Thermoluminescence of irradiated ammonium perchlorate crystals

1976 ◽  
Vol 54 (7) ◽  
pp. 766-770 ◽  
Author(s):  
S. Radhakrishna ◽  
M. Riggin ◽  
P. W. Whippey ◽  
P. W. M. Jacobs

The thermoluminescence of single crystals of ammonium perchlorate irradiated with X rays, uv light, or high energy electrons has been measured between 80 and 420 K. With a heating rate of 5 K/min. prominent peaks occur at 95, 113, 134, 246, and 320 K; an additional peak is found at 347 K after longer irradiation times. The absorption spectrum of uv-irradiated ammonium perchlorate has also been measured and shows bands at 300, 360, and 610 nm. A comparison of these data with chemical and spectroscopic evidence obtained by other workers has permitted the probable identification of ClO3−, ClO−, ClO2, and F centres as radiation products. Three thermoluminescent peaks remain unassigned.

1993 ◽  
Vol 140 (2) ◽  
pp. 353-361 ◽  
Author(s):  
V. I. Vasyltsiv ◽  
Ya. M. Zakharko ◽  
A. O. Matkovskii ◽  
D. Yu. Sugak ◽  
S. B. Ubizskii ◽  
...  

2006 ◽  
Vol 519-521 ◽  
pp. 1569-1578
Author(s):  
Dorte Juul Jensen

By 3 dimensional X-ray diffraction (3DXRD) using high energy X-rays from synchrotron sources it is possible to study in-situ the nucleation and growth during recrystallization. In this paper it is described and discussed how 3DXRD can supplement EBSP measurements of nucleation and growth. Three types of studies are considered: i) orientation relationships between nuclei and parent deformed matrix, ii) recrystallization kinetics of individual bulk grains and iii) filming of growing grains in deformed single crystals.


1974 ◽  
Vol 47 (1) ◽  
pp. 13-14 ◽  
Author(s):  
U. Schiebel ◽  
A. Neufert ◽  
G. Clausnitzer

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