Fabrication of high-density polyethylene/multiwalled carbon nanotube composites via submerged friction stir processing

2016 ◽  
Vol 30 (2) ◽  
pp. 241-254 ◽  
Author(s):  
Jicheng Gao ◽  
Yifu Shen ◽  
Chao Li

The focus of this work was to study the effect of multiwalled carbon nanotubes (MWCNTs) on morphology, mechanical, and thermal properties of high-density polyethylene (HDPE) nanocomposites. MWCNTs/HDPE nanocomposites were prepared using submerged friction stir processing (SFSP) technique. The pristine MWCNTs without any pretreatment were blended with HDPE at a fixed traverse speed of 30 mm min−1 and various rotational speeds ranging from 1200 r min−1 to 2100 r min−1. The effect of rotational speed on MWCNTs dispersion in HDPE matrix was assessed using scanning electron microscopy. The experimental results showed the rotational speed affected the disperision of the MWCNTs. The mechanical properties of the composites were measured, and the results indicated that the tensile strength increased at first and then decreased with the increase of the rotation speed. The thermal properties of MWCNTs-filled HDPE nanocomposites were studied by differential scanning calorimetry, and the crystalline content of the prepared composites by the SFSP technology was increased. From the experimental research, it was found that the SFSP technique was a practical way to fabricate polymeric composites.

Author(s):  
Jicheng Gao ◽  
Chao Li ◽  
Yifu Shen

The aim of this work is to fabricate the high-density polyethylene–copper composites by submerged friction stir processing at different traverse speeds. The scanning electron microscopy is used to analyze the distribution of microstructure and particles. The experimental results indicated that the macrostructure morphology, microstructure and tensile strength vary depending on the traverse speed. Compared with the pure high-density polyethylene, Cu-filled polymer composites showed lower tensile strength and higher microhardness. The maximal values of the tensile strength and microhardness were achieved at traverse speeds of 30 and 15 mm/min, respectively. The thermal properties of Cu-filled high-density polyethylene composites were studied by differential scanning calorimetry. The crystalline content of the composites was decreased due to the addition of copper. From the experimental tests, it can be concluded that submerged fiction stir processing has a great potential for producing polymer–metal composites.


2018 ◽  
Vol 97 (5-8) ◽  
pp. 2489-2499 ◽  
Author(s):  
Mirley Moreno-Moreno ◽  
Yorledis Macea Romero ◽  
Habib Rodríguez Zambrano ◽  
Nora Catalina Restrepo-Zapata ◽  
Conrado Ramos Moreira Afonso ◽  
...  

2017 ◽  
pp. 1293-1305
Author(s):  
G. Venkateswarlu ◽  
M.J. Davidson ◽  
G.R.N. Tagore ◽  
P. Sammaiah

Friction stir processing (FSP) has been developed on the principles of friction stir welding (FSW) as an effective and efficien new method for grain refinement and microstructural modification, providing intense plastic deformation as well as higher strain rates than other conventional severe plastic deformation methods. FSP produces an equiaxed homogeneous microstructure consisting of fine grains, resulting in the enhancement of the properties of the material at room temperature. The objective of the present paper is to examine the influence of friction stir processing (FSP) parameters namely tool rotational speed (RS), tool traverse speed (TS) and tool tilt angle (TA) on the microstructures of friction stir processed AZ31B-O magnesium alloy. This investigation has focused on the microstructural changes occurred in the dynamically recrystallised nugget zone/ stir zone and the thermo mechanically affected zone during FSP. The results presented in this work indicate that all the three FSP process parameters have a significant effect on the resulting microstructure and also found that the rotational speed has greatly influenced the homogenization of the material. The grain refinement is higher at intermediate rotational speed (1150 rpm), traverse speed (32 mm / min and tilt angle (10). It is established that FSP can be a good grain refinement method for improving the properties of the material.


2013 ◽  
Vol 818 ◽  
pp. 14-19 ◽  
Author(s):  
Vahid Rezazadeh ◽  
Ali Sharbatzadeh ◽  
Ali Hosseinzadeh ◽  
Amir Safari ◽  
Salar Salahi

mproving ductility in metals using friction stir processing (FSP) is a challenging effort and is made by means of a rotating tool inserted in a work piece providing heat transfer and plastic deformation. In this investigation, improving ductility during FSP was determined as a purpose and the microstructure and mechanical properties of nugget zone were investigated during friction stir processing (FSP) of pure copper. Ductility was measured using tensile elongations at a temperature of 20 °C. By varying the traverse speed from 40 to 100 mm/min at rotation speeds of 300 and 600 rpm, the ultrafine grain microstructure was achieved .Defects were observed in rotational speed of 300 rpm. By increasing traverse speed at constant rotational speed of 600 rpm grain size of the nugget zone decreased and ductility increased. Achievable ductility was limited by cavity formation due to lower heat input and deformation in samples with defects.


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