Porosity measurements of sedimentary rocks by means of microfocus X-ray computed tomography (μCT)

2003 ◽  
Vol 215 (1) ◽  
pp. 51-60 ◽  
Author(s):  
M. Van Geet ◽  
D. Lagrou ◽  
R. Swennen
Author(s):  
T. F. Johnson ◽  
F. Iacoviello ◽  
J. H. Welsh ◽  
P. R. Shearing ◽  
D. G. Bracewell

AbstractA multiple length scale approach to the imaging and measurement of depth filters using X-ray computed tomography is described. Three different filter grades of varying nominal retention ratings were visualized in 3D and compared quantitatively based on porosity, pore size and tortuosity. Positional based analysis within the filters revealed greater voidage and average pore sizes in the upstream quartile before reducing progressively through the filter from the center to the downstream quartile, with these results visually supported by voidage distance maps in each case. Flow simulation to display tortuous paths that flow may take through internal voidage were examined.Digital reconstructions were capable of identifying individual constituents of voidage, cellulose and perlite inside each depth filter grade, with elemental analysis on upstream and downstream surfaces confirming perlite presence. Achieving an appropriate pixel size was of particular importance when optimizing imaging conditions for all grades examined. A 3 µm pixel size was capable of representing internal macropores of each filter structure; however, for the finest grade, an improvement to a 1 µm pixel size was required in order to resolve micropores and small perlite shards. Enhancing the pixel size resulted in average porosity measurements of 70% to 80% for all grades. Graphical abstract


Author(s):  
Thomas Johnson ◽  
Francesco Iacoviello ◽  
John Welsh ◽  
Paul Shearing ◽  
Daniel Bracewell

A multiple length scale approach to the imaging and measurement of depth filters using X-ray computed tomography is described. Three different filter grades of varying nominal retention ratings were visualized in 3D and compared quantitatively based on porosity, pore size and tortuosity. Positional based analysis within the filters revealed greater voidage and larger average pore sizes in the upstream quartile before reducing progressively through the filter from the center to the downstream quartile, with these results visually supported by voidage distance maps in each case. Flow simulation to display tortuous paths that flow may take through internal voidage were examined. Digital reconstructions were capable of identifying individual constituents of voidage, cellulose and perlite inside each depth filter grade, with elemental analysis on upstream and downstream surfaces confirming perlite presence. Achieving an appropriate pixel size was of particular importance when optimizing imaging conditions for all grades examined. A 3 µm pixel size was capable of representing internal macropores of each filter structure, however for the finest grade an improvement to a 1 µm pixel size was required in order to resolve micropores and small perlite shards. Enhancing pixel size resulted in average porosity measurements of 70% to 80% for all grades.


2021 ◽  
Author(s):  
Yi Zhou ◽  
Michele Pugnetti ◽  
Anneleen Foubert ◽  
Pierre Lanari ◽  
Christoph Neururer ◽  
...  

<p>Magnetic pore fabrics (MPF) are an indirect measure of the 3D pore structure. They are defined by measuring anisotropy of magnetic susceptibility after samples have been impregnated with ferrofluid. Previous studies proposed that MPFs target pores down to 10 nm. Therefore, the method complements X-ray computed tomography (XRCT) datasets, with resolution on the order of 1-10 µm. Empirical relationships exist between MPF and pore fabric, and between MPF and permeability anisotropy. This study investigates quantitative correlations between these three properties, and between measured quantities and digital-rock-model-simulations of permeability anisotropy and MPF. Samples used for this study include natural sedimentary rocks and synthetic samples. Sediments are Plio-Pleistocene calcarenite (Apulia, Italy) with ~50% porosity and complex pore structure, and Upper Marine Molasse sandstone (Belpberg, Switzerland) with 10-20% porosity and relatively homogeneous pore space properties. Synthetic samples were made from quartz sand and calcite powder in different proportions, to simulate sandstone and carbonate rocks. Samples were characterized by pycnometry, XRCT scans, MPF determination and directional permeability measurements to obtain porosity, digital rock models, MPFs and permeability anisotropy. Porosity, permeability anisotropy, and MPFs were also computed based on digital rock models derived from XRCT data, and compared to direct measurements. Permeability anisotropy and MPF are both second-order tensors, representing the average property of the entire sample. To directly relate the XRCT-derived individual pore properties to these second-order tensor quantities, a total shape ellipsoid was computed by adding the second-order tensors reflecting the best-fit ellipsoids of single pores. Once all properties were described by second-order tensors, they were correlated in terms of fabric orientation, degree and shape of anisotropy. The MPF and total shape ellipsoids are coaxial when the samples have sufficiently large pores to be resolved, and good impregnation efficiency, and as expected, total shape ellipsoids have larger anisotropy degree. Preliminary results further indicate that the permeability anisotropy is partly consistent with total shape ellipsoids and MPFs. The defined quantitative relationships facilitate the interpretation of MPF data, thus making the method more applicable to geological and fluid migration studies.</p>


1999 ◽  
Vol 11 (1) ◽  
pp. 199-211
Author(s):  
J. M. Winter ◽  
R. E. Green ◽  
A. M. Waters ◽  
W. H. Green

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