EFFECT OF NANO-Y-ZrO2 ADDITION ON THE MICROSTRUCTURE AND CRITICAL CURRENT DENSITY OF MgB2 SUPERCONDUCTORS

2004 ◽  
Vol 03 (04n05) ◽  
pp. 563-569 ◽  
Author(s):  
Q. W. YAO ◽  
X. L. WANG ◽  
A. H. LI ◽  
S. X. DOU ◽  
P. R. MUNROE
Keyword(s):  
Critical Current Density ◽  
Critical Current ◽  
Current Density ◽  
Magnetic Measurements ◽  
Transmission Electron ◽  
Long Time ◽  
Powder Addition ◽  
Short Time ◽  
Mgb2 Superconductors

Polycrystalline MgB 2 samples with 0, 5, 10, and 20 wt% nano- Y - ZrO 2 (YSZ) powder addition were prepared by short time, as little as several minutes, or long time in-situ reaction process. The phases, microstructures and flux pinning behaviors were characterized using X-ray diffractometry (XRD), Scanning Electron Microscopy (SEM), Transmission Electron Microscope (TEM) and Magnetic Measurements. Results indicated that nano-YSZ particles included in MgB 2 grains. Samples doped with 10wt% YSZ powders showed new record of critical current density Jc as high as 1×106 and 4×106 A/cm 2 in low magnetic fields at 30 and 20K, respectively. However, the Jc drops faster compared to that made by long time sintering samples. It is proposed that the improved Jc in low fields was due to the enhanced density of the sample, which was caused by the YSZ nano-particle inclusion.

STUDY OF THE TEXTURING IN BSCCO-AG TAPES THROUGH MAGNETIC MEASUREMENTS

2000 ◽  
Vol 14 (25n27) ◽  
pp. 3159-3164
Author(s):  
C. FERDEGHINI ◽  
M. R. CIMBERLE ◽  
G. GRASSO ◽  
P. GUASCONI ◽  
A. MALAGOLI ◽  
...  
Keyword(s):  
Magnetic Field ◽  
Critical Current Density ◽  
Critical Current ◽  
Current Density ◽  
Magnetic Measurements ◽  
Texture Evolution ◽  
Rolling Direction ◽  
Longitudinal Direction ◽  
Magnetic Method ◽  
Superconducting Compounds

We have developed a method that allows, by a simple set of magnetic measurements, to study the texturing of the grains inside a BSCCO-Ag tape. Because the texture is anisotropic we define the angle ϑ L that identifies the mean grain misalignment angle with respect to the tape surface in longitudinal direction (i.e. rolling direction) and the angle ϑ T in transverse direction. The technique is based on the assumption that, because of the very high anisotropy of the critical current density in BSCCO superconducting compounds, the magnetic moment is essentially generated by the current circulating in the a-b planes of the BSCCO grains. The different magnetisation cycles, measured when the orientation of the magnetic field with respect to the tape surface is changed, depend only on the grain orientation inside the tape, which determines the effective magnetic field component normal to the a-b planes of the grains. Here we present the texture evolution of the BSCCO grains inside silver sheated multifilamentary tape starting from the initial steps of the mechanical deformation up to the final heating stage. The results obtained from the magnetic method are compared with those obtained with other methods, i.e. X-ray diffraction and critical current density anisotropy. Also results obtained on samples prepared in different way will be presented.

Critical current density and microstructure variations in YBa2Cu3O7−x + BaSnO3 films with different concentrations of BaSnO3

2008 ◽  
Vol 23 (12) ◽  
pp. 3363-3369 ◽  
Author(s):  
C.V. Varanasi ◽  
J. Burke ◽  
L. Brunke ◽  
H. Wang ◽  
J.H. Lee ◽  
...  
Keyword(s):  
Critical Current Density ◽  
Critical Current ◽  
Current Density ◽  
Gradual Increase ◽  
Critical Transition ◽  
Critical Transition Temperature ◽  
Transmission Electron ◽  
Order Of Magnitude ◽  
High Fields ◽  
Magnitude Increase

Previous work on YBa2Cu3O7−x (YBCO) + BaSnO3 (BSO) films with a single composition showed significant critical current density (Jc) improvements at higher fields but lowered Jc in low fields. A detailed study on BSO concentrations provided here demonstrates that significant Jc enhancement can occur even up to 20 mol% BSO inclusion, where typical particulate inclusions in these concentrations degrade the YBCO performance. YBCO + BSO films were processed on (100) LaAlO3 substrates using premixed targets of YBa2Cu3O7-x (YBCO) with additions of 2, 4, 10, and 20 mol% BSO. The critical transition temperature Tc of the films remained high (>87 K), even with large amounts (20 mol%) of BSO. YBCO + BSO films showed a gradual increase in Jc at high fields as the amount of BSO was increased. More than an order of magnitude increase in Jc was measured in YBCO + BSO samples as compared to regular YBCO at 4 T. YBCO + 10 mol% BSO films showed overall improvement at all the field ranges while YBCO + 20 mol% BSO was better only at high fields. Transmission electron microscopy revealed the presence of ∼7–8-nm-diameter BSO nanocolumns, the density of which increased with increasing BSO content correlating well with the observed improvements in Jc.

Critical current density and pinning behaviour of mono-core MgB2 wires prepared by internal magnesium diffusion and in-situ powder-in-tube method

2014 ◽  
Vol 505 ◽  
pp. 39-43 ◽  
Author(s):  
Boris Brunner ◽  
Pavol Kováč ◽  
Michael Reissner ◽  
Imrich Hušek ◽  
Tibor Melišek ◽  
...  
Keyword(s):  
Critical Current Density ◽  
Critical Current ◽  
Current Density ◽  
Mgb2 Wires ◽  
Powder In Tube

YBCO Bulk Superconductors with Sm Addition

2017 ◽  
Vol 891 ◽  
pp. 483-488 ◽  
Author(s):  
Daniela Volochová ◽  
Vitaliy Antal ◽  
Jozef Kováč ◽  
Pavel Diko
Keyword(s):  
Critical Current Density ◽  
Critical Current ◽  
Current Density ◽  
Superconducting Properties ◽  
Ybco Bulk ◽  
Pinning Centers ◽  
Bulk Superconductors ◽  
Powder Addition ◽  
Current Densities ◽  
Precursor Powders

The influence of Sm addition on the microstructure and superconducting properties of Y-Ba-Cu-O (YBCO) bulk superconductors has been studied. Precursor powders YBa2Cu3O7-δ (Y-123), Y2O3 and CeO2 were enriched with different amounts of SmBa2Cu3Oy (Sm-123) or Sm2O3 powders with the aim to increase critical current density, Jc,by introducing additional pinning centers. YBCO bulk superconductors with SmBa2Cu3Oy (Y123-Sm) or Sm2O3 (Y123-SmO) powder addition were prepared by the optimized top seeded melt growth process in the form of single grains. Microstructure analysis revealed that Sm2O3 addition leads to a higher amount of smaller Y2BaCuO5 (Y-211) particles, what is related to high critical current densities (Jc ~ 7 x 104 A/cm2) of the YBCO samples with Sm2O3 addition in low magnetic fields. The effect of Sm addition in the form of SmBa2Cu3Oy as well as Sm2O3 powder on Y2BaCuO5 particle size, critical temperature, Tc, and critical current density, Jc, is reported.

Effect of Pulsed Magnetic Field Processing on MgB2 Superconductors

2007 ◽  
Vol 546-549 ◽  
pp. 2063-2066 ◽  
Author(s):  
W.X. Li ◽  
Ying Li ◽  
M.Y. Zhu ◽  
R.H. Chen ◽  
H.M. Jin ◽  
...  
Keyword(s):  
Magnetic Field ◽  
Critical Current Density ◽  
Critical Current ◽  
Current Density ◽  
Pulsed Magnetic Field ◽  
Pinning Force ◽  
Critical Current Density Jc ◽  
Mgb2 Superconductors ◽  
Doped Mgb2 ◽  
Flux Pinning Force

Pulsed magnetic field was first employed in the study on MgB2 superconductors. Superconductivity properties and microstructures of Zn and SiC doped MgB2 were discussed in this paper. The superconductors showed different superconductivities after magnetic sintering. Critical current density and flux pinning force were relevant to the dopants properties in MgB2. Grains in the pulsed magnetic processed MgB2 matrix were smaller than those in the normal processed one. The refinement microstructures have caused the critical current density (Jc) anisotropy in both the Zn and SiC doped MgB2.

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