scholarly journals Synthesis of Hydroxyapatite Nanoparticles in Presence of a Linear Polysaccharide

2013 ◽  
Vol 2013 ◽  
pp. 1-5 ◽  
Author(s):  
Humberto A. Monreal Romero ◽  
José Mora Ruacho ◽  
Carlos A. Martínez Pérez ◽  
Perla E. García Casillas
Keyword(s):  
Scanning Tunneling Microscope ◽  
Scanning Tunneling ◽  
Gravimetric Analysis ◽  
Hydroxyapatite Nanoparticles ◽  
X Ray Diffraction ◽  
X Ray ◽  
Peak Intensity ◽  
Bet Analysis ◽  
Ir Analysis ◽  
Natural Hydroxyapatite

Hydroxyapatite nanoparticles compounds were synthesized. Natural hydroxyapatite and a linear polysaccharide (1–3 linked   β-D galactopyranose and 1,4 linked 3,6 anhydro-α-L-galactopyranose) were used as a precursor in its formation. Our purpose was to produce nanoparticles in the presence of a linear polysaccharide with the use of a gelification method. The powder sample was evaluated by scanning tunneling microscope (STM), Brunauer-Emmett-Teller (BET) analysis, X-ray diffraction pattern (XRD), differential thermal analysis (DTA), infrared (IR) analysis, and thermal gravimetric analysis (TGA). According to the results, it was found that these nanoparticles can successfully be synthesized using a polysaccharide in a solution. On the other hand, the XRD peak intensity corresponds to hydroxyapatite structure in the range of temperature of 810°C. The influence of the polysaccharide on the evolution of the nanoparticles has been demonstrated. This observation opens up new routes for the fabrication of nanoparticles using polysaccharides network. The synthesized nanoparticles have diameters ranging from 10 nm to 11 nm approximately. The elaboration conditions such as pH and concentration were optimized in this solution.

scholarly journals Preparation of Chitosan Coated Magnetic Hydroxyapatite Nanoparticles and Application for Adsorption of Reactive Blue 19 and Ni2+Ions

2014 ◽  
Vol 2014 ◽  
pp. 1-9 ◽  
Author(s):  
Van Cuong Nguyen ◽  
Quoc Hue Pho
Keyword(s):  
Removal Efficiency ◽  
Weight Percent ◽  
Textile Dye ◽  
Gravimetric Analysis ◽  
Hydroxyapatite Nanoparticles ◽  
X Ray Diffraction ◽  
X Ray ◽  
Reactive Blue 19 ◽  
Adsorption Capacities ◽  
Initial Ph

An adsorbent called chitosan coated magnetic hydroxyapatite nanoparticles (CS-MHAP) was prepared with the purpose of improvement for the removal of Ni2+ions and textile dye by coprecipitation. Structure and properties of CS-MHAP were characterized by scanning electron microscopy (SEM), X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), and vibrating sample magnetometer (VSM). Weight percent of chitosan was investigated by thermal gravimetric analysis (TGA). The prepared CS-MHAP presents a significant improvement on the removal efficiency of Ni2+ions and reactive blue 19 dye (RB19) in comparison with chitosan and magnetic hydroxyapatite nanoparticles. Moreover, the adsorption capacities were affected by several parameters such as contact time, initial concentration, adsorbent dosage, and initial pH. Interestingly, the prepared adsorbent could be easily recycled from an aqueous solution by an external magnet and reused for adsorption with high removal efficiency.

Roughening of Au(111) Surfaces During Ion Beam Erosion: A Scanning Tunneling Microscope and X-Ray Diffraction Study

1999 ◽  
Vol 570 ◽  
Author(s):  
A. Judy ◽  
M.V. Ramana Murty ◽  
E. Butler ◽  
J. Pomeroy ◽  
B.H. Cooper ◽  
...  
Keyword(s):  
Scanning Tunneling Microscope ◽  
Ion Irradiation ◽  
Ion Beam ◽  
Normal Incidence ◽  
Scanning Tunneling ◽  
Layer By Layer ◽  
X Ray Diffraction ◽  
Tunneling Microscopy ◽  
X Ray ◽  
Glancing Angle

ABSTRACTUsing Scanning Tunneling Microscopy(STM) and X-ray diffraction(XRD), we have studied the development of surface roughness on Au(111) during 500eV Ar+ ion irradiation at different angles. During normal incidence erosion the surface roughens and pattern formation occurs. The surface morphology is a mixture of mounds and pits superimposed onto a larger structure of channels and valleys. The characteristic spacing between features grows with a power law behavior t27, where t is the amount of time the sample was irradiated, in agreement with previous measurements[l]. At glancing angles, erosion proceeds smoothly, but not in layer-by-layer fashion. Finally, a combination of glancing angle and normal incidence erosion is used to create a rippled morphology

Observation of ripple conformations of pβ’ phase of dimyristoyl phosphatidylcholine with the scanning tunneling microscope

1992 ◽  
Vol 50 (2) ◽  
pp. 1134-1135
Author(s):  
John T. Woodward ◽  
Joseph A. N. Zasadzinski
Keyword(s):  
Electron Microscopy ◽  
Scanning Tunneling Microscope ◽  
Freeze Fracture ◽  
Scanning Tunneling ◽  
X Ray Diffraction ◽  
Tunneling Microscope ◽  
X Ray ◽  
Dimyristoyl Phosphatidylcholine ◽  
Freeze Fracture Electron Microscopy ◽  
Ripple Phase

The Pβ’ or ripple phase of lecithin-water systems was first observed with x-ray diffraction by Tardieu, Luzzati and Reman in the early 1970's. The ripple phase has been observed in numerous studies using x-ray diffraction, freeze-fracture electron microscopy, and other spectroscopies. Electron microscopy on lecidiins far above full hydration showed the existence of a second ripple conformation nearly twice the wavelength of the ripples observed below full hydration leading to the designation of Λ and Λ/2 ripples. Yet none of these measurements have been able to provide a direct unambiguous measurement of the ripple amplitude and conformation. By modifying the technique of freeze-fracture replication to make it compatible with the scanning tunneling microscope (STM) we have observed both the Λ/2 ripple conformation and, for the first time with an STM, the Λ ripple conformation of dimyristoyl phosphatidylcholine (DMPC) in water.

scholarly journals Rapid four-component synthesis of dihydropyrano[2,3-c]pyrazoles using nano-eggshell/Ti(IV) as a highly compatible natural based catalyst

BMC Chemistry ◽  
2021 ◽  
Vol 15 (1) ◽  
Author(s):  
Arefeh Dehghani Tafti ◽  
Bi Bi Fatemeh Mirjalili ◽  
Abdolhamid Bamoniri ◽  
Naeimeh Salehi
Keyword(s):  
Thermo Gravimetric Analysis ◽  
Reaction Times ◽  
Diffraction Field ◽  
Gravimetric Analysis ◽  
X Ray Diffraction ◽  
X Ray ◽  
Solvent Free Conditions ◽  
High Yields ◽  
Work Up

AbstractNano-eggshell/Ti(IV) as a novel naturally based catalyst was prepared, characterized and applied for the synthesis of dihydropyrano[2,3-c]pyrazole derivatives. The characterization of nano-eggshell/Ti(IV) was performed using Fourier Transform Infrared spectroscopy, X-ray Diffraction, Field Emission Scanning Electron Microscopy, Energy-Dispersive X-ray Spectroscopy, and Thermo Gravimetric Analysis. Dihydropyrano[2,3-c]pyrazoles were synthesized in the presence of nano-eggshell/Ti(IV) via a four component reaction of aldehydes, ethyl acetoacetate, malononitrile and hydrazine hydrate at room temperature under solvent free conditions. The principal affairs of this procedure are mild condition, short reaction times, easy work-up, high yields, reusability of the catalyst and the absence of toxic organic solvents.

scholarly journals Interface morphology of a Cr(001)/Fe(001) superlattice determined by scanning tunneling microscopy and x-ray diffraction: A comparison

2001 ◽  
Vol 89 (1) ◽  
pp. 181-187 ◽  
Author(s):  
C. M. Schmidt ◽  
D. E. Bürgler ◽  
D. M. Schaller ◽  
F. Meisinger ◽  
H.-J. Güntherodt ◽  
...  
Keyword(s):  
Scanning Tunneling Microscopy ◽  
Scanning Tunneling ◽  
Interface Morphology ◽  
X Ray Diffraction ◽  
Tunneling Microscopy ◽  
X Ray

scholarly journals Enhanced Photocatalytic Activity of Cu2O Cabbage/RGO Nanocomposites under Visible Light Irradiation

Polymers ◽  
2021 ◽  
Vol 13 (11) ◽  
pp. 1712
Author(s):  
Appusamy Muthukrishnaraj ◽  
Salma Ahmed Al-Zahrani ◽  
Ahmed Al Otaibi ◽  
Semmedu Selvaraj Kalaivani ◽  
Ayyar Manikandan ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Thermo Gravimetric Analysis ◽  
Visible Region ◽  
Catalytic Performance ◽  
Precipitation Method ◽  
Gravimetric Analysis ◽  
X Ray Diffraction ◽  
X Ray ◽  
Dye Pollutants ◽  
Transmission Electron

Towards the utilization of Cu2O nanomaterial for the degradation of industrial dye pollutants such as methylene blue and methyl orange, the graphene-incorporated Cu2O nanocomposites (GCC) were developed via a precipitation method. Using Hummers method, the grapheme oxide (GO) was initially synthesized. The varying weight percentages (1–4 wt %) of GO was incorporated along with the precipitation of Cu2O catalyst. Various characterization techniques such as Fourier-transform infra-red (FT-IR), X-ray diffraction (XRD), UV–visible diffused reflectance (UV-DRS), Raman spectroscopy, thermo gravimetric analysis (TGA), energy-dispersive X-ray analysis (EDX), and electro chemical impedance (EIS) were followed for characterization. The cabbage-like morphology of the developed Cu2O and its composites were ascertained from field-emission scanning electron microscopy (FESEM) and high-resolution transmission electron microscopy (HR-TEM). In addition, the growth mechanism was also proposed. The results infer that 2 wt % GO-incorporated Cu2O composites shows the highest value of degradation efficiency (97.9% and 96.1%) for MB and MO at 160 and 220 min, respectively. Further, its catalytic performance over visible region (red shift) was also enhanced to an appreciable extent, when compared with that of other samples.

Effect of Synthesis Temperature on Particles Size and Morphology of Zirconium Oxide Nanoparticle

2017 ◽  
Vol 50 ◽  
pp. 18-31 ◽  
Author(s):  
Rudzani Sigwadi ◽  
Simon Dhlamini ◽  
Touhami Mokrani ◽  
Patrick Nonjola
Keyword(s):  
Electron Microscopy ◽  
Particle Size ◽  
Zirconium Oxide ◽  
Thermo Gravimetric Analysis ◽  
Gravimetric Analysis ◽  
X Ray Diffraction ◽  
X Ray ◽  
Transmission Electron ◽  
Crystallite Sizes ◽  
Ft Ir

The paper presents the synthesis and investigation of zirconium oxide (ZrO2) nanoparticles that were synthesised by precipitation method with the effects of the temperatures of reaction on the particles size, morphology, crystallite sizes and stability at high temperature. The reaction temperature effect on the particle size, morphology, crystallite sizes and stabilized a higher temperature (tetragonal and cubic) phases was studied. Thermal decomposition, band structure and functional groups were analyzed by Brunauer-Emmett-Teller (BET), Scanning Electron Microscopy (SEM), Transmission electron microscopy (TEM), X-ray diffraction (XRD), Thermo-gravimetric analysis (TGA) and Fourier transform infrared (FT-IR). The crystal structure was determined using X-ray diffraction. The morphology and the particle size were studied using (SEM) and (TEM). The shaped particles were confirmed through the SEM analysis. The transmission electron microscopic analysis confirmed the formation of the nanoparticles with the particle size. The FT-IR spectra showed the strong presence of ZrO2 nanoparticles.

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