Optical technique for the in situ study of orientation and structure changes accompanied the plastic deformation of polycrystalline specimens of aluminum

2011 ◽  
Vol 47 (15) ◽  
pp. 1663-1666 ◽  
Author(s):  
E. E. Badiyan ◽  
A. G. Tonkopryad ◽  
O. V. Shekhovtsov ◽  
R. V. Shurinov ◽  
T. R. Zetova
2011 ◽  
Vol 82 (9) ◽  
pp. 998-1003 ◽  
Author(s):  
Daria Borisova ◽  
Volker Klemm ◽  
Gerhard Schreiber ◽  
David Rafaja

2006 ◽  
Vol 509 ◽  
pp. 57-62 ◽  
Author(s):  
Nicole Clément ◽  
Mustafa Benyoucef ◽  
M. Legros ◽  
Pierre Caron ◽  
Armand Coujou

An in situ study of the plastic deformation of <001> single crystals of an industrial superalloy has been performed at 850 °C in a TEM to observe directly the micromechanisms which control the deformation under the actual temperature and stress conditions experienced by this material in aeroengines. A comparison between the creation and propagation modes of moving dislocations in the standard microstructure after annealing and the rafted microstructure after 20 h of creep at 1050°C evidence the important role of the width of the γ channels as well as the strength of the γ/γ’ interface in controlling the shearing events of γ’ channels.


Author(s):  
K. Fukushima ◽  
N. Kohyama ◽  
A. Fukami

A film-sealed high resolution environmental cell(E.C) for observing hydrated materials had been developed by us(l). Main specification of the E.C. is as follows: 1) Accelerated voltage; 100 kV. 2) Gas in the E.C.; saturated water vapour with carrier gas of 50 Torr. 3) Thickness of gas layer; 50 μm. 4) Sealing film; evaporated carbon film(20 nm thick) with plastic microgrid. 5) Resolving power; 1 nm. 6) Transmittance of electron beam; 60% at 100 kV. The E.C. had been successfully applied to the study of hydrated halloysite(2) (3). Kaolin minerals have no interlayer water and are basically non-expandable but form intercalation compounds with some specific chemicals such as hydrazine, formamide and etc. Because of these compounds being mostly changed in vacuum, we tried to reveal the structure changes between in wet air and in vacuum of kaolin minerals intercalated with hydrazine and of hydrated state of montmori1lonite using the E.C. developed by us.


2021 ◽  
Vol 27 (S1) ◽  
pp. 1554-1555
Author(s):  
Chen Gu ◽  
Nabil Bassim ◽  
Hatem Zurob

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