Statistical methods to enable practical on-site tomographic imaging of whole-core samples

Geophysics ◽  
2019 ◽  
Vol 84 (3) ◽  
pp. D89-D100 ◽  
Author(s):  
Alberto Mendoza ◽  
Lassi Roininen ◽  
Mark Girolami ◽  
Jere Heikkinen ◽  
Heikki Haario

Statistical methods enable the use of portable industrial scanners with sparse measurements, suitable for fast on-site whole-core X-ray computed tomography (CT), as opposed to conventional (medical) devices that use dense measurements. This approach accelerates an informed first-stage general assessment of core samples. To that end, this novel industrial tomographic measurement principle is feasible for rock-sample imaging, in conjunction with suitable forms of priors in Bayesian inversion algorithms. Gaussian, Cauchy, and total variation priors yield different inversion characteristics for similar material combinations. An evaluation of the inversion performance in rock samples considers, in a discrete form, conditional mean estimators, via Markov Chain Monte Carlo algorithms with noise-contaminated measurements. Additionally, further assessment indicates that this statistical approach better characterizes the attenuation contrast of rock materials, compared with simultaneous iterative reconstruction techniques. Benchmarking includes X-ray CT from numerical simulations of synthetic and measurement-based whole-core samples. To this end, we consider tomographic measurements of fine- to medium-grained sandstone core samples, with igneous-rich pebbles from the Miocene, off the Shimokita Peninsula in Japan, and fractured welded tuff from Big Bend National Park, Texas. Bayesian inversion results confirm that with only 16 radiograms, natural fractures with aperture of less than 2 mm wide are detectable. Additionally, reconstructed images found approximately spherical concretions of 6 mm diameter. To achieve similar results, filtered back projection techniques require hundreds of radiograms, only possible with conventional laboratory scanners.

2006 ◽  
Vol 25 (2) ◽  
pp. 218-228 ◽  
Author(s):  
V. Kolehmainen ◽  
A. Vanne ◽  
S. Siltanen ◽  
S. Jarvenpaa ◽  
J.P. Kaipio ◽  
...  

2010 ◽  
Vol 1 (MEDSI-6) ◽  
Author(s):  
M. Nicola ◽  
H. P. van der Kleij

For some beamlines, where the X-ray beam is focussed to less than 100 nm spot size, it is necessary to rotate the sample using very accurate rotary axes. The accuracy of these devices is defined in terms of radial, axial and tilt errors. At the Precision Engineering Laboratory of the ESRF, we are able to calibrate rotary stages and spindles in agreement with the ISO 230-7 and ASME B89.3.4 standards, in static mode (step by step, at given position increments) or in continuous motion. This type of measurement is possible through the use of non-contact capacitive sensors (with measuring resolution in the field of the nanometre) and reference spherical artefacts, working under controlled environmental conditions to minimize the influence of thermal instabilities. The setup includes a special granite stage with a gantry, supported by an active anti-vibration system. The presentation will illustrate the measurement principle and some examples of calibrations, including results obtained on a motorized air-bearing rotary stage for which the measured errors are about 20 nm.


CATENA ◽  
2020 ◽  
Vol 189 ◽  
pp. 104506 ◽  
Author(s):  
Radu Gabriel Pîrnău ◽  
Cristian Valeriu Patriche ◽  
Bogdan Roşca ◽  
Ionuţ Vasiliniuc ◽  
Nicoleta Vornicu ◽  
...  

SPE Journal ◽  
2011 ◽  
Vol 16 (03) ◽  
pp. 683-691 ◽  
Author(s):  
N.. Watanabe ◽  
T.. Ishibashi ◽  
N.. Hirano ◽  
N.. Tsuchiya ◽  
Y.. Ohsaki ◽  
...  

Summary The present study focuses on the feasibility of a precise 3D numerical modeling coupled with X-ray computed tomography (CT), which enables simple analysis of heterogeneous fracture flows within reservoir core samples, as well as the measurement of porosity and permeability. A numerical modeling was developed and applied to two fractured granite core samples. One of the samples had an artificial single fracture (sample dimensions: 100 mm in diameter, 150 mm in length), and the other had natural multiple fractures (sample dimensions: 100 mm in diameter, 120 mm in length). A linear relationship between the CT value and the fracture aperture (fracture-aperture calibration curve) was obtained by X-ray CT scanning for a fracture-aperture calibration standard while varying the aperture from 0.1 to 0.5 mm. With the fracture-aperture calibration curve, 3D distributions of the CT value for the samples (voxel dimensions: 0.35×0.35×0.50 mm3) were converted into fracture-aperture distributions in order to obtain fracture models for these samples. The numerical porosities reproduced the experimental porosities within factors of approximately 1.3 and 1.1 for the single fracture and the multiple fractures, respectively. Using the fracture models, a single-phase flow simulation was also performed with a local cubic law-based fracture-flow model for steady-state laminar flow of a viscous and incompressible fluid. The numerically obtained permeabilities were larger than the experimentally obtained permeabilities by factors of approximately 2.2 and 2.7 for the single fracture and the multiple fractures, respectively. However, these discrepancies can be reduced to approximately 1.3—2.1 and 1.6-2.6, respectively, by simply using the correction factor for the cubic-law equation proposed by Witherspoon et al. (1980). Consequently, a precise numerical modeling coupled with X-ray CT is essentially feasible. Furthermore, the development of preferential flow paths (i.e., channeling flow) was clearly demonstrated for multiple fractures, which is much more challenging to achieve by most other methods. Further progress in modeling should enable the in-situ evaluation of heterogeneous fracture flow within reservoir core samples, as well as the clarification of the impacts of the heterogeneity on the productivity of wells and, for example, the efficiency of recovery by water-/gasflooding.


1990 ◽  
Vol 5 (04) ◽  
pp. 475-480 ◽  
Author(s):  
A.O. Hove ◽  
Victor Nilsen ◽  
Jorgen Leknes
Keyword(s):  
X Ray ◽  

2020 ◽  
Author(s):  
Rocky D. Barker ◽  
Shaun L.L. Barker ◽  
Siobhan A. Wilson ◽  
Elizabeth D. Stock

Abstract Mineral distributions can be determined in drill core samples from a Carlin-type gold deposit, using micro-X-ray fluorescence (µXRF) raster data. Micro-XRF data were collected using a Bruker Tornado µXRF scanner on split drill core samples (~25 × 8 cm) with data collected at a spatial resolution of ~100 µm. Bruker AMICS software was used to identify mineral species from µXRF raster data, which revealed that many individual sample spots were mineral mixtures due to the fine-grained nature of the samples. In order to estimate the mineral abundances in each pixel, we used a linear programming (LP) approach on quantified µXRF data. Quantification of µXRF spectra was completed using a fundamental parameters (FP) standardless approach. Results of the FP method compared to standardized wavelength dispersive spectrometry (WDS)-XRF of the same samples showed that the FP method for quantification of µXRF spectra was precise (R2 values of 0.98–0.97) although the FP method gave a slight overestimate of Fe and K and an underestimate of Mg abundance. Accuracy of the quantified µXRF chemistry results was further improved by using the WDS-XRF data as a calibration correction before calculating mineralogy using LP. The LP mineral abundance predictions were compared to Rietveld refinement results using X-ray diffraction (XRD) patterns collected from powders of the same drill core samples. The root mean square error (RMSE) for LP-predicted mineralogy compared to quantitative XRD results ranges from 0.91 to 7.15% for quartz, potassium feldspar, pyrite, kaolinite, calcite, dolomite, and illite. The approaches outlined here demonstrates that µXRF maps can be used to determine mineralogy, mineral abundances, and mineralogical textures not visible with the naked eye from fine-grained sedimentary rocks associated with Carlin-type Au deposits. This approach is transferrable to any ore deposit, but particularly useful in sedimentary-hosted ore deposits where ore and gangue minerals are often fine grained and difficult to distinguish in hand specimen.


Sign in / Sign up

Export Citation Format

Share Document