X-ray diffraction study of self-propagating high-temperature synthesis in the Zr–Al–C system

The steel substrate was coated by Fe-based composite using self-propagating high-temperature synthesis (SHS) reaction of reactant coating paste. The green paste was prepared by mixing precursor powders of Al, Fe2O3and Al2O3. It was coated on the steel substrate before igniting by oxy-acetylene flame. The effect of coating paste thickness and the additives on the resulted Fe-based composite coating was studied. The composite coating was characterized by X-ray diffraction (XRD) and scanning electron microscope (SEM) couple with dispersive X-ray (EDS).

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Self-Propagating High-Temperature Synthesis of Fe-W(B, C) Based Composite

Advanced Materials Research ◽

10.4028/www.scientific.net/amr.748.46 ◽

2013 ◽

Vol 748 ◽

pp. 46-50 ◽

Cited By ~ 3

Author(s):

Saowanee Singsarothai ◽

Sutham Niyomwas

Keyword(s):

Electron Microscope ◽

High Temperature ◽

Scanning Electron Microscope ◽

The Self ◽

X Ray Diffraction ◽

Temperature Synthesis ◽

X Ray ◽

High Temperature Synthesis ◽

Flame Ignition ◽

Scanning Electron

Fe-W based composite have successfully been prepared using natural resource. The ferberite (Fe (Mn, Sn)WO4) tailings mixed with aluminum, carbon and boron oxide powder were used as reactants. The reactants were pressed and followed by oxy-acetylene flame ignition. The products from the self-propagating high-temperature synthesis (SHS) reaction were characterized by X-ray diffraction (XRD) and scanning electron microscope (SEM) couple with dispersive X-ray (EDS).

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Microstructure and Wear Performance of Cu-Mo-Si Alloys Fabricated by Self-Propagation High-Temperature Synthesis

Materials Science Forum ◽

10.4028/www.scientific.net/msf.658.408 ◽

2010 ◽

Vol 658 ◽

pp. 408-411

Author(s):

Hui Xie ◽

Lei Jia ◽

Si Ming Wang ◽

Ji Ling Zhu ◽

Zhen Lin Lu

Keyword(s):

High Temperature ◽

Wear Behavior ◽

X Ray Diffraction ◽

Temperature Synthesis ◽

Wear Performance ◽

X Ray ◽

Cu Content ◽

High Temperature Synthesis ◽

Pin On Disc ◽

Worn Surface

Cu-Mo-Si alloys with different Cu contents were prepared by self-propagation high-temperature synthesis (SHS). The microstructure and the worn surface morphology were observed using scanning electron microscopy (SEM) together with energy dispersive X-ray spectroscopy (EDS) analysis. Phase composition was determined by X-ray diffraction (XRD). The wear behavior of the Cu-Mo-Si alloys was characterized by pin-on-disc wear tester. The results showed that most of Si atoms dissolved in Cu matrix or resulted in formation of compound with Cu, while only small amount of Si atoms reacted with Mo atoms to form Mo5Si3 particles in the Cu-Ni-Si alloys with 80% Cu content. The wear rate of Cu-Mo-Si alloys descended with a decrease of Cu content, and the predominant wear mechanism could be identified as abrasive wear for Cu content less than 90% and plastic deformation for Cu content higher than 90%.

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Self-propagating high-temperature synthesis by the method of X-ray diffraction analysis using synchrotron radiation

Combustion Explosion and Shock Waves ◽

10.1007/bf00783640 ◽

1983 ◽

Vol 19 (4) ◽

pp. 430-431 ◽

Cited By ~ 18

Author(s):

V. V. Aleksandrov ◽

M. A. Korchagin ◽

B. P. Tolochko ◽

M. A. Sheromov

Keyword(s):

High Temperature ◽

Synchrotron Radiation ◽

Diffraction Analysis ◽

X Ray Diffraction ◽

Temperature Synthesis ◽

X Ray ◽

High Temperature Synthesis

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Synthesis of WSi2-W5Si3 Intermetallic Alloy via Self-Propagating High Temperature Synthesis

Solid State Phenomena ◽

10.4028/www.scientific.net/ssp.280.121 ◽

2018 ◽

Vol 280 ◽

pp. 121-126

Author(s):

Si Thu Myint Maung ◽

Tawat Chanadee ◽

Sutham Niyomwas

Keyword(s):

High Temperature ◽

Energy Minimization ◽

Standard Gibbs Energy ◽

Equilibrium Composition ◽

Intermetallic Alloy ◽

X Ray Diffraction ◽

Temperature Synthesis ◽

Minimization Method ◽

X Ray ◽

High Temperature Synthesis

Intermetallic alloy of tungsten silicide (WSi2-W5Si3) was synthesized by self-propagating high temperature synthesis (SHS) from the reactant of tungsten oxide (WO3) and silicon lump (Si) using magnesium (Mg) as fuel. The standard Gibbs energy minimization method was used to calculate the equilibrium composition of the possible reacting species. The as-SHS products were characterized by X-ray diffraction (XRD) technique. The magnesiothermic reaction process successfully synthesized dense of WSi2-W5Si3intermetallic alloy. According to the experimental results, it can be proposed that the reaction also promotes the phase separation between alloy and oxide slag of the product.

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