Characterization of mechanical properties of rocks by microindentation test—A new method for testing rock properties

2008 ◽  
pp. 211-216
2021 ◽  
Author(s):  
Umesh Prasad ◽  
Amer Hanif ◽  
Ian McGlynn ◽  
Frank Walles ◽  
Ahmed Abouzaid ◽  
...  

Abstract The influences of mineralogy on rock mechanical properties have profound application in oil and gas exploration and production processes, including hydraulic fracturing operations. In conventional resources, the rock mechanical properties are predominantly controlled by porosity; however, in unconventional tight formations, the importance of mineralogy as a function of rock mechanical properties has not been fully investigated. In unconventional tight formations, mechanical properties are often derived from mineralogy weight fraction together with the best estimate of porosity, assumption of fluid types, the extent of pore fillings, and fluid properties. These properties are then adjusted for their volumetric fractions and subsequently calibrated with acoustics or geomechanical lab measurements. A new method is presented that utilizes mineralogy weight fractions (determined from well logs or laboratory measurements). This process uses public domain information of minerals using Voigt and Reuss averaging algorithms as upper and lower bounds, respectively. An average of these bounds (also known as Hill average) provides a representative value for these parameters. Further, based on isotropic conditions, all the elastic properties are calculated. A typical output consisting of bulk-, shear-, and Young's - modulus, together with Poisson's ratio obtained from traditional methods of volume fractions and this new method using weight fractions is discussed and analyzed along with the sensitivity and the trends for individual rock properties. Furthermore, corresponding strengths, hardness, and fracture toughness could also be estimated using well known public domain algorithms. Data from carbonate reservoirs has been discussed in this work. This method shows how to estimate grain compressibility that can be challenging to be measured in the lab for unconventional tight rock samples. In low-porosity samples, the relative influence of porosity is negligible compared to the mineralogy composition. This approach reduces several assumptions and uncertainties associated with accurate porosity determination in tight rocks as it does not require the amount of pore fluids and fluid properties in calculations. The grain-compressibility and bulk-compressibility (measured by hydrostatic tests in the laboratory on core plugs or calculated from density and cross-dipole log) are used to calculate poroelastic Biot's coefficient, as this coefficient will be used to calculate in-situ principal effective stresses (overburden, minimum horizontal, and maximum horizontal stresses), which are, together with rock properties and pore pressure, constitutes the geomechanical model. The geomechanical model is used for drilling, completions, and hydraulic fracture modeling, including wellbore stability, and reservoir integrity analyses.


2003 ◽  
Vol 67 (5) ◽  
pp. 967-987 ◽  
Author(s):  
P. F. Schofield ◽  
S. J. Covey-Crump ◽  
I. C. Stretton ◽  
M. R. Daymond ◽  
K. S. Knight ◽  
...  

AbstractConventional experiments designed to investigate the mechanical properties of polycrystalline geological materials are generally restricted to measurements of whole-rock properties. However, when comparing the measurements with theoretical models, it is frequently essential to understand how the deformation is accommodated at the grain-scale. This is particularly true for polymineralic rocks because in this case most theories express the whole-rock properties as some function of the properties of their constituent minerals, and hence the contribution which each phase makes to those properties must be measured if the theories are to be fully assessed. The penetrating nature of neutrons offers a method of addressing this problem. By performing deformation experiments in the neutron beam-line and collecting neutron diffraction patterns at different applied loads, the lattice parameters of all the mineral phases present may be determined as a function of load. The elastic strain experienced by each phase is then easily determined. Moreover, the strain in different lattice directions is also obtained. From this information a wide range of problems relevant for the characterization of the elastic and plastic deformation behaviour of polymineralic geological materials can be explored. An experimental technique for carrying out such experiments is described, and its validity is demonstrated by showing that the results obtained from deforming an elastically isotropic olivine + magnesiowüstite sample agree, to within very tight bounds, with the behaviour predicted by theory for elastically isotropic composites.


2020 ◽  
Vol 43 (3) ◽  
Author(s):  
Lithiely Melo de Lima ◽  
José Agnelo Soares

In this article are presented the results obtained for the determination of mineral composition and petrophysical properties of eight sedimentary rock samples through a proposed new method, which is supported by X-ray microtomography image analysis (microCT). The results are compared with their corresponding ones obtained by traditional techniques in order to assess the efficiency of the new method. Three samples of carbonate rocks and five of sandstone were used in this study. Two sandstone samples come from the Rio do Peixe basin (BRP, at northeastern Brazil) while the rest were extracted from USA basins. The best results were obtained in the quantification of the mineral composition of the rocks and, consequently, in the estimation of grain density. Due to its insufficient image resolution, the microtomography was sometimes unable to quantify very small pores, giving low porosity values. The correlation between bulk densities measured by the two methods shows an intermediate efficiency. Although the results presented here indicate that the microCT image analysis is appropriate for quantification of mineral phases, this technique has potential for determination of many other physical properties, such as mechanical, electrical and fluid flow rock properties.


Author(s):  
Gyeung Ho Kim ◽  
Mehmet Sarikaya ◽  
D. L. Milius ◽  
I. A. Aksay

Cermets are designed to optimize the mechanical properties of ceramics (hard and strong component) and metals (ductile and tough component) into one system. However, the processing of such systems is a problem in obtaining fully dense composite without deleterious reaction products. In the lightweight (2.65 g/cc) B4C-Al cermet, many of the processing problems have been circumvented. It is now possible to process fully dense B4C-Al cermet with tailored microstructures and achieve unique combination of mechanical properties (fracture strength of over 600 MPa and fracture toughness of 12 MPa-m1/2). In this paper, microstructure and fractography of B4C-Al cermets, tested under dynamic and static loading conditions, are described.The cermet is prepared by infiltration of Al at 1150°C into partially sintered B4C compact under vacuum to full density. Fracture surface replicas were prepared by using cellulose acetate and thin-film carbon deposition. Samples were observed with a Philips 3000 at 100 kV.


Author(s):  
K.L. More ◽  
R.A. Lowden

The mechanical properties of fiber-reinforced composites are directly related to the nature of the fiber-matrix bond. Fracture toughness is improved when debonding, crack deflection, and fiber pull-out occur which in turn depend on a weak interfacial bond. The interfacial characteristics of fiber-reinforced ceramics can be altered by applying thin coatings to the fibers prior to composite fabrication. In a previous study, Lowden and co-workers coated Nicalon fibers (Nippon Carbon Company) with silicon and carbon prior to chemical vapor infiltration with SiC and determined the influence of interfacial frictional stress on fracture phenomena. They found that the silicon-coated Nicalon fiber-reinforced SiC had low flexure strengths and brittle fracture whereas the composites containing carbon coated fibers exhibited improved strength and fracture toughness. In this study, coatings of boron or BN were applied to Nicalon fibers via chemical vapor deposition (CVD) and the fibers were subsequently incorporated in a SiC matrix. The fiber-matrix interfaces were characterized using transmission and scanning electron microscopy (TEM and SEM). Mechanical properties were determined and compared to those obtained for uncoated Nicalon fiber-reinforced SiC.


Author(s):  
Thais Helena Sydenstricker Flores-Sahagun ◽  
Kelly Priscila Agapito ◽  
ROSA MARIA JIMENEZ AMEZCUA ◽  
Felipe Jedyn

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