Small-angle X-ray diffraction investigation of twinned opal-like structures

2012 ◽  
Vol 54 (10) ◽  
pp. 2073-2082 ◽  
Author(s):  
A. K. Samusev ◽  
I. S. Sinev ◽  
K. B. Samusev ◽  
M. V. Rybin ◽  
A. A. Mistonov ◽  
...  
Keyword(s):  
Small Angle ◽  
X Ray Diffraction ◽  
X Ray

Time-resolved isothermal crystallization of absorbable PGA-co-PLA copolymer by synchrotron small-angle X-ray scattering and wide-angle X-ray diffraction

Polymer ◽  
2001 ◽  
Vol 42 (21) ◽  
pp. 8965-8973 ◽  
Author(s):  
Zhi-Gang Wang ◽  
Xuehui Wang ◽  
Benjamin S. Hsiao ◽  
Saša Andjelić ◽  
Dennis Jamiolkowski ◽  
...  
Keyword(s):  
Small Angle ◽  
Isothermal Crystallization ◽  
Wide Angle ◽  
X Ray Diffraction ◽  
Time Resolved ◽  
X Ray ◽  
X Ray Scattering ◽  
Ray Scattering

A high-throughput assembly of beam-shaping channel-cut monochromators for laboratory high-resolution X-ray diffraction and small-angle X-ray scattering experiments

2021 ◽  
Vol 54 (3) ◽  
Author(s):  
Peter Nadazdy ◽  
Jakub Hagara ◽  
Petr Mikulik ◽  
Zdenko Zaprazny ◽  
Dusan Korytar ◽  
...  
Keyword(s):  
High Resolution ◽  
Small Angle ◽  
Photon Flux ◽  
Photon Flux Density ◽  
X Ray Diffraction ◽  
High Beam ◽  
X Ray ◽  
X Ray Scattering ◽  
Beam Collimation ◽  
Ray Scattering

A four-bounce monochromator assembly composed of Ge(111) and Ge(220) monolithic channel-cut monochromators with V-shaped channels in a quasi-dispersive configuration is presented. The assembly provides an optimal design in terms of the highest transmittance and photon flux density per detector pixel while maintaining high beam collimation. A monochromator assembly optimized for the highest recorded intensity per detector pixel of a linear detector placed 2.5 m behind the assembly was realized and tested by high-resolution X-ray diffraction and small-angle X-ray scattering measurements using a microfocus X-ray source. Conventional symmetric and asymmetric Ge(220) Bartels monochromators were similarly tested and the results were compared. The new assembly provides a transmittance that is an order of magnitude higher and 2.5 times higher than those provided by the symmetric and asymmetric Bartels monochromators, respectively, while the output beam divergence is twice that of the asymmetric Bartels monochromator. These results demonstrate the advantage of the proposed monochromator assembly in cases where the resolution can be partially sacrificed in favour of higher transmittance while still maintaining high beam collimation. Weakly scattering samples such as nanostructures are an example. A general advantage of the new monochromator is a significant reduction in the exposure time required to collect usable experimental data. A comparison of the theoretical and experimental results also reveals the current limitations of the technology of polishing hard-to-reach surfaces in X-ray crystal optics.

scholarly journals Исследование кинетики твердофазного перехода в тетракозане С-=SUB=-24-=/SUB=-Н-=SUB=-50-=/SUB=- методом высокоразрешающей синхротронной рентгеновской порошковой дифракции

2019 ◽  
Vol 61 (6) ◽  
pp. 1190
Author(s):  
B.A. Марихин ◽  
П.В. Дороватовский ◽  
Я.B. Зубавичус ◽  
M.B. Байдакова ◽  
E.M. Иванькова ◽  
...  
Keyword(s):  
Phase Transition ◽  
Small Angle ◽  
Diffuse Phase Transition ◽  
Basic Research ◽  
X Ray Diffraction ◽  
Kurchatov Institute ◽  
X Ray ◽  
First Order ◽  
Basic Research Project ◽  
Diffuse Phase

With the help of small angle X-ray diffraction using synchrotron X-ray beamline"Belok" in NRC «Kurchatov Institute» was shown that the first order sold phase transition in the tetracosane C24H50 develops by a heterogeneous mechanism in a very narrow thermal interval (delta ≈0,1K ) in accordance with the theory of diffuse phase transition. The work was financially supported by the Presidium RAN Program №32 "Nanostructures: physics, chemistry, biology, basics of technology" and Russian Foundation of Basic Research (project 16-03-00493А) using beamline "Belok" in NRC

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