagel ◽  
Elisabeth Keim ◽  
Dieter Siegele

The ASME code cases N-629 and N-631 permits the use of a Master Curve-based index temperature (RTTo ≡ T0 + 19.4°C) as an alternative to traditional RTNDT-based methods of positioning the ASME KIc, and KIR curves. This approach was adopted to enable use of Master Curve technology without requiring the wholesale changes to the structure of the ASME Code that would be needed to use all aspects of Master Curve technology. For the brittle failure analysis considering irradiation embrittlement additionally a procedure to predict the adjustment of fracture toughness for EOL from irradiation surveillance results must be available as by NRC R.G. 1.99 Rev. 2 e.g.: ART = Initial RTNDT + ΔRTNDT + Margin. The conservatism of this procedure when RTNDT is replaced by RTTo is investigated for western nuclear grade pressure vessel steels and their welds. Based on a systematic evaluation of nearly 100 different irradiated material data sets, a simple relation between RTToirr, RTToref and ΔT41JRG is proposed. The relation makes use of the R.G. 1.99 Rev. 2 and enables the minimizing of margins, necessary for conventional correlations based on temperature shifts. As an example, the method is used to assess the RTTo as a function of fluence for several German pressure vessel steels and corresponding welds. It is shown that the method is robust and well suited for codification.


1998 ◽  
Vol 120 (1) ◽  
pp. 24-28 ◽  
Author(s):  
M. A. Sokolov

The American Society of Mechanical Engineers (ASME) KIc curve is a function of test temperature (T) normalized to a reference nil-ductility temperature, RTNDT, namely, T – RTNDT. It was constructed as the lower boundary to the available KIc database. Being a lower bound to the unique but limited database, the ASME KIc curve concept does not discuss probability matters. However, a continuing evolution of fracture mechanics advances has led to employment of the Weibull distribution function to model the scatter of fracture toughness values in the transition range. The Weibull statistic/master curve approach was applied to analyze the current ASME KIc database. It is shown that the Weibull distribution function models the scatter in KIc data from different materials very well, while the temperature dependence is described by the master curve. Probabilistic-based tolerance-bound curves are suggested to describe lower-bound KIc values.


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